Short- and long-term retrogradation of potato starches with varying amylose content.


Journal

Journal of the science of food and agriculture
ISSN: 1097-0010
Titre abrégé: J Sci Food Agric
Pays: England
ID NLM: 0376334

Informations de publication

Date de publication:
30 Mar 2019
Historique:
received: 16 05 2018
revised: 20 09 2018
accepted: 21 10 2018
pubmed: 26 10 2018
medline: 14 3 2019
entrez: 26 10 2018
Statut: ppublish

Résumé

Gels of potato starches with varying amylose content were prepared and the degree of pasting and the course of retrogradation were studied. The average molar masses of granular and pasted starches were estimated. Determination of the degree of pasting involved use of optical microscopy and the study of pasting characteristics. The studies of susceptibility to retrogradation considered mechanical spectra, hardness, syneresis, resistant starch content, and X-ray measurements. Heating of the starch suspensions at 95 °C resulted in almost complete deterioration of granules. Changes in storage modulus (G') exceeded these of loss modulus (G"). Values of G' and G", hardness and syneresis increased with the period of the sample storage and, simultaneously, the relevant tangent of the phase shift angle (tg (G"/G')) decreased. A tendency was observed for the resistant starch (RS) content to increase on prolonged storage of gels. The patterns of diffractograms for the pasted and lyophilized samples only differed slightly. The pastes of all the studied potato starches were characterized by a similar degree of pasting. The most essential changes in the physicochemical properties of the gels were observed between the 30th and 90th days of storage. The susceptibility of potato starch gels to retrogradation, especially within the first 2 h, was controlled, mainly by the amylose content. © 2018 Society of Chemical Industry.

Sections du résumé

BACKGROUND BACKGROUND
Gels of potato starches with varying amylose content were prepared and the degree of pasting and the course of retrogradation were studied. The average molar masses of granular and pasted starches were estimated. Determination of the degree of pasting involved use of optical microscopy and the study of pasting characteristics. The studies of susceptibility to retrogradation considered mechanical spectra, hardness, syneresis, resistant starch content, and X-ray measurements.
RESULTS RESULTS
Heating of the starch suspensions at 95 °C resulted in almost complete deterioration of granules. Changes in storage modulus (G') exceeded these of loss modulus (G"). Values of G' and G", hardness and syneresis increased with the period of the sample storage and, simultaneously, the relevant tangent of the phase shift angle (tg (G"/G')) decreased. A tendency was observed for the resistant starch (RS) content to increase on prolonged storage of gels. The patterns of diffractograms for the pasted and lyophilized samples only differed slightly.
CONCLUSION CONCLUSIONS
The pastes of all the studied potato starches were characterized by a similar degree of pasting. The most essential changes in the physicochemical properties of the gels were observed between the 30th and 90th days of storage. The susceptibility of potato starch gels to retrogradation, especially within the first 2 h, was controlled, mainly by the amylose content. © 2018 Society of Chemical Industry.

Identifiants

pubmed: 30357842
doi: 10.1002/jsfa.9446
doi:

Substances chimiques

Gels 0
Plant Extracts 0
Starch 9005-25-8
Amylose 9005-82-7

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

2393-2403

Informations de copyright

© 2018 Society of Chemical Industry.

Auteurs

Anna Dobosz (A)

Department of Carbohydrates Technology, Faculty of Food Technology, University of Agriculture in Krakow, Krakow, Poland.

Marek Sikora (M)

Department of Carbohydrates Technology, Faculty of Food Technology, University of Agriculture in Krakow, Krakow, Poland.

Magdalena Krystyjan (M)

Department of Carbohydrates Technology, Faculty of Food Technology, University of Agriculture in Krakow, Krakow, Poland.

Piotr Tomasik (P)

Nantes Nanotechnological Systems, Bolesławiec, Poland.

Radosław Lach (R)

Department of Ceramics and Refractories, Faculty of Materials Science and Ceramics, University of Science and Technology, Krakow, Poland.

Barbara Borczak (B)

Department of Human Nutrition, Faculty of Food Technology, University of Agriculture in Krakow, Krakow, Poland.

Wiktor Berski (W)

Department of Carbohydrates Technology, Faculty of Food Technology, University of Agriculture in Krakow, Krakow, Poland.

Marcin Lukasiewicz (M)

Department of Carbohydrates Technology, Faculty of Food Technology, University of Agriculture in Krakow, Krakow, Poland.

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Classifications MeSH