Zirconium Nanoparticles Based Vortex Assisted Ligandless Dispersive Solid Phase Extraction for Trace Determination of Lead in Domestic Wastewater using Flame Atomic Absorption Spectrophotometry.
Flame atomic absorption spectrophotometry
Lead
Ligandless dispersive solid phase extraction
Slotted quartz tube
Wastewater samples
Zirconium nanoparticles
Journal
Bulletin of environmental contamination and toxicology
ISSN: 1432-0800
Titre abrégé: Bull Environ Contam Toxicol
Pays: United States
ID NLM: 0046021
Informations de publication
Date de publication:
Feb 2022
Feb 2022
Historique:
received:
30
03
2021
accepted:
22
06
2021
pubmed:
4
7
2021
medline:
19
2
2022
entrez:
3
7
2021
Statut:
ppublish
Résumé
In this paper, a sensitive and simple zirconium nanoparticles (Zr-NPs) based vortex assisted ligandless dispersive solid phase extraction (VA-LDSPE) method was developed for the preconcentration of lead from wastewater samples for the determination by slotted quartz tube-flame atomic absorption spectrometry (SQT-FAAS). Zr-NPs were synthesized using zirconium (IV) chloride salt as a starting material through a simple reduction process with sodium borohydride, and used as selective adsorbent for the extraction of lead ions from aqueous medium. Single variant experiments were carried out for all optimizations of sorption/desorption steps including pH of solution, amount of nanoparticles, mixing type/period and eluent type. An SQT with five round slots was placed onto the burner of FAAS to increase the interaction between lead atoms and light from radiation source to enhance the absorbance signals. Under the determined optimum conditions, analytical figures of merit were evaluated and the limit of detection and quantification (LOD/LOQ) values were calculated as 5.2 and 17.3 µg L
Identifiants
pubmed: 34215925
doi: 10.1007/s00128-021-03318-0
pii: 10.1007/s00128-021-03318-0
doi:
Substances chimiques
Waste Water
0
Lead
2P299V784P
Zirconium
C6V6S92N3C
Types de publication
Journal Article
Langues
eng
Sous-ensembles de citation
IM
Pagination
324-330Informations de copyright
© 2021. The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature.
Références
Bayrak Y, Yesiloglu Y, Gecgel U (2006) Adsorption behavior of Cr(VI) on activated hazelnut shell ash and activated bentonite. Microporous Mesoporous Mater 91:107–110. https://doi.org/10.1016/j.micromeso.2005.11.010
doi: 10.1016/j.micromeso.2005.11.010
Dönmez KB, Çetinkaya E, Deveci S et al (2017) Preparation of electrochemically treated nanoporous pencil-graphite electrodes for the simultaneous determination of Pb and Cd in water samples. Anal Bioanal Chem 409:4827–4837. https://doi.org/10.1007/s00216-017-0426-3
doi: 10.1007/s00216-017-0426-3
Ghaedi M, Tavallali H, Shokrollahi A et al (2009) Flame atomic absorption spectrometric determination of zinc, nickel, iron and lead in different matrixes after solid phase extraction on sodium dodecyl sulfate (SDS)-coated alumina as their bis (2-hydroxyacetophenone)-1, 3-propanediimine chelates. J Hazard Mater 166:1441–1448. https://doi.org/10.1016/j.jhazmat.2008.12.066
doi: 10.1016/j.jhazmat.2008.12.066
Giakisikli G, Anthemidis AN (2013) Magnetic materials as sorbents for metal/metalloid preconcentration and/or separation. A review. Anal Chim Acta 789:1–16
doi: 10.1016/j.aca.2013.04.021
Hajiaghababaei L, Badiei A, Ganjali MR et al (2011) Highly efficient removal and preconcentration of lead and cadmium cations from water and wastewater samples using ethylenediamine functionalized SBA-15. Desalination 266:182–187. https://doi.org/10.1016/j.desal.2010.08.024
doi: 10.1016/j.desal.2010.08.024
Kaya G, Yaman M (2008) Online preconcentration for the determination of lead, cadmium and copper by slotted tube atom trap (STAT)-flame atomic absorption spectrometry. Talanta 75:1127–1133. https://doi.org/10.1016/J.TALANTA.2008.01.008
doi: 10.1016/J.TALANTA.2008.01.008
Khan M, Yilmaz E, Soylak M (2016) Vortex assisted magnetic solid phase extraction of lead(II) and cobalt(II) on silica coated magnetic multiwalled carbon nanotubes impregnated with 1-(2-pyridylazo)-2-naphthol. J Mol Liq 224:639–647. https://doi.org/10.1016/J.MOLLIQ.2016.10.023
doi: 10.1016/J.MOLLIQ.2016.10.023
Kobya M, Demirbas E, Senturk E, Ince M (2005) Adsorption of heavy metal ions from aqueous solutions by activated carbon prepared from apricot stone. Bioresour Technol 96:1518–1521. https://doi.org/10.1016/j.biortech.2004.12.005
doi: 10.1016/j.biortech.2004.12.005
Lemos VA, Santelli RE, De Carvalho MS, Ferreira SLC (2000) Application of polyurethane foam loaded with BTAC in an on-line preconcentration system: cadmium determination by FAAS. Spectrochim acta: Part B At Spectrosc 55:1497–1502. https://doi.org/10.1016/S0584-8547(00)00257-3
doi: 10.1016/S0584-8547(00)00257-3
Lemos VA, Teixeira LSG, Bezerra M de A, et al (2008) New materials for solid-phase extraction of trace elements. Appl Spectrosc Rev 43:303–334. https://doi.org/10.1080/05704920802031341
doi: 10.1080/05704920802031341
Liu G, Lin Y (2005) Electrochemical sensor for organophosphate pesticides and nerve agents using zirconia nanoparticles as selective sorbents. Anal Chem 77:5894–5901. https://doi.org/10.1021/ac050791t
doi: 10.1021/ac050791t
Mandlate JS, Soares BM, Seeger TS et al (2017) Determination of cadmium and lead at sub-ppt level in soft drinks: an efficient combination between dispersive liquid-liquid microextraction and graphite furnace atomic absorption spectrometry. Food Chem 221:907–912. https://doi.org/10.1016/j.foodchem.2016.11.075
doi: 10.1016/j.foodchem.2016.11.075
Matoso E, Kubota LT, Cadore S (2003) Use of silica gel chemically modified with zirconium phosphate for preconcentration and determination of lead and copper by flame atomic absorption spectrometry. Talanta 60:1105–1111. https://doi.org/10.1016/S0039-9140(03)00215-7
doi: 10.1016/S0039-9140(03)00215-7
Mohammadi SZ, Afzali D, Fallahi Z (2014) Ionic liquid-based dispersive liquid-liquid microextraction for the separation and preconcentration of lead in water samples prior to FAAS determination without chelating agent. Int J Environ Anal Chem 94:765–773. https://doi.org/10.1080/03067319.2013.879297
doi: 10.1080/03067319.2013.879297
Mohammadi SZ, Shamspur T, Afzali D et al (2016) Applicability of cloud point extraction for the separation trace amount of lead ion in environmental and biological samples prior to determination by flame atomic absorption spectrometry. Arab J Chem 9:S610–S615. https://doi.org/10.1016/j.arabjc.2011.07.003
doi: 10.1016/j.arabjc.2011.07.003
Naeemullah, Kazi TG, Shah F et al (2012) A green preconcentration method for determination of cobalt and lead in fresh surface and waste water samples prior to flame atomic absorption spectrometry. J Anal Methods Chem 1:. https://doi.org/10.1155/2012/713862
doi: 10.1155/2012/713862
Nikam A, Pagar T, Ghotekar S et al (2019) A review on plant extract mediated green synthesis of zirconia nanoparticles and their miscellaneous applications. J Chem Rev 1:154–163. https://doi.org/10.33945/sami/jcr.2019.3.1
doi: 10.33945/sami/jcr.2019.3.1
Ozdemir S, Kilinc E, Oner ET (2019) Preconcentrations and determinations of copper, nickel and lead in baby food samples employing Coprinus silvaticus immobilized multi-walled carbon nanotube as solid phase sorbent. Food Chem 276:174–179. https://doi.org/10.1016/j.foodchem.2018.07.123
doi: 10.1016/j.foodchem.2018.07.123
Parham H, Pourreza N, Rahbar N (2009) Solid phase extraction of lead and cadmium using solid sulfur as a new metal extractor prior to determination by flame atomic absorption spectrometry. J Hazard Mater 163:588–592. https://doi.org/10.1016/j.jhazmat.2008.07.007
doi: 10.1016/j.jhazmat.2008.07.007
Reddy CV, Reddy IN, Harish VVN et al (2020) Efficient removal of toxic organic dyes and photoelectrochemical properties of iron-doped zirconia nanoparticles. Chemosphere 239:124766. https://doi.org/10.1016/j.chemosphere.2019.124766
doi: 10.1016/j.chemosphere.2019.124766
Salari S, Bahrami A, Ghamari F, Shahna FG (2018) Multivariate optimization of the hollow fiber-based liquid phase microextraction of lead in human blood and urine samples using graphite furnace atomic absorption spectrometry. Chem Pap 72:1945–1952. https://doi.org/10.1007/s11696-018-0435-5
doi: 10.1007/s11696-018-0435-5
Shah F, Kazi TG, Afridi HI et al (2010) Environmental exposure of lead and iron deficit anemia in children age ranged 1-5years: A cross sectional study. Sci Total Environ 408:5325–5330. https://doi.org/10.1016/j.scitotenv.2010.07.091
doi: 10.1016/j.scitotenv.2010.07.091
Soylak M, Koksal M (2019) Deep eutectic solvent microextraction of lead(II), cobalt(II), nickel(II) and manganese(II) ions for the separation and preconcentration in some oil samples from Turkey prior to their microsampling flame atomic absorption spectrometric determination. Microchem J 147:832–837. https://doi.org/10.1016/j.microc.2019.04.006
doi: 10.1016/j.microc.2019.04.006
Tekin Z, Özdoğan N, Bakırdere S (2020) Zirconium nanoparticles based solid phase extraction-slotted quartz tube-flame atomic absorption spectrophotometry for the determination of cadmium in wastewater samples and evaluation of green profile. Int J Environ Anal Chem. https://doi.org/10.1080/03067319.2020.1728262
doi: 10.1080/03067319.2020.1728262
Vicentino PO, Cassella RJ, Leite D, Resano M (2020) Extraction induced by microemulsion breaking as a novel tool for the simultaneous determination of Cd, Mn, Pb and Sb in gasoline samples by ICP-MS and discrete sample introduction. Talanta 206:120230. https://doi.org/10.1016/j.talanta.2019.120230
doi: 10.1016/j.talanta.2019.120230
Watling RJ (1977) The use of a slotted quartz tube for the determination of arsenic, antimony, selenium and mercury. Anal Chim Acta 94:181–186. https://doi.org/10.1016/S0003-2670(01)83645-X
doi: 10.1016/S0003-2670(01)83645-X
Wei XS, Wu YW, Han LJ (2015) Determination of lead and cadmium in water and pharmaceutical products by inductively coupled plasma optical emission spectrometry with preconcentration by thiourea immobilized silica. Anal Lett 48:996–1008. https://doi.org/10.1080/00032719.2014.966379
doi: 10.1080/00032719.2014.966379
Zhou Q, Zhao N, Xie G (2011) Determination of lead in environmental waters with dispersive liquid-liquid microextraction prior to atomic fluorescence spectrometry. J Hazard Mater 189:48–53. https://doi.org/10.1016/j.jhazmat.2011.01.123
doi: 10.1016/j.jhazmat.2011.01.123