Fluorine labelling for in situ

Fluorine NMR shift anisotropy orientation biomolecule

Journal

Journal of biomolecular NMR
ISSN: 1573-5001
Titre abrégé: J Biomol NMR
Pays: Netherlands
ID NLM: 9110829

Informations de publication

Date de publication:
26 Feb 2024
Historique:
received: 15 06 2023
accepted: 14 02 2024
medline: 26 2 2024
pubmed: 26 2 2024
entrez: 26 2 2024
Statut: aheadofprint

Résumé

The focus of this project is to take advantage of the large NMR chemical shift anisotropy of

Identifiants

pubmed: 38407676
doi: 10.1007/s10858-024-00438-7
pii: 10.1007/s10858-024-00438-7
doi:

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Subventions

Organisme : University of Alberta Faculty of Medicine Transitional Program.
ID : RES0058893

Informations de copyright

© 2024. The Author(s), under exclusive licence to Springer Nature B.V.

Références

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doi: 10.1021/acs.jmedchem.5b01447 pubmed: 26599421
Crowley PB, Kyne C, Monteith WB (2012) Simple and inexpensive incorporation of 19F-Tryptophan for protein NMR spectroscopy Chem. Commun 48:10681–10683. https://doi.org/10.1039/c2cc35347d
doi: 10.1039/c2cc35347d
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doi: 10.1021/acs.jmedchem.8b01210 pubmed: 30295487
DeVries JS, Zhao X, and Sykes BD (2007) A 19F and 1H goniometer split-minicoil NMR probe for solid-state NMR. Concepts in Magnetic Resonance Part B 31B (4):203–208
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Robertson IM, Klein BA, Sykes BD (2020) Optimizing fluorine labelling for 19F solid-state NMR in oriented biological systems. J Biomol NMR 74:1–7. https://doi.org/10.1007/s10858-019-00296-8
doi: 10.1007/s10858-019-00296-8 pubmed: 31912345
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Zhao X, DeVries JS, McDonald R, Sykes (2007) BD determination of the 19F NMR chemical shielding tensor and crystal structure of 5-fluoro-dl-tryptophan. J Mag Res 187(1):88–96. https://doi.org/10.1016/j.jmr.2007.03.022
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Auteurs

Kieran T Cockburn (KT)

Department of Biochemistry, University of Alberta, Edmonton, AB, T6G2H7, Canada.

Brian D Sykes (BD)

Department of Biochemistry, University of Alberta, Edmonton, AB, T6G2H7, Canada. brian.sykes@ualberta.ca.

Classifications MeSH