A modified quick-easy-cheap-effective-rugged-and-safe method involving carbon nano-onions-based dispersive solid-phase extraction and dispersive liquid-liquid microextraction for pesticides from grapes.
carbon nano-onion
dispersive liquid-liquid microextraction
dispersive solid-phase extraction
gas chromatography
pesticide
Journal
Journal of separation science
ISSN: 1615-9314
Titre abrégé: J Sep Sci
Pays: Germany
ID NLM: 101088554
Informations de publication
Date de publication:
Sep 2022
Sep 2022
Historique:
revised:
16
07
2022
received:
13
02
2022
accepted:
16
07
2022
pubmed:
15
8
2022
medline:
30
9
2022
entrez:
14
8
2022
Statut:
ppublish
Résumé
A combination of modified quick easy cheap effective rugged and safe extraction approach with carbon nano-onions-based dispersive solid-phase extraction and dispersive liquid-liquid microextraction was developed for the extraction of several pesticides (diazinon, chlorpyrifos, tebuconazole, deltamethrin, permethrin, haloxyfop-methyl, penconazole, and cyhalothrin) from grape before their analysis by gas chromatography-flame ionization detection. In the extraction approach, an aliquot of grape sample is chopped and after separating its juice, the pesticides that remained in the refuse are extracted by the quick, easy, cheap, effective, rugged, and safe extraction method. The obtained acetonitrile phase is mixed with juice and the analytes are extracted by the carbon nano-onions-based dispersive solid-phase extraction. The analytes are concentrated using the microextraction procedure to obtain high enrichment factors. The results showed low limits of detection (0.5-1.6 ng/g) and quantification (1.8-5.4 ng/g) with satisfactory linearity of the calibration curves (determination coefficient, r
Identifiants
pubmed: 35964286
doi: 10.1002/jssc.202200124
doi:
Substances chimiques
Acetonitriles
0
Pesticides
0
Permethrin
509F88P9SZ
Carbon
7440-44-0
Chlorpyrifos
JCS58I644W
Diazinon
YUS1M1Q929
Types de publication
Journal Article
Langues
eng
Sous-ensembles de citation
IM
Pagination
3582-3593Subventions
Organisme : Research Council of the Tabriz University of Medical Science
ID : 66357
Informations de copyright
© 2022 Wiley-VCH GmbH.
Références
Deng H, Ji Y, Tang S, Yang F, Tang G, Shi H, Lee HK. Application of chiral and achiral supercritical fluid chromatography in pesticide analysis: a review. J Chromatogr A. 2020;1634:461684.
Farajzadeh MA, Feriduni B, Afshar Mogaddam MR. Extraction and enrichment of triazole and triazine pesticides from honey using air-assisted liquid-liquid microextraction. J Food Sci. 2014;79:H2140-8.
Huang G, Deng Y, Zhang Y, Feng P, Xu C, Fu L, Lin B. Study on long-term pest control and stability of double-layer pesticide carrier in indoor and outdoor environment. J Chem Eng. 2021;403:126342.
Chen X, Zhang F, Yao H, Wang J, Qi D, Guo Y. Analyzing multiple pesticides in tobacco leaf using gas chromatography with quadrupole time-of-flight mass spectrometry. J Sep Sci. 2018;41:1983-9.
Varela-Martínez DA, González-Curbelo MÁ, González-Sálamo J, Hernández-Borges J. Determination of pesticides in dried minor tropical fruits from Colombia using the quick, easy, cheap, effective, rugged, and safe method-gas chromatography-tandem mass spectrometry. J Sep Sci. 2020;43:929-35.
Volz SA, Johnston JJ. Solid phase extraction/gas chromatography/electron capture detector method for the determination of organochlorine pesticides in wildlife and wildlife food sources, J Sep Sci 2002;29:119-24.
Hernández F, Grimalt S, Pozo ÓJ, Sancho JV. Use of ultra-high-pressure liquid chromatography-quadrupole time-of-flight MS to discover the presence of pesticide metabolites in food samples, J Sep Sci 2009;32:2245-61.
Nemati M, Tuzen M, Farazajdeh MA, Kaya S, Afshar Mogaddam MR. Development of dispersive solid-liquid extraction method based on organic polymers followed by deep eutectic solvents elution; application in extraction of some pesticides from milk samples prior to their determination by HPLC-MS/MS. Anal Chim Acta. 2020;1199:339570.
Lia Y, Luo Q, Hu R, Chen Z, Qiu P. A sensitive and rapid UV-vis spectrophotometry for organophosphorus pesticides detection based on Ytterbium (Yb3+) functionalized gold nanoparticles, Chin Chem Lett 2018;29:1845-8.
Pinho GP, Augusto Neves A, Ribeirode Queiroz MEL, Oliveira Silvério F. Optimization of the liquid-liquid extraction method and low temperature purification (LLE-LTP) for pesticide residue analysis in honey samples by gas chromatography, Food Control. 2010;21:1307-11.
Farajzadeh MA, Khoshmaram L, Mogaddam MRA. Combination of solid-phase extraction-hollow fiber for ultra-preconcentration of some triazole pesticides followed by gas chromatography-flame ionization detection, J Sep Sci 2012;35:121-7.
Blasco C, Fernández M, Picó Y, Font G. Comparison of solid-phase microextraction and stir bar sorptive extraction for determining six organophosphorus insecticides in honey by liquid chromatography-mass spectrometry, J Chromatogr A. 2004;1030:77-85.
Farajzadeh MA, Khoshmaram L. Air-assisted liquid-liquid microextraction-gas chromatography-flame ionisation detection: a fast and simple method for the assessment of triazole pesticides residues in surface water, cucumber, tomato and grape juices samples, Food Chem. 2013;141:1881-7.
Li Y, Li B, Qi Y, Zhang Z, Cong S, She Y, Cao X. Synthesis of metal-organic framework @molecularly imprinted polymer adsorbents for solid phase extraction of organophosphorus pesticides from agricultural products, J Chromatogr B. 2022;1188:123081.
Camel V. Solid phase extraction of trace elements, J Spectrochim Acta. 2003;58:1177-233.
Franke JP, de Zeeuw RA. Solid−phase extraction procedures in systematic toxicological analysis, J Chromatogr B. 1998;713:51-9.
Focant JF, De Pauw E. Fast automated extraction and clean−up of biological fluids for polychlorinated dibenzo−p−dioxins, dibenzofurans and coplanar polychlorinated biphenyls analysis, J Chromatogr B. 2002;776:199-212.
Hengel MJ, Shibamoto T. Gas chromatographic−mass spectrometric method for the analysis of dimethomorph fungicide in dried hops, J Agric Food Chem 2000;48:5824-8.
Abdelaty Habila M, ALOthman ZA, Al-Tamrah SA, Abdel Ghafar A, Soylak M. Activated carbon from waste as an efficient adsorbent for malathion for detection and removal purposes, J Ind Eng Chem 2015;32:336-44.
ALOthman ZA, Yilmaz E, Habila MA, Ghfar AA, Alhenaki B, Soylak M, Badjah Hadj AY. Supramolecular solvent microextraction and ultra-performance liquid chromatography-tandem mass spectrometry combination for the preconcentration and determination of malathion in environmental samples, Desalin Water Treat 2019;144:166-71.
Habila MA, Alhenaki B, El-Marghany A, Sheikh M, Ghfar A, ALO Zeid, Soylak M. Metal-organic frameworks enhanced dispersive solid phase microextraction of malathion before detection by UHPLC-MS/MS, J Sep Sci 2020;43:3103-9.
Habila MA, Alhenaki B, El-Marghany A, Sheikh M, Ghfar AA, ALOthman ZA, Soylak M. Metal-organic framework-based dispersive solid-phase microextraction of carbaryl from food and water prior to detection by ultra-performance liquid chromatography-tandem mass spectrometry, Separations. 2022;9:32.
Zhao P, Wang L, Jiang Y, Zhang F, Pan C. Dispersive cleanup of acetonitrile extracts of tea samples by mixed multiwalled carbon nanotubes, primary secondary amine, and graphitized carbon black sorbents, J Agric Food Chem 2012;60:4026-33.
Guan W, Li C, Liu X, Zhou S, Ma Y. Graphene as dispersive solid phase extraction materials for pesticides LC-MS/MS multi-residue analysis in leek, onion and garlic, J Food Addit.Contam Part A. 2014;31:250-61.
Zhang M, Ma G, Zhang L, Chen H, Zhu L, Wang C, Liu X. Chitosan-reduced graphene oxide composites with 3D structures as effective reverse dispersed solid phase extraction adsorbents for pesticides analysis, Analyst 2019;144:5164-71.
Zhao P, Wang L, Zhou L, Zhang F, Kang S, Pan C. Multi-walled carbon nanotubes as alternative reversed-dispersive solid phase extraction materials in pesticide multi-residue analysis with QuEChERS method, J Chromatogr A. 2012;1225:17-25.
Khosrowshahi EM, Farajzadeh MA, Tuzen M, Mogaddam MRA, Nemati M. Application of magnetic carbon nano-onions in dispersive solid-phase extraction combined with DLLME for extraction of pesticide residues from water and vegetable samples, Anal Methods. 2021;13:3592-604.
Pech D, Brunet M, Durou H, Huang PH, Mochalin V, Gogotsi Y. Ultrahigh-power micrometer-sized supercapacitors based on onion-like carbon Nat. Nanotechnol. 2010;5:651-4.
Breczko J, Plonska-Brzezinska ME, Echegoyen L. Electrochemical oxidation and determination of dopamine in the presence of uric and ascorbic acids using a carbon nano-onion and poly(diallyldimethylammonium chloride) composite, Electrochim Acta. 2012;72:61-7.
Farajzadeh MA, Mohebbi A, Fouladvand H, Afshar Mogaddam MR A new and facile method for preparation of amorphous carbon nanoparticles and their application as an efficient and cheap sorbent for the extraction of some pesticides from fruit juices. Microchem J 2020;155:104795.
Park J, Kim YJ, Na YC. A modified quick, easy, cheap, effective, rugged, and safe method for determination of by-products originating from ozonation of chlorpyrifos and diazinon spiked in cherry tomato and perilla leaf. J Sep Sci 2020;45:422-31.
Ye X, Ye B, Xu J, Fang M, Dong D, Wu C, Lin X, Hu Y, Cao X, Mo W. A modified quick, easy, cheap, effective, rugged, and safe method with hydrophobic natural deep eutectic solvent as extractant and analyte protectant for analyzing pyrethroid residues in tomatoes. J Sep Sci 2020;43:3546-54.
Mongwe TH, Matsoso BJB, Mutuma K., Coville NJ, Maubane MS. Synthesis of chain-like carbon nano-onions by a flame assisted pyrolysis technique using different collecting plates, Diam Relat Mater. 2018;90:135-43.
https://www.ich.org/page/multidisciplinary-guidelines Accessed July 6, 2022
Ibrahim WAW, Farhani H, Sanagi MM, Aboul-Enein HY. Solid phase microextraction using new sol-gel hybrid polydimethylsiloxane-2-hydroxymethyl-18-crown-6-coated fiber for determination of organophosphorus pesticides, J Chromatogr A. 2010;1217:4890-7.
Marzi Khosrowshahi E, Ghalkhani M, Afshar Mogaddam MR, Farajzadeh MA, Sohouli E, Nemati M. Evaluation of MXene as an adsorbent in dispersive solid phase extraction of several pesticides from fresh fruit juices prior to their determination by HPLC-MS/MS. Food Chem. 2022;386:132773.
Farajzadeh MA, Afshar Mogaddam MR. Acid-base reaction-based dispersive liquid-liquid microextraction method for extraction of three classes of pesticides from fruit juice samples, J Chromatogr A. 2016;1431:8-16.
Abolghasemi MM, Piryaei M, Imani RM. Deep eutectic solvents as extraction phase in headspace single-drop microextraction for determination of pesticides in fruit juice and vegetable samples, Microchem J 2020;158:105041.