New Determination Method of Two Bioactive Saponins in Lysimachia capillipes Hemsl. by Quantitative Analysis of Multi-Components by Single-Marker.

Chromatography, High Pressure Liquid Drugs, Chinese Herbal Phytochemicals / chemistry Primulaceae / chemistry Saponins / chemistry

Journal

Journal of chromatographic science
ISSN: 1945-239X
Titre abrégé: J Chromatogr Sci
Pays: United States
ID NLM: 0173225

Informations de publication

Date de publication:
29 Oct 2021
Historique:
received: 30 09 2020
revised: 29 12 2020
accepted: 09 02 2021
pubmed: 18 3 2021
medline: 5 11 2021
entrez: 17 3 2021
Statut: ppublish

Résumé

Capilliposide B (CPS-B) and Capilliposide C (CPS-C), as the key components in Lysimachia capillipes Hemsl., increasingly aroused the interest and research concern of many researchers due to the good bioactivities. Nowadays, the reference standards of CPS-B and CPS-C yield were very limited. Due to the deficit of reference standards, the determination could be difficult to carry out, and the quality control and evaluation would be restrained afterwards. To solve this urgent problem, a quantitative analysis of multi-components by single-marker (QAMS) method was proposed and established based on high-performance liquid-chromatography tandem evaporative light-scattering detector. In this QAMS method, the content of the two bioactive components could be calculated by buddlejasaponin IV, which is applied as an external standard and readily obtained. And the methodological experiments were evaluated and indicated accuracy, stability and feasibility of this QAMS method. Therefore, in this study, this built method would properly meet the requirement of determination of CPS-B, CPS-C and quality control of the L. capillipes Hemsl. plant.

Identifiants

DOI: 10.1093/chromsci/bmab028 PMID: 33728454
pubmed: 33728454
pii: 6174328
doi: 10.1093/chromsci/bmab028
doi:

Substances chimiques

Drugs, Chinese Herbal 0
Phytochemicals 0
Saponins 0

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

941-948

Subventions

Organisme : National Science and Technology Major Project of China
ID : 2019ZX09301108
Organisme : National Natural Science Foundation of China
ID : 81872973
Organisme : Jiangsu Provincial Natural Science Foundation of China
ID : BK20190234
Organisme : Zhejiang Provincial Science and Technology Planning Project
ID : 2016C04005

Informations de copyright

© The Author(s) 2021. Published by Oxford University Press. All rights reserved. For permissions, please email: journals.permissions@oup.com.

Auteurs

Xiaoyong Zhang (X)

College of Biomedical Engineering and Instrument Science, Zhejiang University, Hangzhou 310027, China.

Xuezhao Chen (X)

College of Biomedical Engineering and Instrument Science, Zhejiang University, Hangzhou 310027, China.

Juan Jin (J)

Zhejiang Provincial People's Hospital, People's Hospital of Hangzhou Medical of College, Hangzhou 310014, China.

Minghua Gong (M)

Changshu Qiushi Technology Co., Ltd, Suzhou 215500, China.

Qiang He (Q)

Zhejiang Provincial People's Hospital, People's Hospital of Hangzhou Medical of College, Hangzhou 310014, China.

Shouxin Li (S)

College of Biomedical Engineering and Instrument Science, Zhejiang University, Hangzhou 310027, China.
Key Laboratory for Biomedical Engineering of Ministry of Education, Zhejiang-Malaysia Joint Research Center for Traditional Medicine, Zhejiang University, Hangzhou 310027, China.

Jinkui Tian (J)

College of Biomedical Engineering and Instrument Science, Zhejiang University, Hangzhou 310027, China.
Key Laboratory for Biomedical Engineering of Ministry of Education, Zhejiang-Malaysia Joint Research Center for Traditional Medicine, Zhejiang University, Hangzhou 310027, China.
ORCID: 0000-0001-5472-204X

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Classifications MeSH

questionsmedicales.fr › Techniques d'investigation › Techniques de chimie analytique › Chromatographie › Chromatographie en phase liquide › Chromatographie en phase liquide à haute performance › New Determination Method of Two Bioactive...
questionsmedicales.fr › Préparations pharmaceutiques › Médicaments issus de plantes chinoises › New Determination Method of Two Bioactive...
questionsmedicales.fr › Facteurs biologiques › Composés phytochimiques › New Determination Method of Two Bioactive...
questionsmedicales.fr › Eucaryotes › Viridiplantae › Streptophyta › Embryophyta › Tracheobionta › Magnoliopsida › Theales › Primulaceae › New Determination Method of Two Bioactive...
questionsmedicales.fr › Glucides › Hétérosides › Saponines › New Determination Method of Two Bioactive...