Total Synthesis of the Proposed Structure for Protoaculeine B, a Polycationic Marine Sponge Metabolite, with a Homogeneous Long-Chain Polyamine.

Animals Indoles / chemical synthesis Magnetic Resonance Spectroscopy Mass Spectrometry Molecular Structure Polyamines / chemical synthesis Porifera / chemistry Stereoisomerism

Journal

Journal of natural products
ISSN: 1520-6025
Titre abrégé: J Nat Prod
Pays: United States
ID NLM: 7906882

Informations de publication

Date de publication:
25 09 2020
Historique:
pubmed: 2 9 2020
medline: 2 9 2021
entrez: 2 9 2020
Statut: ppublish

Résumé

By establishing the procedures for sequential deprotections, reaction monitoring, purification, and handling, for the first time, we achieved the total synthesis of the proposed structure for protoaculeine B (

Identifiants

DOI: 10.1021/acs.jnatprod.0c00761 PMID: 32869997
pubmed: 32869997
doi: 10.1021/acs.jnatprod.0c00761
doi:

Substances chimiques

Indoles 0
Polyamines 0
protoaculeine B 0

Types de publication

Journal Article Research Support, Non-U.S. Gov't

Langues

eng

Sous-ensembles de citation

IM

Pagination

2769-2775

Auteurs

Raku Irie (R)

Yokohama City University, Seto 22-2, Kanazawa-ku, Yokohama 236-0027, Japan.
ORCID: 0000-0002-8877-4179

Masayoshi Miyahara (M)

Yokohama City University, Seto 22-2, Kanazawa-ku, Yokohama 236-0027, Japan.

Shota Nakamura (S)

Yokohama City University, Seto 22-2, Kanazawa-ku, Yokohama 236-0027, Japan.

Akito Honda (A)

Faculty of Fisheries Sciences, Hokkaido University, Hakodate 041-8611, Japan.

Ryuichi Sakai (R)

Faculty of Fisheries Sciences, Hokkaido University, Hakodate 041-8611, Japan.
ORCID: 0000-0001-6490-0495

Masato Oikawa (M)

Yokohama City University, Seto 22-2, Kanazawa-ku, Yokohama 236-0027, Japan.
ORCID: 0000-0002-3919-811X

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Classifications MeSH

questionsmedicales.fr › Eucaryotes › Animaux › Total Synthesis of the Proposed Structure for...
questionsmedicales.fr › Composés hétérocycliques › Composés hétérocycliques à cycles fusionnés › Composés hétérobicycliques › Indoles › Total Synthesis of the Proposed Structure for...
questionsmedicales.fr › Techniques d'investigation › Techniques de chimie analytique › Analyse spectrale › Spectroscopie par résonance magnétique › Total Synthesis of the Proposed Structure for...
questionsmedicales.fr › Techniques d'investigation › Techniques de chimie analytique › Spectrométrie de masse › Total Synthesis of the Proposed Structure for...
questionsmedicales.fr › Phénomènes chimiques › Structure moléculaire › Total Synthesis of the Proposed Structure for...
questionsmedicales.fr › Composés chimiques organiques › Amines › Polyamines › Total Synthesis of the Proposed Structure for...
questionsmedicales.fr › Eucaryotes › Animaux › Invertébrés › Porifera › Total Synthesis of the Proposed Structure for...
questionsmedicales.fr › Phénomènes chimiques › Phénomènes de chimie organique › Isomérie › Stéréoisomérie › Total Synthesis of the Proposed Structure for...