Effect of applying carbodiimide combined with a two-step self-etch adhesive durability.
Humans
Carbodiimides
/ chemistry
Resin Cements
/ chemistry
Shear Strength
Materials Testing
Dentin
Microscopy, Electron, Scanning
Dentin-Bonding Agents
/ chemistry
Dental Stress Analysis
Cross-Linking Reagents
/ chemistry
Dental Bonding
/ methods
In Vitro Techniques
Acid Etching, Dental
/ methods
Molar, Third
Temperature
Time Factors
Surface Properties
Aging
Carbodiimide
Dentin bonding agent
Shear strength
Journal
BMC oral health
ISSN: 1472-6831
Titre abrégé: BMC Oral Health
Pays: England
ID NLM: 101088684
Informations de publication
Date de publication:
07 Jun 2024
07 Jun 2024
Historique:
received:
28
02
2024
accepted:
27
05
2024
medline:
8
6
2024
pubmed:
8
6
2024
entrez:
7
6
2024
Statut:
epublish
Résumé
This study investigated the effect of carbodiimide (EDC) combined with Clearfil SE self-etch adhesive on the shear bond strength (SBS), crosslinking degree, denaturation temperature, and enzyme activity of dentin in vitro. Collected human sound third molars were randomly divided into different groups with or without EDC treatment (0.01-1 M). The specimens (n = 16)were stored for 24 h (immediate) or 12 months (aging) before testing the SBS. Fine dentin powder was obtained and treated with the same solutions. Then the crosslinking degree, denaturation temperature (Td), and enzyme activity were tested. Statistical analysis was performed using a one-way analysis of variance (ANOVA) to compare the differences of data between groups (α = 0.05). There was a significant drop in immediate SBS and more adhesive fracture of 1.0 M EDC group, while there were no significant differences among the other groups. SEM showed a homogeneous interface under all treatments. After 12 months of aging, the SBS significantly decreased. Less decreases of SBS in the 0.3 and 0.5 M groups were found. Due to thermal and enzymatical properties consideration, the 0.3 and 0.5 M treatments also showed higher cross-link degree and Td with lower enzyme activity. 0.3 and 0.5 M EDC may be favorable for delaying the aging of self-etch bond strength for 12 months. But it is still needed thoroughly study.
Sections du résumé
BACKGROUND
BACKGROUND
This study investigated the effect of carbodiimide (EDC) combined with Clearfil SE self-etch adhesive on the shear bond strength (SBS), crosslinking degree, denaturation temperature, and enzyme activity of dentin in vitro.
MATERIALS AND METHODS
METHODS
Collected human sound third molars were randomly divided into different groups with or without EDC treatment (0.01-1 M). The specimens (n = 16)were stored for 24 h (immediate) or 12 months (aging) before testing the SBS. Fine dentin powder was obtained and treated with the same solutions. Then the crosslinking degree, denaturation temperature (Td), and enzyme activity were tested. Statistical analysis was performed using a one-way analysis of variance (ANOVA) to compare the differences of data between groups (α = 0.05).
RESULTS
RESULTS
There was a significant drop in immediate SBS and more adhesive fracture of 1.0 M EDC group, while there were no significant differences among the other groups. SEM showed a homogeneous interface under all treatments. After 12 months of aging, the SBS significantly decreased. Less decreases of SBS in the 0.3 and 0.5 M groups were found. Due to thermal and enzymatical properties consideration, the 0.3 and 0.5 M treatments also showed higher cross-link degree and Td with lower enzyme activity.
CONCLUSION
CONCLUSIONS
0.3 and 0.5 M EDC may be favorable for delaying the aging of self-etch bond strength for 12 months. But it is still needed thoroughly study.
Identifiants
pubmed: 38849778
doi: 10.1186/s12903-024-04415-2
pii: 10.1186/s12903-024-04415-2
doi:
Substances chimiques
Carbodiimides
0
Resin Cements
0
Clearfil SE Bond
0
Dentin-Bonding Agents
0
Cross-Linking Reagents
0
Types de publication
Journal Article
Langues
eng
Sous-ensembles de citation
IM
Pagination
667Subventions
Organisme : National Natural Science Foundation of China
ID : 81801027
Informations de copyright
© 2024. The Author(s).
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