New Proluciferin Substrates for Human CYP4 Family Enzymes.

CYP4Z1 Cytochrome P450 Docking Fission yeast Homo sapiens Pharmacology Proluciferin Site of metabolism prediction

Journal

Applied biochemistry and biotechnology
ISSN: 1559-0291
Titre abrégé: Appl Biochem Biotechnol
Pays: United States
ID NLM: 8208561

Informations de publication

Date de publication:
Jan 2021
Historique:
received: 03 03 2020
accepted: 16 07 2020
pubmed: 2 9 2020
medline: 27 5 2021
entrez: 2 9 2020
Statut: ppublish

Résumé

We report the synthesis of seven new proluciferins for convenient activity determination of enzymes belonging to the cytochrome P450 (CYP) 4 family. Biotransformation of these probe substrates was monitored using each of the twelve human CYP4 family members, and eight were found to act at least on one of them. For all substrates, activity of CYP4Z1 was always highest, while that of CYP4F8 was always second highest. Site of metabolism (SOM) predictions involving SMARTCyp and docking experiments helped to rationalize the observed activity trends linked to substrate accessibility and reactivity. We further report the first homology model of CYP4F8 including suggested substrate recognition residues in a catalytically competent conformation accessed by replica exchange solute tempering (REST) simulations.

Identifiants

pubmed: 32869209
doi: 10.1007/s12010-020-03388-6
pii: 10.1007/s12010-020-03388-6
doi:

Substances chimiques

Thiazoles 0
Aryl Hydrocarbon Hydroxylases EC 1.14.14.1
CYP4F8 protein, human EC 1.14.14.1
CYP4Z1 protein, human EC 1.14.14.1
Cytochrome P450 Family 4 EC 1.14.14.1

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

218-237

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Auteurs

Jingyao Liu (J)

School of Pharmaceutical Science and Technology, Health Sciences Platform, Tianjin University, Tianjin, 300072, China.

David Machalz (D)

Pharmaceutical and Medicinal Chemistry (Computer-Aided Drug Design), Institute of Pharmacy, Freie Universität Berlin, 14195, Berlin, Germany.

Gerhard Wolber (G)

Pharmaceutical and Medicinal Chemistry (Computer-Aided Drug Design), Institute of Pharmacy, Freie Universität Berlin, 14195, Berlin, Germany.

Erik J Sorensen (EJ)

School of Pharmaceutical Science and Technology, Health Sciences Platform, Tianjin University, Tianjin, 300072, China. ejs@princeton.edu.
Department of Chemistry, Princeton University, Princeton, NJ, 08544, USA. ejs@princeton.edu.

Matthias Bureik (M)

School of Pharmaceutical Science and Technology, Health Sciences Platform, Tianjin University, Tianjin, 300072, China. matthias@tju.edu.cn.

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