Trace determination of parabens in cosmetics and personal care products using fabric-phase sorptive extraction and high-performance liquid chromatography with UV detection.
cosmetics
fabric-phase sorptive extraction
parabens
personal care products
sample preparation
Journal
Journal of separation science
ISSN: 1615-9314
Titre abrégé: J Sep Sci
Pays: Germany
ID NLM: 101088554
Informations de publication
Date de publication:
Jul 2020
Jul 2020
Historique:
received:
22
09
2019
revised:
29
03
2020
accepted:
30
03
2020
pubmed:
8
4
2020
medline:
1
4
2021
entrez:
8
4
2020
Statut:
ppublish
Résumé
A simple, fast, and sensitive analytical protocol using fabric-phase sorptive extraction followed by high performance liquid chromatography with ultraviolet detection has been developed and validated for the extraction of five parabens including methylparaben, ethylparaben, propylparaben, butylparaben, and benzylparaben. In the present work, sol-gel polyethylene glycol coated fabric-phase sorptive extraction membrane is used for the preconcentration of parabens (polar) from complex matrices. The use of fabric-phase sorptive extraction membrane provides a high surface area which offers high sorbent loading, shortened equilibrium time, and overall decrease in the sample preparation time. Various factors affecting the performance of fabric-phase sorptive extraction, including extraction time, eluting solvent, elution time, and pH of the sample matrix, were optimized. Separation was performed using a mobile phase consisting of water:acetonitrile (63:37; v/v) at an isocratic elution mode at a flow rate of 0.9 mL/min with wavelength at 254 nm. The calibration curves of the target analytes were prepared with good correlation coefficient values (r
Identifiants
pubmed: 32259348
doi: 10.1002/jssc.201900978
doi:
Substances chimiques
Cosmetics
0
Parabens
0
Types de publication
Journal Article
Langues
eng
Sous-ensembles de citation
IM
Pagination
2626-2635Subventions
Organisme : University Grant Commission (UGC), New Delhi, India
Informations de copyright
© 2020 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.
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