Aromatic Ring-Fused Amidine Based Allosteric Receptors Activated by Guest-Induced π-Conjugation Switching.

allosteric effect cooperativity hydrogen bond molecular recognition π-conjugation

Journal

ChemPlusChem
ISSN: 2192-6506
Titre abrégé: Chempluschem
Pays: Germany
ID NLM: 101580948

Informations de publication

Date de publication:
27 Oct 2024
Historique:
received: 18 09 2024
accepted: 24 10 2024
medline: 27 10 2024
pubmed: 27 10 2024
entrez: 27 10 2024
Statut: aheadofprint

Résumé

Amidine-substituted allosteric receptors 2a and 2b for benzenediols were synthesized. Receptor 2a with five-membered amidines exhibited greater allostericity than the amide-substituted receptor 1, while 2b with six-membered amidines exhibited less allostericity. NMR titration experiments revealed that a significant enthalpic factor was involved in the allostericity of these receptors. X-ray and DFT optimized structures of 2a and 2b revealed that 2a adopted a coplanar conformation with π-conjugation between the amidines and the phenylene ring of the hydrindacene framework, resulting in high allostericity due to inactivation of the initial binding.

Identifiants

pubmed: 39462205
doi: 10.1002/cplu.202400612
doi:

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

e202400612

Informations de copyright

© 2024 Wiley‐VCH GmbH.

Auteurs

Takayuki Kataoka (T)

Tokyo University of Science: Tokyo Rika Daigaku, Department of Chemistry, Faculty of Science, 1-3, Kagurazaka, 162-8601, Shinjuku-ku, JAPAN.

Kotaro Matsumura (K)

Tokyo University of Science: Tokyo Rika Daigaku, Department of Chemistry, Faculty of Science, 1-3, Kagurazaka, 162-8601, Shinjuku-ku, JAPAN.

Kosuke Ono (K)

Tokyo Institute of Technology: Tokyo Kogyo Daigaku, School of Science, 2-12-1 Ookayama, 152-8551, Meguro-ku, JAPAN.

Yoshitaka Tsuchido (Y)

Tokyo University of Science: Tokyo Rika Daigaku, Department of Chemistry, Faculty of Science, 1-3 Kagurazaka, 162-8601, Shinjuku-ku, JAPAN.

Hidetoshi Kawai (H)

Tokyo University of Science, Department of Chemistry, Faculty of Science, Kagurazaka, 1-3, 162-8601, Shinjuku-ku, JAPAN.

Classifications MeSH