Regulating the pH of bicarbonate solutions without purging gases: Application to dissolution testing of enteric coated tablets, pellets and microparticles.


Journal

International journal of pharmaceutics
ISSN: 1873-3476
Titre abrégé: Int J Pharm
Pays: Netherlands
ID NLM: 7804127

Informations de publication

Date de publication:
30 Jul 2020
Historique:
received: 06 04 2020
revised: 14 06 2020
accepted: 15 06 2020
pubmed: 23 6 2020
medline: 4 3 2021
entrez: 23 6 2020
Statut: ppublish

Résumé

Dissolution media based on bicarbonate buffers closely mimic the environment of intestinal fluids and thus improve in vitro in vivo correlation compared to phosphate buffers. Purging gases into the medium is used as a method to stabilise bicarbonate buffers; however, this causes issues due to the disturbance of the hydrodynamics in the dissolution vessel. The aim of this study was to develop a novel system to regulate and stabilise the pH of bicarbonate buffers without purging gases for the application of dissolution testing of enteric coated products. A novel enclosure system was applied to the USP II dissolution vessel to supply N

Identifiants

pubmed: 32565282
pii: S0378-5173(20)30546-9
doi: 10.1016/j.ijpharm.2020.119562
pii:
doi:

Substances chimiques

Bicarbonates 0
Buffers 0
Gases 0
Tablets, Enteric-Coated 0

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

119562

Informations de copyright

Copyright © 2020 Elsevier B.V. All rights reserved.

Déclaration de conflit d'intérêts

Declaration of Competing Interest The authors declare that they have no known competing financial interests or personal relationships that could have appeared to influence the work reported in this paper.

Auteurs

Nathan Scott (N)

Department of Clinical and Pharmaceutical Sciences, University of Hertfordshire, Hatfield AL10 9AB, United Kingdom.

Kavil Patel (K)

Department of Clinical and Pharmaceutical Sciences, University of Hertfordshire, Hatfield AL10 9AB, United Kingdom.

Tariro Sithole (T)

Department of Clinical and Pharmaceutical Sciences, University of Hertfordshire, Hatfield AL10 9AB, United Kingdom.

Konstantina Xenofontos (K)

Department of Clinical and Pharmaceutical Sciences, University of Hertfordshire, Hatfield AL10 9AB, United Kingdom.

Valentyn Mohylyuk (V)

Department of Clinical and Pharmaceutical Sciences, University of Hertfordshire, Hatfield AL10 9AB, United Kingdom.

Fang Liu (F)

Department of Clinical and Pharmaceutical Sciences, University of Hertfordshire, Hatfield AL10 9AB, United Kingdom; Fluid Pharma Ltd, Nexus, Discovery Way, Leeds LS2 3AA, United Kingdom. Electronic address: f.liu3@herts.ac.uk.

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Classifications MeSH