Cu-Catalyzed Oxidative 3-Amination of Indoles via Formation of Indolyl(aryl)iodonium Imides Using

Cu catalyst C–N coupling reaction hypervalent iodine indole o-substituted iodoarene one-pot reaction regioselectivity

Journal

Molecules (Basel, Switzerland)
ISSN: 1420-3049
Titre abrégé: Molecules
Pays: Switzerland
ID NLM: 100964009

Informations de publication

Date de publication:
22 Mar 2019
Historique:
received: 27 02 2019
revised: 14 03 2019
accepted: 21 03 2019
entrez: 27 3 2019
pubmed: 27 3 2019
medline: 16 7 2019
Statut: epublish

Résumé

An oxidative 3-amination of indole derivatives using hypervalent iodine(III) and bissulfonimides, which proceeds via the formation of indolyl(aryl)iodonium imides, was developed. This reaction was followed by an indole-selective copper-catalyzed oxidative C⁻N coupling reaction to obtain 3-amino indole derivatives as single regioisomers.

Identifiants

pubmed: 30909483
pii: molecules24061147
doi: 10.3390/molecules24061147
pmc: PMC6471596
pii:
doi:

Substances chimiques

Imides 0
Indoles 0
Solvents 0
Copper 789U1901C5
Iodine 9679TC07X4

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Références

J Med Chem. 2001 Mar 15;44(6):949-60
pubmed: 11300877
Bioorg Med Chem. 2003 Nov 17;11(23):5293-9
pubmed: 14604693
Bioorg Med Chem. 2007 May 1;15(9):3248-65
pubmed: 17339113
J Med Chem. 2008 Mar 13;51(5):1464-8
pubmed: 18260616
Org Biomol Chem. 2010 Mar 7;8(5):1149-53
pubmed: 20165807
Bioorg Med Chem Lett. 2011 Jan 1;21(1):346-9
pubmed: 21134749
J Am Chem Soc. 2012 Sep 19;134(37):15436-42
pubmed: 22913396
J Am Chem Soc. 2014 May 14;136(19):6920-8
pubmed: 24739120
Chem Commun (Camb). 2015 Feb 11;51(12):2273-6
pubmed: 25556519
Org Biomol Chem. 2016 Mar 21;14(11):3027-30
pubmed: 26911555
Chem Asian J. 2016 Dec 19;11(24):3583-3588
pubmed: 27879062
Org Lett. 2017 Mar 17;19(6):1314-1317
pubmed: 28281340
Chem Commun (Camb). 2018 Apr 24;54(34):4258-4261
pubmed: 29457182
J Org Chem. 2018 Dec 7;83(23):14827-14833
pubmed: 30371085

Auteurs

Kazuhiro Watanabe (K)

Department of Chemistry, Graduate School of Science, and Molecular Chirality Research Center, Chiba University, 1-33 Yayoi-cho, Inage-ku, Chiba 263-8522, Japan. cars9s66@chiba-u.jp.

Katsuhiko Moriyama (K)

Department of Chemistry, Graduate School of Science, and Molecular Chirality Research Center, Chiba University, 1-33 Yayoi-cho, Inage-ku, Chiba 263-8522, Japan. moriyama@faculty.chiba-u.jp.

Articles similaires

A molecular mechanism for bright color variation in parrots.

Roberto Arbore, Soraia Barbosa, Jindich Brejcha et al.
1.00
Animals Feathers Pigmentation Parrots Aldehyde Dehydrogenase
Osteosarcoma Animals Glutathione Oxidation-Reduction Mice
Perylene Dopamine Electrochemical Techniques Imides Luminescent Measurements
Peroxynitrous Acid Animals Escherichia coli Immunotherapy Mice

Classifications MeSH