Performance of innovative nanomaterials for bone remains consolidation and effect on


Journal

Scientific reports
ISSN: 2045-2322
Titre abrégé: Sci Rep
Pays: England
ID NLM: 101563288

Informations de publication

Date de publication:
28 04 2022
Historique:
received: 22 12 2021
accepted: 12 04 2022
entrez: 28 4 2022
pubmed: 29 4 2022
medline: 3 5 2022
Statut: epublish

Résumé

An innovative protocol for the consolidation of ancient bone remains based on the use of nanometric HydroxyAPatite (HAP) was set up and tested through a multidisciplinary approach. A new protocol for the synthesis of HAP nanoparticles was developed, and the composition of the obtained nanomaterial was investigated through Fourier Transform Infrared Spectroscopy (FTIR) and X-Ray Diffraction (XRD); sizes, shape and morphology of the synthesized particles were studied by Scanning Electron Microscopy (SEM). The consolidation performance was evaluated by testing the new nanomaterial on degraded ancient bone findings. An increase of the mineral density and of the micro-hardness of the bone were observed. The new consolidation method was also tested to assess possible effects on the palaeogenetic analysis and radiocarbon dating on the treated bones. The consolidation treatment does not introduce any contaminations that could affect radiocarbon dating and has no general detrimental impact on the genetic characterization of the skeletal remains. This consolidation procedure represents a more compatible conservation tool with respect to traditional procedures: it has been shown that the treatment is effective, easily-applicable and compatible with post-consolidation analysis.

Identifiants

pubmed: 35484192
doi: 10.1038/s41598-022-10798-5
pii: 10.1038/s41598-022-10798-5
pmc: PMC9050738
doi:

Substances chimiques

Durapatite 91D9GV0Z28

Types de publication

Journal Article Research Support, Non-U.S. Gov't

Langues

eng

Sous-ensembles de citation

IM

Pagination

6975

Informations de copyright

© 2022. The Author(s).

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Auteurs

Francesca Porpora (F)

Department of Chemistry Ugo Schiff" and CSGI Consortium, University of Florence, via della Lastruccia 3-13, 50019, Sesto Fiorentino, FI, Italy.

Valentina Zaro (V)

Department of Biology, University of Florence, via del Proconsolo 12, 50122, Florence, FI, Italy.

Lucia Liccioli (L)

INFN (Istituto Nazionale Di Fisica Nucleare) Sezione Di Firenze, via G. Sansone 1, 50019, Sesto Fiorentino, FI, Italy.

Alessandra Modi (A)

Department of Biology, University of Florence, via del Proconsolo 12, 50122, Florence, FI, Italy.

Arianna Meoli (A)

Department of Chemistry Ugo Schiff" and CSGI Consortium, University of Florence, via della Lastruccia 3-13, 50019, Sesto Fiorentino, FI, Italy.

Giulia Marradi (G)

Department of Chemistry Ugo Schiff" and CSGI Consortium, University of Florence, via della Lastruccia 3-13, 50019, Sesto Fiorentino, FI, Italy.

Serena Barone (S)

INFN (Istituto Nazionale Di Fisica Nucleare) Sezione Di Firenze, via G. Sansone 1, 50019, Sesto Fiorentino, FI, Italy.

Stefania Vai (S)

Department of Biology, University of Florence, via del Proconsolo 12, 50122, Florence, FI, Italy.

Luigi Dei (L)

Department of Chemistry Ugo Schiff" and CSGI Consortium, University of Florence, via della Lastruccia 3-13, 50019, Sesto Fiorentino, FI, Italy.

David Caramelli (D)

Department of Biology, University of Florence, via del Proconsolo 12, 50122, Florence, FI, Italy.

Mariaelena Fedi (M)

INFN (Istituto Nazionale Di Fisica Nucleare) Sezione Di Firenze, via G. Sansone 1, 50019, Sesto Fiorentino, FI, Italy. fedi@fi.infn.it.

Martina Lari (M)

Department of Biology, University of Florence, via del Proconsolo 12, 50122, Florence, FI, Italy. martina.lari@unifi.it.

Emiliano Carretti (E)

Department of Chemistry Ugo Schiff" and CSGI Consortium, University of Florence, via della Lastruccia 3-13, 50019, Sesto Fiorentino, FI, Italy. emiliano.carretti@unifi.it.

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Classifications MeSH