Dilution and microfiltration of particulate corticosteroids for spinal epidural injections: impact on drug concentration and agglomerate formation.


Journal

Anaesthesia
ISSN: 1365-2044
Titre abrégé: Anaesthesia
Pays: England
ID NLM: 0370524

Informations de publication

Date de publication:
12 2019
Historique:
accepted: 15 05 2019
pubmed: 23 6 2019
medline: 12 11 2019
entrez: 23 6 2019
Statut: ppublish

Résumé

Particulate corticosteroids have been described to lead to greater pain improvement compared with their non-particulate counterparts when used in epidural injections. It is hypothesised that filtering may significantly impact their concentration and long-term efficacy. We investigated if passing particulate suspensions through different commonly-used filters affects drug dosage. Two particulate corticosteroid formulations, triamcinolone acetonide and methylprednisolone acetate, were mixed at different concentrations with either bupivacaine hydrochloride or 0.9% sodium chloride. Solutions were passed through a 5-μm and a 0.2-μm filter. Mass spectroscopy results indicated a complete loss of corticosteroid from the solutions using both filters, and light microscopy imaging demonstrated agglomerate formation, suggesting that filtering interferes with drug dosage. The choice of diluents must also be considered to reduce large agglomerate formation. Clinicians should be aware of the consequences of filtering particulate suspensions and carefully consider the selection of diluent when considering treatment plans.

Identifiants

pubmed: 31228255
doi: 10.1111/anae.14733
doi:

Substances chimiques

Adrenal Cortex Hormones 0
Particulate Matter 0
Suspensions 0
Triamcinolone Acetonide F446C597KA
Methylprednisolone X4W7ZR7023

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

1551-1557

Commentaires et corrections

Type : CommentIn

Informations de copyright

© 2019 Association of Anaesthetists.

Références

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Auteurs

A Alcántara Guardado (A)

School of Mechanical, Aerospace & Civil Engineering, University of Manchester, UK.

G Cooper (G)

School of Mechanical, Aerospace & Civil Engineering, University of Manchester, UK.

A Weightman (A)

School of Mechanical, Aerospace & Civil Engineering, University of Manchester, UK.

R Spiess (R)

Experimental Officer, Manchester Institute of Biotechnology, University of Manchester, UK.

A D L Baker (ADL)

Royal Preston Hospital, Preston, UK.

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