Structure-activity relationship studies of Bz amide-containing α-GalCer derivatives as natural killer T cell modulators.


Journal

Bioorganic & medicinal chemistry letters
ISSN: 1464-3405
Titre abrégé: Bioorg Med Chem Lett
Pays: England
ID NLM: 9107377

Informations de publication

Date de publication:
15 04 2019
Historique:
received: 26 12 2018
revised: 18 02 2019
accepted: 18 02 2019
pubmed: 3 3 2019
medline: 11 3 2020
entrez: 3 3 2019
Statut: ppublish

Résumé

CD1d is a non-polymorphic antigen-presenting glycoprotein that recognizes glycolipids as ligands. Ligands bind to the hydrophobic grooves of CD1d, and the resulting ligand-CD1d complexes activate natural killer T (NKT) cells by means of T cell receptor recognition, leading to the secretion of various cytokines. However, details of the ligand recognition mechanism of a large hydrophobic ligand binding pocket and the relationship between cytokine induction and ligand structure are unclear. We report the synthesis of α-GalCer derivatives containing a Bz amide group having various substituting groups in the ceramide moiety, and the analysis of the structure-activity relationships. The assays reveal that the Bz amide-containing CD1d ligands function as NKT cell modulators displaying Th2 cytokine biasing responses. Furthermore, molecular dynamics simulation studies suggest that the phenyl groups can interact with the aromatic amino acid residues in the lipid binding pocket of CD1d.

Identifiants

pubmed: 30824201
pii: S0960-894X(19)30102-7
doi: 10.1016/j.bmcl.2019.02.018
pii:
doi:

Substances chimiques

Amides 0
Antigens, CD1d 0
Cytokines 0
Galactosylceramides 0
Ligands 0
alpha-galactosylceramide 0
Benzene J64922108F

Types de publication

Journal Article Research Support, Non-U.S. Gov't

Langues

eng

Sous-ensembles de citation

IM

Pagination

970-973

Informations de copyright

Copyright © 2019 Elsevier Ltd. All rights reserved.

Auteurs

Junichiro Kishi (J)

Faculty of Science and Technology, Keio University, 3-14-1 Hiyoshi, Yokohama, Kanagawa 223-8522, Japan.

Shinsuke Inuki (S)

Faculty of Science and Technology, Keio University, 3-14-1 Hiyoshi, Yokohama, Kanagawa 223-8522, Japan; Graduate School of Pharmaceutical Sciences, Kyoto University, 46-29 Yoshida-Shimo-Adachi-cho, Sakyo-ku, Kyoto 606-8501, Japan.

Natsumi Hirata (N)

Faculty of Science and Technology, Keio University, 3-14-1 Hiyoshi, Yokohama, Kanagawa 223-8522, Japan.

Emi Kashiwabara (E)

Faculty of Science and Technology, Keio University, 3-14-1 Hiyoshi, Yokohama, Kanagawa 223-8522, Japan.

Daisuke Yoshidome (D)

Schrödinger K. K., 1-8-1 Marunouchi Chiyoda-ku, Tokyo 100-0005, Japan.

Osamu Ichihara (O)

Schrödinger K. K., 1-8-1 Marunouchi Chiyoda-ku, Tokyo 100-0005, Japan.

Yukari Fujimoto (Y)

Faculty of Science and Technology, Keio University, 3-14-1 Hiyoshi, Yokohama, Kanagawa 223-8522, Japan. Electronic address: fujimotoy@chem.keio.ac.jp.

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Classifications MeSH