Preparation of Mesophase Pitch through Supercritical Fluid Extraction of Coal Tar Pitch.
Journal
ACS omega
ISSN: 2470-1343
Titre abrégé: ACS Omega
Pays: United States
ID NLM: 101691658
Informations de publication
Date de publication:
13 Feb 2024
13 Feb 2024
Historique:
received:
18
10
2023
revised:
24
12
2023
accepted:
19
01
2024
medline:
19
2
2024
pubmed:
19
2
2024
entrez:
19
2
2024
Statut:
epublish
Résumé
This paper explores the preparation of mesophase pitch by employing supercritical fluid extraction on coal tar pitch sourced from a coal chemical company. The raw material undergoes pretreatment using various extraction solvents, and the resulting refined components are thermally polycondensed in a laboratory microreactor to create mesophase pitch. Qualitative and quantitative analyses of the mesophase pitch's structure are conducted through polarized light microscopy, X-ray diffraction (XRD), scanning electron microscopy (SEM), Raman spectroscopy, and other analytical methods to identify an optimal supercritical fluid extraction pretreatment solvent for coal tar pitch. The results reveal that using
Identifiants
pubmed: 38371791
doi: 10.1021/acsomega.3c08206
pmc: PMC10870362
doi:
Types de publication
Journal Article
Langues
eng
Pagination
6837-6844Informations de copyright
© 2024 The Authors. Published by American Chemical Society.
Déclaration de conflit d'intérêts
The authors declare no competing financial interest.