Development and validation of ultra-high performance supercritical fluid chromatography method for quantitative determination of six compounds in Guizhi Fuling capsule and tablet samples.
Guizhi fuling formula
multiple compounds
ultra-high performance supercritical fluid chromatography
Journal
Journal of separation science
ISSN: 1615-9314
Titre abrégé: J Sep Sci
Pays: Germany
ID NLM: 101088554
Informations de publication
Date de publication:
Sep 2021
Sep 2021
Historique:
revised:
24
06
2021
received:
05
03
2021
accepted:
30
06
2021
pubmed:
3
7
2021
medline:
12
1
2022
entrez:
2
7
2021
Statut:
ppublish
Résumé
A fast and simple ultra-high performance supercritical fluid chromatography method has been developed for the determination of six analytes, namely (paeonol, coumarin, cinnamic alcohol, cinnamic acid, paeoniflorin, and amygdalin) in Guizhi Fuling capsule and tablet samples. The influence of the key chromatographic parameters for the separation purposes was evaluated. The optimal column was Trefoil CEL1 column. The optimal mobile phase was a gradient mixture of carbon dioxide and methanol at flow rate of 1.0 mL/min. The back pressure of the system was set to 1.38 × 10
Identifiants
pubmed: 34213832
doi: 10.1002/jssc.202100181
doi:
Substances chimiques
Acetophenones
0
Capsules
0
Cinnamates
0
Coumarins
0
Drugs, Chinese Herbal
0
Glucosides
0
Monoterpenes
0
Propanols
0
Tablets
0
guizhi-fuling
0
cinnamic acid
140-10-3
Amygdalin
214UUQ9N0H
peoniflorin
21AIQ4EV64
paeonol
3R834EPI82
coumarin
A4VZ22K1WT
cinnamyl alcohol
SS8YOP444F
Types de publication
Journal Article
Validation Study
Langues
eng
Sous-ensembles de citation
IM
Pagination
3199-3207Subventions
Organisme : the Project of Young innovative talents in Colleges and Universities in Guangdong Province
ID : 2018KQNCX263
Organisme : Jiangmen Program for Innovative Research Team
ID : 2018630100180019806
Organisme : the Jiangmen City Science and Technology Basic Research Project
ID : 2020030102060005412
Organisme : the team project of Wuyi University
ID : 2019td09
Organisme : High-level Talents for Scientific Research
ID : 2018AL007
Organisme : High-level Talents for Scientific Research
ID : 2018AL002
Organisme : High-level Talents for Scientific Research
ID : 2018AL003
Informations de copyright
© 2021 Wiley-VCH GmbH.
Références
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