A combined qualitative and quantitative method development and validation of vancomycin hydrochloride injection formulation by HPLC and UV involving quality by design.
DoE
QbD
analytical method
validation
vancomycin HCl
Journal
Biomedical chromatography : BMC
ISSN: 1099-0801
Titre abrégé: Biomed Chromatogr
Pays: England
ID NLM: 8610241
Informations de publication
Date de publication:
Mar 2023
Mar 2023
Historique:
revised:
25
11
2022
received:
02
11
2022
accepted:
07
12
2022
pubmed:
16
12
2022
medline:
15
2
2023
entrez:
15
12
2022
Statut:
ppublish
Résumé
A selective, specific, precise, linear, accurate and robust analytical method was developed and validated for the assay of vancomycin HCl in vancomycin hydrochloride injection. Comparative UV spectrophotometric and reverse-phase HPLC were used to develop the quantitative determination. Acetonitrile and pH 2.2 phosphate buffer in the ratio 20:80 v/v were used as the mobile phase, and a flow rate of 1.0 ml/min with a 20 min run time. The detection was carried out at 235 nm with a Nucleosil C
Substances chimiques
Vancomycin
6Q205EH1VU
Types de publication
Journal Article
Langues
eng
Sous-ensembles de citation
IM
Pagination
e5568Subventions
Organisme : University Hyderabad, India
Informations de copyright
© 2022 John Wiley & Sons Ltd.
Références
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