Persistent Water Repellency of Syndiotactic Polymethylene with Perfluoroethyl Hexyloxycarbonyl Side Chains.


Journal

Macromolecular rapid communications
ISSN: 1521-3927
Titre abrégé: Macromol Rapid Commun
Pays: Germany
ID NLM: 9888239

Informations de publication

Date de publication:
Sep 2021
Historique:
revised: 07 07 2021
received: 18 05 2021
pubmed: 7 8 2021
medline: 9 9 2021
entrez: 6 8 2021
Statut: ppublish

Résumé

Polyacrylates bearing long fluoroalkyl (Rf) side chains are known to have ultralow surface energies that are appropriate for functional coating and fabric finishing. However, these long Rf chains cause health concerns because of the risk of toxic and bioaccumulative perfluoroalcanoic acid emission via oxidative degradation. This work demonstrates that incorporating a short Rf chain of perfluoroethylene at the end of the side chains of syndiotactic poly(substituted methylene) (PM) produces hydrophobicity. A contact angle of 105° of PM remains constant for more than 50 s, whereas that of the polyacrylate (PA) with the same side chain rapidly decreases from 85° to 44° over the same period. Such persistent water repellency of the PM is ascribed to a liquid crystal structure comprised the main chains arranged in a 2D hexagonal lattice and side chains that extend perpendicularly from these main chains.

Identifiants

pubmed: 34355439
doi: 10.1002/marc.202100311
doi:

Substances chimiques

Water 059QF0KO0R

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

e2100311

Subventions

Organisme : JST CREST
ID : JPMJCR19I3

Informations de copyright

© 2021 Wiley-VCH GmbH.

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Auteurs

Ayano Yoshitake (A)

Department of Chemical Science and Engineering, Tokyo Institute of Technology, Ookayama, Meguro-ku, Tokyo, 152-8550, Japan.

Hiroyuki Kudo (H)

Department of Chemical Science and Engineering, Tokyo Institute of Technology, Ookayama, Meguro-ku, Tokyo, 152-8550, Japan.

Hidetoshi Matsumoto (H)

Department of Materials Science and Engineering, Tokyo Institute of Technology, Ookayama, Meguro-ku, Tokyo, 152-8550, Japan.

Masatoshi Tokita (M)

Department of Chemical Science and Engineering, Tokyo Institute of Technology, Ookayama, Meguro-ku, Tokyo, 152-8550, Japan.

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