Designing of ZnO nanoparticles oriented interface imprinted electrochemical sensor for fluoxetine detection.

Electrochemical determination Fluoxetine Interface imprinting Molecularly imprinted polymer Photopolymerization

Journal

Bioelectrochemistry (Amsterdam, Netherlands)
ISSN: 1878-562X
Titre abrégé: Bioelectrochemistry
Pays: Netherlands
ID NLM: 100953583

Informations de publication

Date de publication:
Aug 2023
Historique:
received: 27 12 2022
revised: 03 03 2023
accepted: 05 03 2023
medline: 5 6 2023
pubmed: 17 3 2023
entrez: 16 3 2023
Statut: ppublish

Résumé

This study represents nanoparticle-based well-oriented recognition sites via interface imprinting, followed by selective and sensitive determination of fluoxetine (FLX). Herein, FLX was firstly immobilized onto ZnO NPs, and then polymerization was carried out with MAPA, HEMA, and EGDMA on the glassy carbon electrode via photopolymerization. After the etching of ZnO with and 10 mM HCI solution, a porous structure with recognition sites for FLX was constructed onto surface. The characterization of the electrochemical sensor was accomplished by utilizing CV, EIS, ATR-FTIR AFM, and SEM analysis. The DPV was used to determine FLX in standard solution, serum sample, and tap water. The effect of FLX concentration variation was studied using the DPV in the range of 1.0 × 10

Identifiants

pubmed: 36924575
pii: S1567-5394(23)00048-8
doi: 10.1016/j.bioelechem.2023.108411
pii:
doi:

Substances chimiques

Fluoxetine 01K63SUP8D
Zinc Oxide SOI2LOH54Z
Polymers 0
Water 059QF0KO0R

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

108411

Informations de copyright

Copyright © 2023 Elsevier B.V. All rights reserved.

Déclaration de conflit d'intérêts

Declaration of Competing Interest The authors declare that they have no known competing financial interests or personal relationships that could have appeared to influence the work reported in this paper.

Auteurs

M Emin Çorman (M)

Ankara University, Faculty of Pharmacy, Department of Analytical Chemistry, Ankara, Turkey; University of Health Sciences, Gülhane Faculty of Pharmacy, Department of Biochemistry, Ankara, Turkey. Electronic address: mehmetemin.corman@sbu.edu.tr.

Ahmet Cetinkaya (A)

Ankara University, Faculty of Pharmacy, Department of Analytical Chemistry, Ankara, Turkey; Ankara University, Graduate School of Health Sciences, Ankara, Turkey.

Canan Armutcu (C)

Hacettepe University, Faculty of Science, Department of Chemistry, Ankara, Turkey.

Lokman Uzun (L)

Hacettepe University, Faculty of Science, Department of Chemistry, Ankara, Turkey.

Sibel A Ozkan (SA)

Ankara University, Faculty of Pharmacy, Department of Analytical Chemistry, Ankara, Turkey.

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Classifications MeSH