Stir bar sorptive-dispersive microextraction for trace determination of triphenyl and diphenyl phosphate in urine of nail polish users.

Biphenyl Compounds / isolation & purification Chromatography, Liquid Cosmetics Humans Limit of Detection Linear Models Liquid Phase Microextraction / methods Organophosphates / isolation & purification Reproducibility of Results Tandem Mass Spectrometry
Cosmetics Endocrine disruptors Magnetic composite Nail polish Stir bar sorptive-dispersive microextraction Urine samples

Journal

Journal of chromatography. A
ISSN: 1873-3778
Titre abrégé: J Chromatogr A
Pays: Netherlands
ID NLM: 9318488

Informations de publication

Date de publication:
24 May 2019
Historique:
received: 31 10 2018
revised: 18 01 2019
accepted: 06 02 2019
pubmed: 18 2 2019
medline: 4 6 2019
entrez: 18 2 2019
Statut: ppublish

Résumé

This work describes a new analytical method useful for monitoring the human exposure to the endocrine-disrupting plasticizer triphenyl phosphate (TPP) via nail polish use. The method allows trace determination of this parent compound and its main metabolite, namely diphenyl phosphate (DPP), in urine samples of nail polish users. The method is based on a novel microextraction technique termed stir bar sorptive-dispersive microextraction (SBSDME) using a magnetic composite made of CoFe

Identifiants

DOI: 10.1016/j.chroma.2019.02.014 PMID: 30772058
pubmed: 30772058
pii: S0021-9673(19)30144-X
doi: 10.1016/j.chroma.2019.02.014
pii:
doi:

Substances chimiques

Biphenyl Compounds 0
Cosmetics 0
Organophosphates 0
diphenyl 2L9GJK6MGN
triphenyl phosphate YZE19Z66EA

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

9-16

Informations de copyright

Copyright © 2019 Elsevier B.V. All rights reserved.

Auteurs

José Grau (J)

Department of Analytical Chemistry, University of Valencia, 46100, Burjassot, Valencia, Spain.

Juan L Benedé (JL)

Department of Analytical Chemistry, University of Valencia, 46100, Burjassot, Valencia, Spain.

Javier Serrano (J)

Department of Analytical Chemistry, University of Valencia, 46100, Burjassot, Valencia, Spain.

Andrea Segura (A)

Department of Analytical Chemistry, University of Valencia, 46100, Burjassot, Valencia, Spain.

Alberto Chisvert (A)

Department of Analytical Chemistry, University of Valencia, 46100, Burjassot, Valencia, Spain. Electronic address: alberto.chisvert@uv.es.

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Classifications MeSH

questionsmedicales.fr › Composés chimiques organiques › Hydrocarbures › Hydrocarbures cycliques › Hydrocarbures aromatiques › Dérivés du benzène › Dérivés du biphényle › Stir bar sorptive-dispersive microextraction...
questionsmedicales.fr › Techniques d'investigation › Techniques de chimie analytique › Chromatographie › Chromatographie en phase liquide › Stir bar sorptive-dispersive microextraction...
questionsmedicales.fr › Technologie, industrie et agriculture › Produits domestiques › Cosmétiques › Stir bar sorptive-dispersive microextraction...
questionsmedicales.fr › Eucaryotes › Animaux › Chordés › Vertébrés › Mammifères › Eutheria › Primates › Haplorhini › Catarrhini › Hominidae › Humains › Stir bar sorptive-dispersive microextraction...
questionsmedicales.fr › Environnement et santé publique › Santé publique › Méthodes épidémiologiques › Statistiques comme sujet › Sensibilité et spécificité › Limite de détection › Stir bar sorptive-dispersive microextraction...
questionsmedicales.fr › Environnement et santé publique › Santé publique › Méthodes épidémiologiques › Statistiques comme sujet › Analyse de régression › Modèles linéaires › Stir bar sorptive-dispersive microextraction...
questionsmedicales.fr › Techniques d'investigation › Techniques de chimie analytique › Fractionnement chimique › Extraction liquide-liquide › Microextraction en phase liquide › Stir bar sorptive-dispersive microextraction...
questionsmedicales.fr › Composés chimiques organiques › Composés organiques du phosphore › Organophosphates › Stir bar sorptive-dispersive microextraction...
questionsmedicales.fr › Environnement et santé publique › Santé publique › Méthodes épidémiologiques › Méthodologie en recherche épidémiologique › Reproductibilité des résultats › Stir bar sorptive-dispersive microextraction...
questionsmedicales.fr › Techniques d'investigation › Techniques de chimie analytique › Spectrométrie de masse › Spectrométrie de masse en tandem › Stir bar sorptive-dispersive microextraction...