Zn complexed on hybrid manganese doped cobalt ferrite nanoparticles covered by silica as a catalyst in the synthesis of 2-amino-4
2-Amino-4H-pyrans
Green chemistry
Magnetic nanoparticles
N- arylquinolines
Nanocatalyst
Journal
Heliyon
ISSN: 2405-8440
Titre abrégé: Heliyon
Pays: England
ID NLM: 101672560
Informations de publication
Date de publication:
15 May 2024
15 May 2024
Historique:
received:
26
01
2024
revised:
27
04
2024
accepted:
30
04
2024
medline:
20
5
2024
pubmed:
20
5
2024
entrez:
20
5
2024
Statut:
epublish
Résumé
In the present work, Zn complexed on hybrid manganese doped cobalt ferrite nanoparticles covered by silica were synthesized. These MNPs were characterized using different techniques including Fourier-transform infrared spectroscopy (FT-IR), X-ray diffraction analysis (XRD), Field emission-scanning electron micro-scope (FE-SEM), Energy-dispersive X-ray spectroscopy (EDS), Vibration sample magnetometer (VSM), Inductively coupled plasma atomic emission spectroscopy (ICP), Zeta potential and Thermogravimetric analysis (TGA). FE-SEM Images showed uniform spherical shape with rough surfaces and an aggregation in structure of MNPs. A decrease in Ms is visible in VSM analysis due to the increase in particle diameter as a result of loading the organic coating on the surface of the magnetic nanoparticles. According to TGA analysis, the synthesized MNPs have good stability up to 125 °C. The ICP analysis indicates the presence of 0.13 mmol/g zinc on the surface of loaded MNPs. The effect of these prepared MNPs as a catalyst was studied in the synthesis of 2-amino-4
Identifiants
pubmed: 38765097
doi: 10.1016/j.heliyon.2024.e30620
pii: S2405-8440(24)06651-9
pmc: PMC11098855
doi:
Types de publication
Journal Article
Langues
eng
Pagination
e30620Informations de copyright
© 2024 The Authors. Published by Elsevier Ltd.
Déclaration de conflit d'intérêts
The authors declare the following financial interests/personal relationships which may be considered as potential competing interests: Akbar Mobinikhaledi reports was provided by Arak University. Akbar Mobinikhaledi reports a relationship with Arak University that includes: employment. Akbar Mobinikhaledi has patent pending to: No patent. Authors have no relevant financial or non-financial interests to disclose. If there are other authors, they declare that they have no known competing financial interests or personal relationships that could have appeared to influence the work reported in this paper.