Cadmium recovery from acid leachates of Tunisian phosphoric acid purification residues.

Cadmium-rich sludges Chemical precipitation Hydrometallurgy Metal sulphides

Journal

Environmental science and pollution research international
ISSN: 1614-7499
Titre abrégé: Environ Sci Pollut Res Int
Pays: Germany
ID NLM: 9441769

Informations de publication

Date de publication:
10 Oct 2024
Historique:
received: 04 06 2024
accepted: 20 09 2024
medline: 13 10 2024
pubmed: 13 10 2024
entrez: 10 10 2024
Statut: aheadofprint

Résumé

The management of cadmium-rich sludges, which are pollutant residues from the phosphorus industry, including the valorization of these sludges through the selective recovery of heavy metals, is a promising prospect. However, there is still a need to develop recovery methods that are both optimized for efficiency, cost-effectiveness, and environmentally friendly. This study aims to enhance cadmium extraction from the polymetallic sludge by optimizing the processes of sulfuric acid (SA) leaching and sodium sulfide precipitation. Key parameters including SA concentration, temperature, solid/liquid ratio, and stirring velocity were optimized to maximize the heavy metals extraction. Over 90% of the Cd and Zn present in the sludge were successfully extracted. Subsequently, investigates the selective precipitation of metal sulfide from acidic leachates (pH < 2), focusing particularly on cadmium. Through the optimization of chemical precipitation parameters (Na

Identifiants

pubmed: 39388089
doi: 10.1007/s11356-024-35150-4
pii: 10.1007/s11356-024-35150-4
doi:

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Subventions

Organisme : Horizon 2020 Framework Programme (Twinning of research institutions)
ID : TUNTWIN GA: 952306

Informations de copyright

© 2024. The Author(s), under exclusive licence to Springer-Verlag GmbH Germany, part of Springer Nature.

Références

Akfas F, Elghali A, Bodinier JL, Parat F, Muñoz M (2023) Geochemical and mineralogical characterization of phosphogypsum and leaching tests for the prediction of the mobility of trace elements. Environ Sci Pollut Res 30(15):43778–43794. https://doi.org/10.1007/s11356-023-25357-2
doi: 10.1007/s11356-023-25357-2
Arunadevi R, Latha M, Velumani S, Oza G, Reyes-Figueroa P, Rohini M, Becerril-Juarez IG, Lee JH, Yi J (2015) Synthesis and characterization of cadmium sulfide nanoparticles by chemical precipitation method. J Nanosci Nanotechnol 15(11):8434–8439. https://doi.org/10.1166/jnn.2015.11472
doi: 10.1166/jnn.2015.11472
Awwad NS, El-Nadi YA, Hamed MM (2013) Successive processes for purification and extraction of phosphoric acid produced by wet process. Chem Eng Process 74:69–74. https://doi.org/10.1016/j.cep.2012.11.009
doi: 10.1016/j.cep.2012.11.009
Balkanski M, and J. Des Cloizeaux (1960) Structure de bandes des cristaux de type wurtzite. Transitions optiques intrinsèques dans le cds. Journal de Physique et Le Radium 21(12):825–34. https://doi.org/10.1051/jphysrad:019600021012082500
doi: 10.1051/jphysrad:019600021012082500
Bessiere J, Bruant M, Jdid EA, Blazy P (1986) Flottation ionique du cadmium et de l’arsenic par un dithiophosphate dans les solutions concentrées en acide phosphorique. Int J Miner Process 16(1–2):63–74. https://doi.org/10.1016/0301-7516(86)90075-X
doi: 10.1016/0301-7516(86)90075-X
Bilal E, Bellefqih H, Bourgier V, Mazouz H, Dumitraş DG, Bard F, Laborde M, Caspar JP, Guilhot B, Iatan EL, Bounakhla M, Iancu MA, Marincea Ş, Essakhraoui M, Li B, Diwa RR, Ramirez JD, Chernysh Y, Chubur V, … Haneklaus N (2023) Phosphogypsum circular economy considerations: a critical review from more than 65 storage sites worldwide. J Clean Prod 414(February). https://doi.org/10.1016/j.jclepro.2023.137561
Booker NA (1989) Removal of cadmium from wet phosphoric acid by cation exchange. Imperial College London
Box GEP, Draper NR (1987) Empirical model-building and response surfaces. In: Empirical model-building and response surfaces. John Wiley & Sons
Box GEP, Behnken DW (1960) Some new three level designs for the study of quantitative variables. Technometrics 2(4):455–475
doi: 10.1080/00401706.1960.10489912
Cao Y, Cui Y, Yu X, Li T, Chang IS, Wu J (2021) Bibliometric analysis of phosphogypsum research from 1990 to 2020 based on literatures and patents. Environ Sci Pollut Res 28(47):66845–66857. https://doi.org/10.1007/s11356-021-15237-y
doi: 10.1007/s11356-021-15237-y
Chatfield C (1995) Model uncertainty, data mining and statistical inference. J R Stat Soc Ser A: Stat Soc 158(3):419–466. https://doi.org/10.2307/2983440
doi: 10.2307/2983440
El Zrelli R, Rabaoui L, Daghbouj N, Abda H, Castet S, Josse C, van Beek P, Souhaut M, Michel S, Bejaoui N, Courjault-Radé P (2018) Characterization of phosphate rock and phosphogypsum from Gabes phosphate fertilizer factories (SE Tunisia): high mining potential and implications for environmental protection. Environ Sci Pollut Res 25(15):14690–14702. https://doi.org/10.1007/s11356-018-1648-4
doi: 10.1007/s11356-018-1648-4
Elyahyaoui A, Bouhlassa S (2001) Extraction of cadmium and iodocadmat species by di(2-ethylhexyl) phosphoric acid from perchloric and phosphoric media. Appl Radiat Isot 54(6):921–926. https://doi.org/10.1016/S0969-8043(00)00341-9
doi: 10.1016/S0969-8043(00)00341-9
Ennaassia E, El Kacemi K, Kossir A, Cote G (2002) Study of the removal of Cd(II) from phosphoric acid solutions by precipitation of CdS with Na2S. Hydrometallurgy 64(2):101–109. https://doi.org/10.1016/S0304-386X(02)00009-9
doi: 10.1016/S0304-386X(02)00009-9
Estay H, Barros L, Troncoso E (2021) Metal sulfide precipitation: recent breakthroughs and future outlooks. Minerals 11(12):1–27. https://doi.org/10.3390/min11121385
doi: 10.3390/min11121385
Fu F, Wang Q (2011) Removal of heavy metal ions from wastewaters: a review. J Environ Manag 92(3):407–418. https://doi.org/10.1016/j.jenvman.2010.11.011
doi: 10.1016/j.jenvman.2010.11.011
Gharabaghi M, Irannajad M, Azadmehr AR (2011) Physicochem Probl Miner Process 47:91–104
Habashi F, Awadalla FT (1986) The recovery of uranium during the purification of phosphoric acid by organic solvents. Sep Sci Technol 21(4):327–337. https://doi.org/10.1080/01496398608057165
doi: 10.1080/01496398608057165
Hamdi R, Hannachi A (2012) Comparative Simulation of the purification of wet phosphoric acid by Tbp, Mibk and a mixture (MIBK+TBP). J Chem Eng Process Technol 03(02). https://doi.org/10.4172/2157-7048.1000134
Hannachi A, Habaili D, Chtara C, Ratel A (2007) Purification of wet process phosphoric acid by solvent extraction with TBP and MIBK mixtures. Sep Purif Technol 55(2):212–216. https://doi.org/10.1016/j.seppur.2006.12.014
doi: 10.1016/j.seppur.2006.12.014
Hu S-H, Hu S-C, Fu Y-P (2011) Resource recovery of copper-contaminated sludge with jarosite process and selectiveprecipitation. Environmental Progress & Sustainable Energy 31(3):379–385. https://doi.org/10.1002/ep.10559
doi: 10.1002/ep.10559
Kabay N, Gizli N, Demircioğlu M, Yuksel M, Sağlam M, Arda M, Yuksel U, Saha B, Streat M (2003) Removal of cadmium from phosphoric acid solution by solvent-impregnated resins (sirs) - sorption kinetics and equilibria studies. Chem Eng Commun 190(5–8):936–947. https://doi.org/10.1080/00986440302116
doi: 10.1080/00986440302116
Kossir A, Cappelle P (2008) Method for processing cadmiferous solids, PCT/EP2007/052066, WO 2008/113403 A1
Kouzbour S, Gourich B, Gros F, Vial C, Allam F, Stiriba Y (2019) Comparative analysis of industrial processes for cadmium removal from phosphoric acid: a review. Hydrometallurgy 188(May):222–247. https://doi.org/10.1016/j.hydromet.2019.06.014
doi: 10.1016/j.hydromet.2019.06.014
Levasseur B, Blais JF, Mercier G (2005) Study of the metal precipitation from decontamination leachates of municipal wastes fly ash incinerators. Environ Technol 26(4):421–432. https://doi.org/10.1080/09593332608618547
doi: 10.1080/09593332608618547
Lewis AE (2010) Review of metal sulphide precipitation. Hydrometallurgy 104(2):222–234. https://doi.org/10.1016/j.hydromet.2010.06.010
doi: 10.1016/j.hydromet.2010.06.010
Nazari K, Ghadiri A, Babaie H (2005) Elimination of cadmium from wet process phosphoric acid with Alamine 336. Miner Eng 18(13–14):1233–1238. https://doi.org/10.1016/j.mineng.2005.07.008
doi: 10.1016/j.mineng.2005.07.008
Nogueira C, Margarido F (2004) Leaching behaviour of electrode materials of spent nickel–cadmium batteries in sulphuric acid media. Hydrometallurgy 72(1–2):111–118. https://doi.org/10.1016/S0304-386X(03)00123-3
doi: 10.1016/S0304-386X(03)00123-3
Pérez-López R, Nieto JM, Álvarez-Valero AM, Ruiz de Almondóvar G (2007) Mineralogy of the hardpan formation processes in the interface between sulfide-rich sludge and fly ash: applications for acid mine drainage mitigation. Am Mineral 92 (11–12): 1966–77. https://doi.org/10.2138/am.2007.2686
Peters RW, Ku Y, Bhattacharyya D (1985) Evaluation of recent treatment techniques for removal of heavy metals from industrial wastewaters. AIChE Symp Ser 81(243):165–203
Purkayastha D, Mishra U, Biswas S (2014) A comprehensive review on Cd(II) removal from aqueous solution. J Water Process Eng 2:105–128. https://doi.org/10.1016/j.jwpe.2014.05.009
doi: 10.1016/j.jwpe.2014.05.009
Safarzadeh MS, Ilkhchi MO (2007) A review on hydrometallurgical extraction and recovery of cadmium from various resources. 20:211–220. https://doi.org/10.1016/j.mineng.2006.07.001
Sahinkaya E, Gungor M, Bayrakdar A, Yucesoy Z, Uyanik S (2009) Separate Recovery of Copper and Zinc fromAcid Mine Drainage Using Biogenic Sulfide. J Hazard Mater 171(1–3):901–6. https://doi.org/10.1016/j.jhazmat.2009.06.089
doi: 10.1016/j.jhazmat.2009.06.089
Salem M, Souissi R, Souissi F, Abbes N, Moutte J (2019) Phosphoric acid purification sludge: potential in heavy metals and rare earth elements. Waste Manag 83:46–56. https://doi.org/10.1016/j.wasman.2018.10.040
doi: 10.1016/j.wasman.2018.10.040
Sanz J, Tomasa O, Jimenez-Franco A, Sidki-Rius N (2022) Elements and mineral resources. In Cadmium (Issue 8.5.2017). Springer International Publishing. https://doi.org/10.1007/978-3-030-85889-6
Sethurajan M, Huguenot D, Lens PNL, Horn HA, Figueiredo LHA, Van Hullebusch ED (2016) Leaching and selective copper recovery from acidic leachates of Tres Marias zinc plant (MG, Brazil) metallurgical purification residues. J Environ Manag 177:26–35. https://doi.org/10.1016/j.jenvman.2016.03.041
doi: 10.1016/j.jenvman.2016.03.041
Singh AK, Vijayashri KM, Singh SP, Mishra MK (2022) Synthesis and characterization of zinc doped cadmium sulphide nanoparticles. Mater Today: Proc 66:2017–2027. https://doi.org/10.1016/J.MATPR.2022.05.484
doi: 10.1016/J.MATPR.2022.05.484
Smida O, Souissi R, Salem M, Souissi F (2021) Geochemical assessment and mobility of undesired elements in the sludge of the phosphate industry of Gafsa-Metlaoui Basin, (Southern Tunisia). Appl Sci (Switzerland) 11(3):1–16. https://doi.org/10.3390/app11031075
doi: 10.3390/app11031075
Traill RJ, Boyle RW (1955) Hawleyite, isometric cadmium sulphide, a New Mineral. Am Miner 40(7–8):555–559
U.S. Geological Survey. (2022). Mineral commodity summaries 2022, CADMIUM, p 202 (42–43). https://doi.org/10.3133/mcs2022
Urtiaga AM, Alonso A, Ortiz I, Daoud JA, El-Reefy SA, Pérez De Ortiz S, Gallego T (2000) Comparison of liquid membrane processes for the removal of cadmium from wet phosphoric acid. J Membr Sci 164(1–2):229–240. https://doi.org/10.1016/S0376-7388(99)00197-0
doi: 10.1016/S0376-7388(99)00197-0
Zieliński J, Huculak-Mączka M, Kaniewski M, Nieweś D, Hoffmann K, Hoffmann J (2019) Kinetic modelling of cadmium removal from wet phosphoric acid by precipitation method. Hydrometallurgy 190(August):105157. https://doi.org/10.1016/j.hydromet.2019.105157
doi: 10.1016/j.hydromet.2019.105157

Auteurs

Marzougui Salem (M)

LMU Laboratory, National Institute for Research and Physico-chemical Analysis, Sidi Thabet Technopole, Tunis, Tunisia. mar_706@outlook.com.
Department of Geology, Faculty of Sciences of Tunis, El Manar University, Tunis, Tunisia. mar_706@outlook.com.

Radhia Souissi (R)

LMU Laboratory, National Institute for Research and Physico-chemical Analysis, Sidi Thabet Technopole, Tunis, Tunisia.

Kais Jebali (K)

Support Research and Technology Transfer Unit, Centre of Biotechnology of Borj-Cedria, Hammam-Lif, Tunisia.

Wassim Trabelsi (W)

Tunisian Chemical Group, Sfax, Tunisia.

Houyem Abderrazak (H)

LMU Laboratory, National Institute for Research and Physico-chemical Analysis, Sidi Thabet Technopole, Tunis, Tunisia.

Fouad Souissi (F)

LMU Laboratory, National Institute for Research and Physico-chemical Analysis, Sidi Thabet Technopole, Tunis, Tunisia.
Department of Geology, Faculty of Sciences of Tunis, El Manar University, Tunis, Tunisia.

Classifications MeSH