Analysis of Patulin in Apple Products Marketed in Belgium: Intra-Laboratory Validation Study and Occurrence.
Belgium
apple
juices
mycotoxins
patulin
puree
Journal
Toxins
ISSN: 2072-6651
Titre abrégé: Toxins (Basel)
Pays: Switzerland
ID NLM: 101530765
Informations de publication
Date de publication:
30 05 2023
30 05 2023
Historique:
received:
14
04
2023
revised:
23
05
2023
accepted:
25
05
2023
medline:
29
6
2023
pubmed:
27
6
2023
entrez:
27
6
2023
Statut:
epublish
Résumé
Apple and apple derivatives (e.g., juices, puree) are the most important foodstuffs contaminated with patulin (PAT) in the human diet. To routinely monitor these foodstuffs and ensure that the PAT levels are below the maximum permitted levels, a method using liquid chromatography combined with tandem mass spectrometry (LC-MS/MS) has been developed. Afterwards, the method was successfully validated, reaching quantification limits of 1.2 μg/L for apple juice and cider, and 2.1 μg/kg for puree. Recovery experiments were performed with samples fortified with PAT in the range of 25-75 μg/L for juice/cider and 25-75 μg/kg for puree. The results show overall average recovery rates of 85% (RSD
Identifiants
pubmed: 37368669
pii: toxins15060368
doi: 10.3390/toxins15060368
pmc: PMC10302775
pii:
doi:
Substances chimiques
Patulin
95X2BV4W8R
Types de publication
Journal Article
Langues
eng
Sous-ensembles de citation
IM
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