Computational analyses of the vibrational spectra of fentanyl, carfentanil and remifentanil.


Journal

Spectrochimica acta. Part A, Molecular and biomolecular spectroscopy
ISSN: 1873-3557
Titre abrégé: Spectrochim Acta A Mol Biomol Spectrosc
Pays: England
ID NLM: 9602533

Informations de publication

Date de publication:
05 Apr 2022
Historique:
received: 16 04 2021
revised: 30 11 2021
accepted: 12 12 2021
pubmed: 11 1 2022
medline: 9 2 2022
entrez: 10 1 2022
Statut: ppublish

Résumé

The infrared (IR) spectra of fentanyl, carfentanil and remifentanil, and protonated salts, are computed using quantum chemistry methods. New experimental FTIR spectra are also reported and compared to the calculations. The accuracy of two density functional theory methods, B3LYP and M06-2X, are tested against higher level theories (MP2) and the experimental data. Gas phase IR spectra are calculated for both the neutral and protonated molecules in order to compare with the experimental data measured for various salts of fentanyl and its analogues. Key vibrational modes are selected and studied in detail using a vibrational mode locality calculation. The main contributing atomic movements in these vibrational modes are identified.

Identifiants

pubmed: 35007908
pii: S1386-1425(21)01340-8
doi: 10.1016/j.saa.2021.120763
pii:
doi:

Substances chimiques

carfentanil LA9DTA2L8F
Remifentanil P10582JYYK
Fentanyl UF599785JZ

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

120763

Informations de copyright

Crown Copyright © 2022. Published by Elsevier B.V. All rights reserved.

Déclaration de conflit d'intérêts

Declaration of Competing Interest The authors declare that they have no known competing financial interests or personal relationships that could have appeared to influence the work reported in this paper.

Auteurs

Xiao Shan (X)

Physical and Theoretical Chemistry Laboratory, Department of Chemistry, University of Oxford, South Parks Road, Oxford OX1 3QZ, United Kingdom.

Linda Lee (L)

Chemical, Biological and Radiological Division, Defence Science and Technology Laboratory (Dstl), Porton Down, Salisbury, Wiltshire SP4 0JQ, United Kingdom.

Rhea J Clewes (RJ)

Chemical, Biological and Radiological Division, Defence Science and Technology Laboratory (Dstl), Porton Down, Salisbury, Wiltshire SP4 0JQ, United Kingdom.

Christopher R Howle (CR)

Chemical, Biological and Radiological Division, Defence Science and Technology Laboratory (Dstl), Porton Down, Salisbury, Wiltshire SP4 0JQ, United Kingdom.

Mark R Sambrook (MR)

Chemical, Biological and Radiological Division, Defence Science and Technology Laboratory (Dstl), Porton Down, Salisbury, Wiltshire SP4 0JQ, United Kingdom.

David C Clary (DC)

Physical and Theoretical Chemistry Laboratory, Department of Chemistry, University of Oxford, South Parks Road, Oxford OX1 3QZ, United Kingdom. Electronic address: david.clary@chem.ox.ac.uk.

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Classifications MeSH