Development and Validation of Liquid Chromatographic Method for Fast Determination of Lincomycin, Polymyxin and Vancomycin in Preservation Solution for Transplants.

Lincomycin / analysis Vancomycin / analysis Polymyxins / analysis Chromatography, Liquid / methods Organ Preservation Solutions Anti-Bacterial Agents / analysis Reproducibility of Results Chromatography, High Pressure Liquid / methods
lincomycin liquid chromatography polymyxin superficially porous particles transplant preservation solution validation vancomycin

Journal

Molecules (Basel, Switzerland)
ISSN: 1420-3049
Titre abrégé: Molecules
Pays: Switzerland
ID NLM: 100964009

Informations de publication

Date de publication:
03 Jul 2024
Historique:
received: 27 05 2024
revised: 25 06 2024
accepted: 27 06 2024
medline: 13 7 2024
pubmed: 13 7 2024
entrez: 13 7 2024
Statut: epublish

Résumé

In this study, a liquid chromatographic method was developed for the fast determination of lincomycin, polymyxin and vancomycin in a preservation solution for transplants. A Kinetex EVO C18 (150 × 4.6 mm, 2.6 µm) column was utilized at 45 °C. Gradient elution was applied using a mixture of mobile phases A and B, both including 30 mM phosphate buffer at pH 2.0 and acetonitrile, at a ratio of 95:5 (

Identifiants

DOI: 10.3390/molecules29133166 PMID: 38999118
pubmed: 38999118
pii: molecules29133166
doi: 10.3390/molecules29133166
pii:
doi:

Substances chimiques

Lincomycin BOD072YW0F
Vancomycin 6Q205EH1VU
Polymyxins 0
Organ Preservation Solutions 0
Anti-Bacterial Agents 0

Types de publication

Journal Article Validation Study

Langues

eng

Sous-ensembles de citation

IM

Auteurs

Qi Lin (Q)

Department of Pharmaceutical and Pharmacological Sciences, Pharmaceutical Analysis, KU Leuven, Herestraat 49, O&N2, PB 923, 3000 Leuven, Belgium.

Tam Nguyen (T)

Department of Pharmaceutical and Pharmacological Sciences, Pharmaceutical Analysis, KU Leuven, Herestraat 49, O&N2, PB 923, 3000 Leuven, Belgium.

Chiara Staffieri (C)

Department of Pharmaceutical and Pharmacological Sciences, Pharmaceutical Analysis, KU Leuven, Herestraat 49, O&N2, PB 923, 3000 Leuven, Belgium.

Ann Van Schepdael (A)

Department of Pharmaceutical and Pharmacological Sciences, Pharmaceutical Analysis, KU Leuven, Herestraat 49, O&N2, PB 923, 3000 Leuven, Belgium.
ORCID: 0000-0002-9583-984X

Erwin Adams (E)

Department of Pharmaceutical and Pharmacological Sciences, Pharmaceutical Analysis, KU Leuven, Herestraat 49, O&N2, PB 923, 3000 Leuven, Belgium.
ORCID: 0000-0002-4545-2989

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Classifications MeSH

questionsmedicales.fr › Glucides › Hétérosides › Lincosamides › Lincomycine › Development and Validation of Liquid...
questionsmedicales.fr › Acides aminés, peptides et protéines › Peptides › Glycopeptides › Vancomycine › Development and Validation of Liquid...
questionsmedicales.fr › Acides aminés, peptides et protéines › Protéines › Protéines membranaires › Perforines › Peptides antimicrobiens cationiques › Polymyxines › Development and Validation of Liquid...
questionsmedicales.fr › Techniques d'investigation › Techniques de chimie analytique › Chromatographie › Chromatographie en phase liquide › Development and Validation of Liquid...
questionsmedicales.fr › Préparations pharmaceutiques › Solutions › Solution conservation organe › Development and Validation of Liquid...
questionsmedicales.fr › Actions chimiques et utilisations › Actions pharmacologiques › Utilisations thérapeutiques › Anti-infectieux › Antibactériens › Development and Validation of Liquid...
questionsmedicales.fr › Environnement et santé publique › Santé publique › Méthodes épidémiologiques › Méthodologie en recherche épidémiologique › Reproductibilité des résultats › Development and Validation of Liquid...
questionsmedicales.fr › Techniques d'investigation › Techniques de chimie analytique › Chromatographie › Chromatographie en phase liquide › Chromatographie en phase liquide à haute performance › Development and Validation of Liquid...