Development and validation of an ultra high performance liquid chromatography-tandem mass spectrometry method for the determination of phthalate esters in Greek grape marc spirits.

Alcoholic Beverages / analysis Chromatography, High Pressure Liquid / methods Distillation Esters / analysis Fermentation Greece Humans Limit of Detection Molecular Weight Phthalic Acids / analysis Reference Standards Reproducibility of Results Solutions Sugars / analysis Tandem Mass Spectrometry / methods Temperature Time Factors Vitis / chemistry
Grape marc spirits Phthalate esters Tandem mass spectrometry Ultra high performance liquid chromatography

Journal

Journal of chromatography. A
ISSN: 1873-3778
Titre abrégé: J Chromatogr A
Pays: Netherlands
ID NLM: 9318488

Informations de publication

Date de publication:
11 Oct 2019
Historique:
received: 14 03 2019
revised: 29 05 2019
accepted: 12 06 2019
pubmed: 27 6 2019
medline: 30 10 2019
entrez: 27 6 2019
Statut: ppublish

Résumé

An Ultra High Performance Liquid Chromatography - Tandem Mass Spectrometry method has been developed for the analysis of 12 phthalate esters in Greek grape marc spirits. The phthalates were separated on a U-VDSpher PUR 100 C18-E (100 mm x 2.0 mm, 1.8 μm) column by gradient elution. The analytes were ionized by positive electrospray ionization using the multiple reaction monitoring mode. The standard addition method was used for quantification and the Student's t-test was carried out to evaluate the matrix effect. The accuracy of the method was assessed by recovery experiments resulting in values from 81.6 to 109.6%. The detection limits ranged from 0.3 to 33.3 μg L

Identifiants

DOI: 10.1016/j.chroma.2019.06.034 PMID: 31239151
pubmed: 31239151
pii: S0021-9673(19)30643-0
doi: 10.1016/j.chroma.2019.06.034
pii:
doi:

Substances chimiques

Esters 0
Phthalic Acids 0
Solutions 0
Sugars 0
phthalic acid 6O7F7IX66E

Types de publication

Journal Article Validation Study

Langues

eng

Sous-ensembles de citation

IM

Pagination

165-178

Commentaires et corrections

Type : ErratumIn

Informations de copyright

Copyright © 2019 Elsevier B.V. All rights reserved.

Auteurs

Dimitra Diamantidou (D)

Laboratory of Analytical Chemistry, Department of Chemistry, Aristotle University of Thessaloniki, 54124, Thessaloniki, Greece; BIOMIC Auth, Center for Interdisciplinary Research and Innovation (CIRI-AUTH), Balkan Center, Buldings A&B, Thessaloniki, 10thkm Thessaloniki-Thermi Rd, P.O. Box 8318, GR, 57001, Greece; FoodOmicsGR, Center for Interdisciplinary Research & Innovation, Aristotle University of Thessaloniki, 57001, Thessaloniki, Greece.

Olga Begou (O)

Laboratory of Analytical Chemistry, Department of Chemistry, Aristotle University of Thessaloniki, 54124, Thessaloniki, Greece; BIOMIC Auth, Center for Interdisciplinary Research and Innovation (CIRI-AUTH), Balkan Center, Buldings A&B, Thessaloniki, 10thkm Thessaloniki-Thermi Rd, P.O. Box 8318, GR, 57001, Greece; FoodOmicsGR, Center for Interdisciplinary Research & Innovation, Aristotle University of Thessaloniki, 57001, Thessaloniki, Greece.

Georgios Theodoridis (G)

Laboratory of Analytical Chemistry, Department of Chemistry, Aristotle University of Thessaloniki, 54124, Thessaloniki, Greece; BIOMIC Auth, Center for Interdisciplinary Research and Innovation (CIRI-AUTH), Balkan Center, Buldings A&B, Thessaloniki, 10thkm Thessaloniki-Thermi Rd, P.O. Box 8318, GR, 57001, Greece; FoodOmicsGR, Center for Interdisciplinary Research & Innovation, Aristotle University of Thessaloniki, 57001, Thessaloniki, Greece.

Helen Gika (H)

BIOMIC Auth, Center for Interdisciplinary Research and Innovation (CIRI-AUTH), Balkan Center, Buldings A&B, Thessaloniki, 10thkm Thessaloniki-Thermi Rd, P.O. Box 8318, GR, 57001, Greece; FoodOmicsGR, Center for Interdisciplinary Research & Innovation, Aristotle University of Thessaloniki, 57001, Thessaloniki, Greece; Laboratory of Forensic Medicine and Toxicology, School of Medicine, Aristotle University of Thessaloniki, 54124, Thessaloniki, Greece.

Emmanouil Tsochatzis (E)

Department of Chemical Engineering, Aristotle University of Thessaloniki, 54124, Thessaloniki, Greece.

Stavros Kalogiannis (S)

FoodOmicsGR, Center for Interdisciplinary Research & Innovation, Aristotle University of Thessaloniki, 57001, Thessaloniki, Greece; Department of Nutrition and Dietetics, Alexander Technological Educational Institute of Thessaloniki, 57400, Thessaloniki, Greece.

Natalia Kataiftsi (N)

Laboratory of Oenology and Alcoholic Beverages, Department of Food Science and Technology, School of Agriculture, Aristotle University of Thessaloniki, 54124, Thessaloniki, Greece.

Evangelos Soufleros (E)

Laboratory of Oenology and Alcoholic Beverages, Department of Food Science and Technology, School of Agriculture, Aristotle University of Thessaloniki, 54124, Thessaloniki, Greece.

Anastasia Zotou (A)

Laboratory of Analytical Chemistry, Department of Chemistry, Aristotle University of Thessaloniki, 54124, Thessaloniki, Greece; FoodOmicsGR, Center for Interdisciplinary Research & Innovation, Aristotle University of Thessaloniki, 57001, Thessaloniki, Greece. Electronic address: azotou@chem.auth.gr.

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Classifications MeSH

questionsmedicales.fr › Aliments et boissons › Boissons › Boissons alcooliques › Development and validation of an ultra high...
questionsmedicales.fr › Techniques d'investigation › Techniques de chimie analytique › Chromatographie › Chromatographie en phase liquide › Chromatographie en phase liquide à haute performance › Development and validation of an ultra high...
questionsmedicales.fr › Techniques d'investigation › Techniques de chimie analytique › Fractionnement chimique › Distillation › Development and validation of an ultra high...
questionsmedicales.fr › Composés chimiques organiques › Acides carboxyliques › Esters › Development and validation of an ultra high...
questionsmedicales.fr › Métabolisme › Métabolisme glucidique › Fermentation › Development and validation of an ultra high...
questionsmedicales.fr › Régions géographiques › Europe › Grèce › Development and validation of an ultra high...
questionsmedicales.fr › Eucaryotes › Animaux › Chordés › Vertébrés › Mammifères › Eutheria › Primates › Haplorhini › Catarrhini › Hominidae › Humains › Development and validation of an ultra high...
questionsmedicales.fr › Environnement et santé publique › Santé publique › Méthodes épidémiologiques › Statistiques comme sujet › Sensibilité et spécificité › Limite de détection › Development and validation of an ultra high...
questionsmedicales.fr › Phénomènes chimiques › Masse moléculaire › Development and validation of an ultra high...
questionsmedicales.fr › Composés chimiques organiques › Acides carboxyliques › Acides carbocycliques › Acides phtaliques › Development and validation of an ultra high...
questionsmedicales.fr › Techniques d'investigation › Poids et mesures › Normes de référence › Development and validation of an ultra high...
questionsmedicales.fr › Environnement et santé publique › Santé publique › Méthodes épidémiologiques › Méthodologie en recherche épidémiologique › Reproductibilité des résultats › Development and validation of an ultra high...
questionsmedicales.fr › Préparations pharmaceutiques › Solutions › Development and validation of an ultra high...
questionsmedicales.fr › Glucides › Sucres › Development and validation of an ultra high...
questionsmedicales.fr › Techniques d'investigation › Techniques de chimie analytique › Spectrométrie de masse › Spectrométrie de masse en tandem › Development and validation of an ultra high...
questionsmedicales.fr › Environnement et santé publique › Environnement › Concepts météorologiques › Atmosphère › Temps (météorologie) › Température › Development and validation of an ultra high...
questionsmedicales.fr › Phénomènes physiques › Temps › Facteurs temps › Development and validation of an ultra high...
questionsmedicales.fr › Eucaryotes › Viridiplantae › Streptophyta › Embryophyta › Tracheobionta › Magnoliopsida › Vitaceae › Vitis › Development and validation of an ultra high...