Wipe-sampling procedure optimisation for the determination of 23 antineoplastic drugs used in the hospital pharmacy.


Journal

European journal of hospital pharmacy : science and practice
ISSN: 2047-9956
Titre abrégé: Eur J Hosp Pharm
Pays: England
ID NLM: 101578294

Informations de publication

Date de publication:
03 2021
Historique:
received: 10 05 2019
revised: 02 07 2019
accepted: 09 07 2019
entrez: 20 2 2021
pubmed: 21 2 2021
medline: 2 4 2022
Statut: ppublish

Résumé

Optimise a wipe sampling procedure to evaluate the surface contamination for 23 antineoplastic drugs used in the hospital pharmacy. The influence of various parameters (ie, sampling device, sampling solution, desorption modes) was evaluated using a validated liquid chromatography-mass spectrometry (LC-MS/MS) method able to quantify 23 antineoplastic drugs widely used in the hospital pharmacy: 5-fluorouracil, busulfan, cyclophosphamide, cytarabine, dacarbazine, daunorubicin, docetaxel, doxorubicin, epirubicin, etoposide, etoposide phosphate, fludarabine phosphate, ganciclovir, gemcitabine, idarubicin, ifosfamide, irinotecan, methotrexate, paclitaxel, pemetrexed, raltitrexed, topotecan and vincristine. Best conditions were tested with real samples from a hospital pharmacy chemotherapy compounding unit. Polyester swabs (TX714 and TX716) gave satisfactory results for the desorption step for all compounds with mean recoveries of 90% and 95%, respectively. For the wiping step, higher recoveries were obtained using TX716 and isopropanol 75% as wiping solution. As anticipated, most intense contaminations were found close to the chemotherapy production site, on surfaces the most frequently in contact with operators' hands. Wipe sampling method was successfully developed and applied to real samples to determine surface contamination with 23 antineoplastic agents in trace amounts.

Identifiants

pubmed: 33608437
pii: ejhpharm-2019-001983
doi: 10.1136/ejhpharm-2019-001983
pmc: PMC7907690
doi:

Substances chimiques

Antineoplastic Agents 0
Ifosfamide UM20QQM95Y

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

94-99

Informations de copyright

© European Association of Hospital Pharmacists 2021. No commercial re-use. See rights and permissions. Published by BMJ.

Déclaration de conflit d'intérêts

Competing interests: None declared.

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Auteurs

Nicolas Guichard (N)

CYTOXLAB, Geneva University Hospitals, Geneva, Switzerland nicolas.guichard@hcuge.ch.
School of Pharmaceutical Sciences, University of Geneva, Geneva, Switzerland.
Pharmacy, Geneva University Hospitals, Geneva, Switzerland.

Julien Boccard (J)

School of Pharmaceutical Sciences, University of Geneva, Geneva, Switzerland.

Serge Rudaz (S)

School of Pharmaceutical Sciences, University of Geneva, Geneva, Switzerland.

Pascal Bonnabry (P)

School of Pharmaceutical Sciences, University of Geneva, Geneva, Switzerland.
Pharmacy, Geneva University Hospitals, Geneva, Switzerland.

Sandrine Fleury Souverain (S)

CYTOXLAB, Geneva University Hospitals, Geneva, Switzerland.
School of Pharmaceutical Sciences, University of Geneva, Geneva, Switzerland.
Pharmacy, Geneva University Hospitals, Geneva, Switzerland.

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Classifications MeSH