Optimizing Chitin Depolymerization by Lysozyme to Long-Chain Oligosaccharides.

chemo-enzymatic synthesis chitin oligosaccharides lysozyme response surface methodology

Journal

Marine drugs
ISSN: 1660-3397
Titre abrégé: Mar Drugs
Pays: Switzerland
ID NLM: 101213729

Informations de publication

Date de publication:
31 May 2021
Historique:
received: 18 05 2021
revised: 27 05 2021
accepted: 28 05 2021
entrez: 2 6 2021
pubmed: 3 6 2021
medline: 15 12 2021
Statut: epublish

Résumé

Chitin oligosaccharides (COs) hold high promise as organic fertilizers in the ongoing agro-ecological transition. Short- and long-chain COs can contribute to the establishment of symbiotic associations between plants and microorganisms, facilitating the uptake of soil nutrients by host plants. Long-chain COs trigger plant innate immunity. A fine investigation of these different signaling pathways requires improving the access to high-purity COs. Here, we used the response surface methodology to optimize the production of COs by enzymatic hydrolysis of water-soluble chitin (WSC) with hen egg-white lysozyme. The influence of WSC concentration, its acetylation degree, and the reaction time course were modelled using a Box-Behnken design. Under optimized conditions, water-soluble COs up to the nonasaccharide were formed in 51% yield and purified to homogeneity. This straightforward approach opens new avenues to determine the complex roles of COs in plants.

Identifiants

pubmed: 34072871
pii: md19060320
doi: 10.3390/md19060320
pmc: PMC8229320
pii:
doi:

Substances chimiques

Oligosaccharides 0
Chitin 1398-61-4
hen egg lysozyme EC 3.2.1.-
Muramidase EC 3.2.1.17

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Subventions

Organisme : Agence Nationale de la Recherche
ID : ANR 14-CE18-0008

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Auteurs

Arnaud Masselin (A)

Université Grenoble Alpes, CNRS, CERMAV, 38000 Grenoble, France.

Antoine Rousseau (A)

Université Grenoble Alpes, CNRS, CERMAV, 38000 Grenoble, France.

Stéphanie Pradeau (S)

Université Grenoble Alpes, CNRS, CERMAV, 38000 Grenoble, France.

Laure Fort (L)

Université Grenoble Alpes, CNRS, DCM, 38000 Grenoble, France.

Rodolphe Gueret (R)

Université Grenoble Alpes, CNRS, DCM, 38000 Grenoble, France.

Laurine Buon (L)

Université Grenoble Alpes, CNRS, CERMAV, 38000 Grenoble, France.

Sylvie Armand (S)

Université Grenoble Alpes, CNRS, CERMAV, 38000 Grenoble, France.

Sylvain Cottaz (S)

Université Grenoble Alpes, CNRS, CERMAV, 38000 Grenoble, France.

Luc Choisnard (L)

Université Grenoble Alpes, CNRS, DPM, 38000 Grenoble, France.

Sébastien Fort (S)

Université Grenoble Alpes, CNRS, CERMAV, 38000 Grenoble, France.

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