[Pesticide Analysis in Agricultural Products by GC-MS/MS Using STQ Method].
GC-MS/MS
STQ method
large-volume injection
pesticide residue
polymer-based solid-phase extraction mini-column
stomach-type glass line
Journal
Shokuhin eiseigaku zasshi. Journal of the Food Hygienic Society of Japan
ISSN: 0015-6426
Titre abrégé: Shokuhin Eiseigaku Zasshi
Pays: Japan
ID NLM: 0142214
Informations de publication
Date de publication:
2020
2020
Historique:
entrez:
28
4
2020
pubmed:
28
4
2020
medline:
4
8
2020
Statut:
ppublish
Résumé
As a method to detect pesticide residues in agricultural products, we evaluated the pretreatment of agricultural product samples by the solid-phase extracton technique with QuEChERS (STQ) method followed by GC-MS/MS with large-volume injection using a stomach-type glass-lined injector. This method satisfied the target criteria of recovery (70-120%) and the standard deviation of repeatability (RSD<25%) in 238-282 pesticides found in six types of agricultural products.
Identifiants
pubmed: 32336719
doi: 10.3358/shokueishi.61.47
doi:
Substances chimiques
Pesticide Residues
0
Types de publication
Journal Article
Langues
jpn
Sous-ensembles de citation
IM