Analysis of Procollagen C-Proteinase Enhancer-1/Glycosaminoglycan Binding Sites and of the Potential Role of Calcium Ions in the Interaction.


Journal

International journal of molecular sciences
ISSN: 1422-0067
Titre abrégé: Int J Mol Sci
Pays: Switzerland
ID NLM: 101092791

Informations de publication

Date de publication:
10 Oct 2019
Historique:
received: 13 09 2019
revised: 07 10 2019
accepted: 09 10 2019
entrez: 30 10 2019
pubmed: 30 10 2019
medline: 1 4 2020
Statut: epublish

Résumé

In this study, we characterize the interactions between the extracellular matrix protein, procollagen C-proteinase enhancer-1 (PCPE-1), and glycosaminoglycans (GAGs), which are linear anionic periodic polysaccharides. We applied molecular modeling approaches to build a structural model of full-length PCPE-1, which is not experimentally available, to predict GAG binding poses for various GAG lengths, types and sulfation patterns, and to determine the effect of calcium ions on the binding. The computational data are analyzed and discussed in the context of the experimental results previously obtained using surface plasmon resonance binding assays. We also provide experimental data on PCPE-1/GAG interactions obtained using inhibition assays with GAG oligosaccharides ranging from disaccharides to octadecasaccharides. Our results predict the localization of GAG-binding sites at the amino acid residue level onto PCPE-1 and is the first attempt to describe the effects of ions on protein-GAG binding using modeling approaches. In addition, this study allows us to get deeper insights into the in silico methodology challenges and limitations when applied to GAG-protein interactions.

Identifiants

pubmed: 31658765
pii: ijms20205021
doi: 10.3390/ijms20205021
pmc: PMC6829435
pii:
doi:

Substances chimiques

Extracellular Matrix Proteins 0
Glycosaminoglycans 0
Ions 0
PCOLCE protein, human 0
Calcium SY7Q814VUP

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Subventions

Organisme : Narodowe Centrum Nauki
ID : UMO-2018/30/E/ST4/00037
Organisme : Narodowe Centrum Nauki
ID : UMO-2017/25/B/ST4/01026

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Auteurs

Jan Potthoff (J)

Faculty of Chemistry, University of Gdańsk, ul. Wita Stwosza 63, 80-308 Gdańsk, Poland. potthoff.jan@googlemail.com.
Institute of Chemistry and Biochemistry, Free University of Berlin, Takustr. 3, 14195 Berlin, Germany. potthoff.jan@googlemail.com.

Krzysztof K Bojarski (KK)

Faculty of Chemistry, University of Gdańsk, ul. Wita Stwosza 63, 80-308 Gdańsk, Poland. krzysztof.bojarski@ug.edu.pl.

Gergely Kohut (G)

Institute of Materials and Environmental Chemistry, Research Centre for Natural Sciences, Hungarian Academy of Sciences, Magyar tudósok körútja 2, 1117 Budapest, Hungary. kohut.gergely@ttk.mta.hu.
MTA-ELTE Research Group of Peptide Chemistry, Hungarian Academy of Sciences, Eötvös Loránd University, Budapest 112, P.O. Box 32, 1518 Budapest, Hungary. kohut.gergely@ttk.mta.hu.

Agnieszka G Lipska (AG)

Faculty of Chemistry, University of Gdańsk, ul. Wita Stwosza 63, 80-308 Gdańsk, Poland. lypstyk@gmail.com.

Adam Liwo (A)

Faculty of Chemistry, University of Gdańsk, ul. Wita Stwosza 63, 80-308 Gdańsk, Poland. adam.liwo@ug.edu.pl.

Efrat Kessler (E)

Maurice and Gabriela Goldschleger Eye Research Institute, Tel-Aviv University Sackler Faculty of Medicine, Sheba Medical Center, Tel-Hashomer, 52621 Ramat Gan, Israel. ekessler@post.tau.ac.il.

Sylvie Ricard-Blum (S)

Institute of Molecular and Supramolecular Chemistry and Biochemistry, UMR 5246, CNRS, INSA Lyon, CPE, University Claude Bernard Lyon 1, Univ Lyon, 69622 Villeurbanne CEDEX, France. sylvie.ricard-blum@univ-lyon1.fr.

Sergey A Samsonov (SA)

Faculty of Chemistry, University of Gdańsk, ul. Wita Stwosza 63, 80-308 Gdańsk, Poland. sergey.samsonov@ug.edu.pl.

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Classifications MeSH