Determination of multiclass personal care products in continental waters by solid-phase microextraction followed by gas chromatography-tandem mass spectrometry.

Cosmetics / analysis Gas Chromatography-Mass Spectrometry / methods Limit of Detection Solid Phase Microextraction / methods Tandem Mass Spectrometry / methods Water Pollutants, Chemical / analysis
GC–MS/MS Personal care products Solid-phase microextraction Water monitoring

Journal

Journal of chromatography. A
ISSN: 1873-3778
Titre abrégé: J Chromatogr A
Pays: Netherlands
ID NLM: 9318488

Informations de publication

Date de publication:
06 Dec 2019
Historique:
received: 15 04 2019
revised: 22 07 2019
accepted: 23 07 2019
pubmed: 4 8 2019
medline: 11 1 2020
entrez: 4 8 2019
Statut: ppublish

Résumé

A methodology based on solid-phase microextraction (SPME) followed by gas chromatography-tandem mass spectrometry (GC-MS/MS) was developed for the simultaneous analysis of different families of personal care products (PCPs) including fragrance allergens, synthetic musks, phthalates, antioxidants and UV filters in continental waters. The main parameters affecting SPME procedure were optimized by an ANOVA study. The final selected conditions comprised the use of 10 mL of sample with 20% (w/v) of sodium chloride (NaCl), polydimtehylsiloxane/divinylbenzene (PDMS/DVB) fiber and 20 min of extraction time at 100 °C in the head-space mode. Good linearity (R

Identifiants

DOI: 10.1016/j.chroma.2019.460398 PMID: 31375329
pubmed: 31375329
pii: S0021-9673(19)30782-4
doi: 10.1016/j.chroma.2019.460398
pii:
doi:

Substances chimiques

Cosmetics 0
Water Pollutants, Chemical 0

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

460398

Informations de copyright

Copyright © 2019 Elsevier B.V. All rights reserved.

Auteurs

Maria Celeiro (M)

Laboratory of Research and Development of Analytical Solutions (LIDSA), Department of Analytical Chemistry, Nutrition and Food Science, Faculty of Chemistry, University of Santiago de Compostela, E-15782, Santiago de Compostela, Spain.

J Pablo Lamas (JP)

Laboratory of Research and Development of Analytical Solutions (LIDSA), Department of Analytical Chemistry, Nutrition and Food Science, Faculty of Chemistry, University of Santiago de Compostela, E-15782, Santiago de Compostela, Spain.

Marlene Vila (M)

Laboratory of Research and Development of Analytical Solutions (LIDSA), Department of Analytical Chemistry, Nutrition and Food Science, Faculty of Chemistry, University of Santiago de Compostela, E-15782, Santiago de Compostela, Spain.

Carmen Garcia-Jares (C)

Laboratory of Research and Development of Analytical Solutions (LIDSA), Department of Analytical Chemistry, Nutrition and Food Science, Faculty of Chemistry, University of Santiago de Compostela, E-15782, Santiago de Compostela, Spain.

Vera Homem (V)

Laboratory for Process Engineering, Environment, Biotechnology and Energy (LEPABE), Faculty of Engineering, University of Porto, 4200-465, Porto, Portugal.

Nuno Ratola (N)

Laboratory for Process Engineering, Environment, Biotechnology and Energy (LEPABE), Faculty of Engineering, University of Porto, 4200-465, Porto, Portugal.

Thierry Dagnac (T)

Agronomic and Agrarian Research Centre (AGACAL-CIAM). Unit of Organic Contaminants, Apartado 10, 15080, A Coruña, Spain.

Maria Llompart (M)

Laboratory of Research and Development of Analytical Solutions (LIDSA), Department of Analytical Chemistry, Nutrition and Food Science, Faculty of Chemistry, University of Santiago de Compostela, E-15782, Santiago de Compostela, Spain. Electronic address: maria.llompart@usc.es.

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Classifications MeSH

questionsmedicales.fr › Technologie, industrie et agriculture › Produits domestiques › Cosmétiques › Determination of multiclass personal care...
questionsmedicales.fr › Techniques d'investigation › Techniques de chimie analytique › Spectrométrie de masse › Chromatographie gazeuse-spectrométrie de masse › Determination of multiclass personal care...
questionsmedicales.fr › Environnement et santé publique › Santé publique › Méthodes épidémiologiques › Statistiques comme sujet › Sensibilité et spécificité › Limite de détection › Determination of multiclass personal care...
questionsmedicales.fr › Techniques d'investigation › Techniques de chimie analytique › Fractionnement chimique › Extraction en phase solide › Microextraction en phase solide › Determination of multiclass personal care...
questionsmedicales.fr › Techniques d'investigation › Techniques de chimie analytique › Spectrométrie de masse › Spectrométrie de masse en tandem › Determination of multiclass personal care...
questionsmedicales.fr › Actions chimiques et utilisations › Actions toxiques › Polluants environnementaux › Polluants de l'eau › Polluants chimiques de l'eau › Determination of multiclass personal care...