Determination of pesticide residues in edible snails with QuEChERS coupled to GC-MS/MS.


Journal

Food additives & contaminants. Part A, Chemistry, analysis, control, exposure & risk assessment
ISSN: 1944-0057
Titre abrégé: Food Addit Contam Part A Chem Anal Control Expo Risk Assess
Pays: England
ID NLM: 101485040

Informations de publication

Date de publication:
Nov 2020
Historique:
pubmed: 9 9 2020
medline: 18 5 2021
entrez: 8 9 2020
Statut: ppublish

Résumé

A QuEChERS multi-residue GC-MS/MS method was developed for determining 160 pesticides in fresh edible snails. The method was validated according to the EU guidance SANTE/12682/2019. Twenty-seven different pesticides were quantified in the 824 samples analysed. Of these, 22.09% contained pesticide residues; in one case six different pesticides. The most frequently quantified pesticides were chlorpyrifos (108 samples), cypermethrin (50), difenoconazole (24), oxyfluorfen (13), lambda-cyhalothrin (12), tetraconazole and azoxystrobin (7). Other pesticides were found in <5 samples. Of the samples containing residues, 154 exceeded the EU legal limit. However, the estimated daily intake of pesticide residues showed that snail consumption does not represent appreciable risks to consumer health.

Identifiants

pubmed: 32897807
doi: 10.1080/19440049.2020.1809720
doi:

Substances chimiques

Chlorobenzenes 0
Halogenated Diphenyl Ethers 0
Nitriles 0
Pesticide Residues 0
Pyrethrins 0
Pyrimidines 0
Strobilurins 0
Triazoles 0
cypermethrin 1TR49121NP
oxyfluorofen 46GY4Y6567
tetraconazole 8FGY868T0G
Chlorpyrifos JCS58I644W
azoxystrobin NYH7Y08IPM
cyhalothrin V0V73PEB8M

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

1881-1887

Auteurs

Miguel Angel Camara (MA)

Research Group of Pesticide Chemistry, Agrofood Pollution, Ecoefficiency and Toxicology, Faculty of Chemistry, University of Murcia , Murcia, Spain.

Aurelio Fuster (A)

Research Group of Pesticide Chemistry, Agrofood Pollution, Ecoefficiency and Toxicology, Faculty of Chemistry, University of Murcia , Murcia, Spain.

José Oliva (J)

Research Group of Pesticide Chemistry, Agrofood Pollution, Ecoefficiency and Toxicology, Faculty of Chemistry, University of Murcia , Murcia, Spain.

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Classifications MeSH