Sensitive spectrofluorimetric determination of the prokinetic drug prucalopride succinate based on supramolecular aggregation approach with evaluation of method greenness: application to content uniformity test.
content uniformity testing
method greenness
prokinetic drug
spectrofluorimetry
supramolecular aggregation
Journal
Luminescence : the journal of biological and chemical luminescence
ISSN: 1522-7243
Titre abrégé: Luminescence
Pays: England
ID NLM: 100889025
Informations de publication
Date de publication:
Dec 2023
Dec 2023
Historique:
revised:
24
08
2023
received:
29
07
2023
accepted:
18
09
2023
medline:
5
12
2023
pubmed:
23
9
2023
entrez:
23
9
2023
Statut:
ppublish
Résumé
The prokinetic drug, prucalopride (PCP) succinate, was determined using a new spectrofluorimetric approach with a highly sensitive, rapid, and simple procedure. The method exploited the enhancement of the inherent native fluorescence of PCP by micellar aggregation with sodium lauryl sulfate (SLS) as an anionic surfactant. Different factors that could affect the fluorescence intensity were carefully studied in order to achieve the maximal fluorescence signal. Measurement of the enhanced fluorescence was done at 354 nm after the excitation at 276 nm. The fluorescence intensity-concentration plot was rectilinear in the concentration range of 50-600 ng/ml with detection and quantitation limits of 13.9 and 42.1 ng/ml, respectively. The method underwent validation according to the International Council for Harmonisation criteria in order to assess its analytical performance, and promising results were achieved that proved the validity and reliability of the method. Furthermore, the method was employed effectively for the analysis of the cited drug in commercial pharmaceutical tablets.
Substances chimiques
prucalopride
0A09IUW5TP
Succinates
0
Tablets
0
Types de publication
Journal Article
Langues
eng
Sous-ensembles de citation
IM
Pagination
2065-2072Informations de copyright
© 2023 John Wiley & Sons Ltd.
Références
S. S. Bharate, Drug Discovery Today 2021, 26, 384.
G. Bassotti, D. Gambaccini, M. Bellini, Expert Rev. Gastroent. Hepatol 2016, 10, 291.
V. N. Akhani, K. Patel, K. Patel, L. Prajapati, C. Patel, World J. Pharm. Res. 2020, 9, 1568.
G. Bojja, M. A. Mukthinuthalapati, Acta Sci. Pharm. Sci. 2020, 4, 78.
D. Venkateswarlu, I. E. Chakravarthy, J. Emerg. Technol. Innov. Res. 2019, 6, 743.
G. Bojja, M. A. Mukthinuthalapati, Acta Sci. Pharm. Sci. 2020, 4, 74.
A. Bhosale, V. Bhagat, V. Kunjir, D. Kardile, R. Shete, Res. J. Pharm. Technol. 2021, 14, 4189.
M. S. Elshahed, S. S. Toubar, A. A. Ashour, R. T. El-Eryan, BMC Chem. 2022, 16, 1.
M. T. Saad, H. E. Zaazaa, T. A. Fattah, S. A. Boltia, J. Fluoresc. 2023, 33, 1609.
I. M. Nour, A. R. Mohamed, M. A. Hasan, M. Badrawy, Spectrochim. Acta A 2023, 296, 122715.
B. I. Salman, BMC Chem. 2023, 17, 83.
Z. Sun, L. Zuo, J. Kang, L. Zhou, M. Jia, Z. Li, Z. Yang, X. Zhang, Z. Zhu, J. Chromatogr., B 2016, 1033-1034, 328.
S. Kanthale, S. Thonte, S. Pekamwar, D. Mahapatra, Int. J. Pharm. Sci. Drug Res. 2020, 12, 166.
C. Sreedhar, K. Manogna, H. Akkamma, B. J. K. Boruah, J. Pharm. Sci. 2021, 11, 39.
B. S. Mahamuni, A. Jajula, A. Awasthi, P. D. Kalariya, M. K. Talluri, J. Pharm. Biomed. Anal. 2016, 125, 219.
R. T. Eleryan, M. Salem, R. Tony, Egyptian J. Chem. 2023, 66, 15.
M. S. Elshahed, S. S. Toubar, A. A. Ashour, R. T. El-Eryan, Measurement 2022, 204, 112071.
N. N. Atia, A. M. Mahmoud, S. R. El-Shabouri, W. M. El-Koussi, Int. J. Anal. Chem. 2013, 2013, 1.
A. M. El-Kosasy, L. A. Hussein, N. G. Sedki, N. N. Salama, Spectrochim. Acta A 2016, 153, 422.
J. L. Vilchez, J. Taoufiki, O. Ballesteros, A. Navalon, Microchim. Acta 2005, 150, 247.
D. A. Nour-Eldeen, M. A. Omar, S. K. Mohamed, A. A. Mohamed, Luminescence 2022, 37, 1057.
J. A. Ocana, F. J. Barragan, M. Callejon, J. Pharm. Biomed. Anal. 2005, 37, 327.
M. Pesez, J. Bartos, Colorimetric and Fluorimetric Analysis of Organic Compounds and Drugs, Marcel Dekker, Madison Avenue, New York 1974.
M. Rockville, The United States Pharmacopoeia 30, the National Formulary 25 US Pharmacopeial Convention, electronic version, 2007.
A. J. Valente, H. D. Burrows, R. F. Pereira, A. C. Ribeiro, J. L. Costa Pereira, V. M. Lobo, Langmuir 2006, 22, 5625.
A. C. S. Neves, A. Valente, H. Burrows, A. Ribeiro, V. Lobo, J. Colloid Interface Sci. 2007, 306, 166.
Validation of analytical procedures: methodology International Conference on Harmonization (ICH) of Technical Requirements for the Registration Pharmaceuticals for Human Use Geneva, 1996. https://www.ema.europa.eu/documents/scientific-guideline/ich-guideline-q2r2-validation-analytical-procedures-step-2b_en.pdf (accessed: October 2023).
A. Gałuszka, Z. M. Migaszewski, P. Konieczka, J. Namieśnik, TrAC, Trends Anal. Chem. 2012, 37, 61.
F. Pena-Pereira, W. Wojnowski, M. Tobiszewski, Anal. Chem. 2020, 92, 10076.