Determination of pesticide residues in edible snails with QuEChERS coupled to GC-MS/MS.
Animals
Chlorobenzenes
/ analysis
Chlorpyrifos
/ analysis
Food Contamination
/ analysis
Gas Chromatography-Mass Spectrometry
Halogenated Diphenyl Ethers
/ analysis
Humans
Nitriles
/ analysis
No-Observed-Adverse-Effect Level
Pesticide Residues
/ analysis
Pyrethrins
/ analysis
Pyrimidines
/ analysis
Snails
/ chemistry
Solid Phase Extraction
Strobilurins
/ analysis
Triazoles
/ analysis
GC-MS/MS
Pesticide residues
daily intake
edible snails
Journal
Food additives & contaminants. Part A, Chemistry, analysis, control, exposure & risk assessment
ISSN: 1944-0057
Titre abrégé: Food Addit Contam Part A Chem Anal Control Expo Risk Assess
Pays: England
ID NLM: 101485040
Informations de publication
Date de publication:
Nov 2020
Nov 2020
Historique:
pubmed:
9
9
2020
medline:
18
5
2021
entrez:
8
9
2020
Statut:
ppublish
Résumé
A QuEChERS multi-residue GC-MS/MS method was developed for determining 160 pesticides in fresh edible snails. The method was validated according to the EU guidance SANTE/12682/2019. Twenty-seven different pesticides were quantified in the 824 samples analysed. Of these, 22.09% contained pesticide residues; in one case six different pesticides. The most frequently quantified pesticides were chlorpyrifos (108 samples), cypermethrin (50), difenoconazole (24), oxyfluorfen (13), lambda-cyhalothrin (12), tetraconazole and azoxystrobin (7). Other pesticides were found in <5 samples. Of the samples containing residues, 154 exceeded the EU legal limit. However, the estimated daily intake of pesticide residues showed that snail consumption does not represent appreciable risks to consumer health.
Identifiants
pubmed: 32897807
doi: 10.1080/19440049.2020.1809720
doi:
Substances chimiques
Chlorobenzenes
0
Halogenated Diphenyl Ethers
0
Nitriles
0
Pesticide Residues
0
Pyrethrins
0
Pyrimidines
0
Strobilurins
0
Triazoles
0
cypermethrin
1TR49121NP
oxyfluorofen
46GY4Y6567
tetraconazole
8FGY868T0G
Chlorpyrifos
JCS58I644W
azoxystrobin
NYH7Y08IPM
cyhalothrin
V0V73PEB8M
Types de publication
Journal Article
Langues
eng
Sous-ensembles de citation
IM