Chromatographic determination of the free energy of adsorption and absorption characteristic of 4-(trans-4'-n-alkylcyclohexyl) benzoates.

Inverse gas chromatography Liquid crystalline stationary phases The free energy of adsorption and absorption (dissolution)

Journal

Journal of chromatography. A
ISSN: 1873-3778
Titre abrégé: J Chromatogr A
Pays: Netherlands
ID NLM: 9318488

Informations de publication

Date de publication:
05 Jul 2020
Historique:
received: 21 02 2020
revised: 06 04 2020
accepted: 07 04 2020
pubmed: 30 4 2020
medline: 1 8 2020
entrez: 30 4 2020
Statut: ppublish

Résumé

The characterisation of the energetic properties of liquid crystals, i.e., esters with elongated molecules has been performed. The changes of the free energies of adsorption and absorption (dissolutions), ΔG, for liquid crystals have been estimated, based on the retention times of the centre of gravity of the elution peaks determined for the substances with defined physicochemical properties. The temperature-dependent van der Waals component of the free energy, [Formula: see text] , for a crystalline form of liquid crystal has been estimated by employing the Dorris-Gray approach. These approaches have been widened to mesophases, namely, the absorption(dissolution) of n-alkanes in the smectic B and nematic phases.

Identifiants

pubmed: 32345440
pii: S0021-9673(20)30351-4
doi: 10.1016/j.chroma.2020.461120
pii:
doi:

Substances chimiques

Alkanes 0
Benzoates 0

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

461120

Informations de copyright

Copyright © 2020. Published by Elsevier B.V.

Déclaration de conflit d'intérêts

Declaration of Competing Interest No potential conflict of interest was reported by the authors.

Auteurs

Marcin Purchała (M)

Department of Advanced Technology and Chemistry, Institute of Chemistry, Military University of Technology, Warsaw, Poland. Electronic address: marcin1771@vp.pl.

Henryk Grajek (H)

Department of Advanced Technology and Chemistry, Institute of Chemistry, Military University of Technology, Warsaw, Poland. Electronic address: hgrajek5819@wp.pl.

Zygfryd Witkiewicz (Z)

Department of Advanced Technology and Chemistry, Institute of Chemistry, Military University of Technology, Warsaw, Poland. Electronic address: witkiew@wp.pl.

Mateusz Szala (M)

Department of Advanced Technology and Chemistry, Institute of Chemistry, Military University of Technology, Warsaw, Poland. Electronic address: mateusz.szala@wat.edu.pl.

Kajetan Kalus (K)

Department of Environment Hygiene and Animal Welfare, Wrocław University of Environmental and Life Sciences, Wrocław, Poland.

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