L-Asparaginase from Erwinia carotovora: insights about its stability and activity.


Journal

Molecular biology reports
ISSN: 1573-4978
Titre abrégé: Mol Biol Rep
Pays: Netherlands
ID NLM: 0403234

Informations de publication

Date de publication:
Feb 2019
Historique:
received: 09 08 2018
accepted: 30 10 2018
pubmed: 18 11 2018
medline: 11 7 2019
entrez: 18 11 2018
Statut: ppublish

Résumé

Enzymatic prospection indicated that L-asparaginase from Erwinia carotovora (ECAR-LANS) posses low glutaminase activity and much effort has been made to produce therapeutic ECAR-LANS. However, its low stability precludes its use in therapy. Herein, biochemical and biophysical assays provided data highlighting the influence of solubilization and storage into ECAR-LANS structure, stability, and activity. Moreover, innovations in recombinant expression and purification guaranteed the purification of functional tetramers. According to solubilization condition, the L-asparaginase activity and temperature of melting ranged up to 25-32%, respectively. CD spectra indicate the tendency of ECAR-LANS to instability and the influence of β-structures in activity. These results provide relevant information to guide formulations with prolonged action in the bloodstream.

Identifiants

pubmed: 30446961
doi: 10.1007/s11033-018-4459-2
pii: 10.1007/s11033-018-4459-2
doi:

Substances chimiques

Asparaginase EC 3.5.1.1

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

1313-1316

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Auteurs

Marcele Faret (M)

Instituto Carlos Chagas, ICC - FIOCRUZ/PR, Rua Algacyr Munhoz Mader, 3775, bloco C, Curitiba,, Paraná, 81350-010, Brazil.

Stephanie Bath de Morais (SB)

Instituto Carlos Chagas, ICC - FIOCRUZ/PR, Rua Algacyr Munhoz Mader, 3775, bloco C, Curitiba,, Paraná, 81350-010, Brazil.

Nilson Ivo Tonin Zanchin (NIT)

Instituto Carlos Chagas, ICC - FIOCRUZ/PR, Rua Algacyr Munhoz Mader, 3775, bloco C, Curitiba,, Paraná, 81350-010, Brazil.

Tatiana de Arruda Campos Brasil de Souza (TACB)

Instituto Carlos Chagas, ICC - FIOCRUZ/PR, Rua Algacyr Munhoz Mader, 3775, bloco C, Curitiba,, Paraná, 81350-010, Brazil. tatianabrasil@fiocruz.br.

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