Insight into Protein-Polymer Conjugate Relaxation Dynamics: The Importance of Polymer Grafting.

dynamical transition hydration water neutron scattering properties of protein-polymer conjugates protein dynamics

Journal

Macromolecular bioscience
ISSN: 1616-5195
Titre abrégé: Macromol Biosci
Pays: Germany
ID NLM: 101135941

Informations de publication

Date de publication:
06 2020
Historique:
received: 29 11 2019
revised: 27 03 2020
pubmed: 15 4 2020
medline: 3 6 2021
entrez: 15 4 2020
Statut: ppublish

Résumé

The bio and chemical physics of protein-polymer conjugates are related to parameters that characterize each component. With this work, it is intended to feature the dynamical properties of the protein-polymer conjugate myoglobin (Mb)-poly(ethyl ethylene phosphate), in the ps and ns time scales, in order to understand the respective roles of the protein and of the polymer size in the dynamics of the conjugate. Elastic and quasi-elastic neutron scattering is performed on completely hydrogenated samples with variable number of polymer chains covalently attached to the protein. The role of the polymer length in the protein solvation and internal dynamics is investigated using two conjugates formed by polymers of different molecular weight. It is confirmed that the flexibility of the complex increases with the number of grafted polymer chains and that a sharp dynamical transition appears when either grafting density or polymer molecular weight are high. It is shown that protein size is crucial for the polymer structural organization and interaction on the protein surface and it is established that the glass properties of the polymer change upon conjugation. The results give a better insight of the equivalence of the polymer coating and the role of water on the surface of proteins.

Identifiants

pubmed: 32285628
doi: 10.1002/mabi.201900410
doi:

Substances chimiques

Myoglobin 0
Polyesters 0

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

e1900410

Informations de copyright

© 2020 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

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Auteurs

Daniela Russo (D)

Consiglio Nazionale delle Ricerche & Istituto Officina dei Materiali c/o Institut Laue Langevin, Grenoble, 38042, France.
Australian Nuclear Science and Technology Organisation, New Illawarra Road, Lucas Heights, NSW, 2234, Australia.

Chiara Pelosi (C)

Dipartimento di Chimica e Chimica Industriale, Università di Pisa, Via Moruzzi, Pisa, 56124, Italy.

Frederik R Wurm (FR)

Max-Planck-Institut für Polymerforschung, Ackermannweg 10, Mainz, 55128, Germany.

Bernhard Frick (B)

Institut Laue Langevin, Grenoble, 38042, France.

Jacques Ollivier (J)

Institut Laue Langevin, Grenoble, 38042, France.

Jose Teixeira (J)

Laboratoire Léon Brillouin (CEA/CNRS), CEA Saclay, Gif-sur-Yvette Cedex, 91191, France.

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