Fucose Binding Motifs on Mucin Core Glycopeptides Impact Bacterial Lectin Recognition.


Journal

Angewandte Chemie (International ed. in English)
ISSN: 1521-3773
Titre abrégé: Angew Chem Int Ed Engl
Pays: Germany
ID NLM: 0370543

Informations de publication

Date de publication:
07 08 2023
Historique:
received: 16 02 2023
medline: 3 8 2023
pubmed: 18 4 2023
entrez: 17 4 2023
Statut: ppublish

Résumé

Mucin glycoproteins are essential components of the mucosal barrier, which protects the host from pathogens. Throughout evolution, bacteria have developed strategies to modulate and penetrate this barrier, and cause virulence by interacting with mucin O-glycans at the epithelial cell-surface. O-fucosylated glycan epitopes on mucins are key ligands of many bacterial lectins. Here, a chemoenzymatic synthesis strategy is described to prepare a library of fucosylated mucin core glycopeptides to enable studies of mucin-interacting and fucose-binding bacterial lectins. Glycan cores with biologically important Lewis and H-antigens were prepared decorating the peptide backbone at different sites and densities. The fucosylated mucin glycopeptides were applied in microarray binding studies to explore the importance of glycan core and peptide backbone presentation of these antigens in binding interactions with the P. aeruginosa lectin LecB and the C. difficile toxin A.

Identifiants

pubmed: 37067376
doi: 10.1002/anie.202302437
doi:

Substances chimiques

Mucins 0
Lectins 0
Fucose 28RYY2IV3F
Glycopeptides 0
Polysaccharides 0

Types de publication

Journal Article Research Support, Non-U.S. Gov't

Langues

eng

Sous-ensembles de citation

IM

Pagination

e202302437

Informations de copyright

© 2023 The Authors. Angewandte Chemie International Edition published by Wiley-VCH GmbH.

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Auteurs

Sandra Behren (S)

Department of Chemistry, Umeå University, 90187, Umeå, Sweden.
Leibniz-Institut für Analytische Wissenschaften - ISAS - e.V., 44227, Dortmund, Germany.

Jin Yu (J)

Leibniz-Institut für Analytische Wissenschaften - ISAS - e.V., 44227, Dortmund, Germany.
Glycosciences Laboratory, Imperial College London, London, W12 0NN, UK.

Christian Pett (C)

Department of Chemistry, Umeå University, 90187, Umeå, Sweden.
Leibniz-Institut für Analytische Wissenschaften - ISAS - e.V., 44227, Dortmund, Germany.

Manuel Schorlemer (M)

Department of Chemistry, Umeå University, 90187, Umeå, Sweden.
Leibniz-Institut für Analytische Wissenschaften - ISAS - e.V., 44227, Dortmund, Germany.

Viktoria Heine (V)

Laboratory for Biomaterials, Institute of Biotechnology and Helmholtz-Institute for Biomedical Engineering, RWTH Aachen University, Pauwelsstraße 20, 52074, Aachen, Germany.

Thomas Fischöder (T)

Laboratory for Biomaterials, Institute of Biotechnology and Helmholtz-Institute for Biomedical Engineering, RWTH Aachen University, Pauwelsstraße 20, 52074, Aachen, Germany.

Lothar Elling (L)

Laboratory for Biomaterials, Institute of Biotechnology and Helmholtz-Institute for Biomedical Engineering, RWTH Aachen University, Pauwelsstraße 20, 52074, Aachen, Germany.

Ulrika Westerlind (U)

Department of Chemistry, Umeå University, 90187, Umeå, Sweden.
Leibniz-Institut für Analytische Wissenschaften - ISAS - e.V., 44227, Dortmund, Germany.

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