Slow lactate gluconate exchange in calcium complexes during precipitation from supersaturated aqueous solutions.

Calcium hydroxycarboxylates Kinetic modelling Supersaturation

Journal

Food research international (Ottawa, Ont.)
ISSN: 1873-7145
Titre abrégé: Food Res Int
Pays: Canada
ID NLM: 9210143

Informations de publication

Date de publication:
11 2020
Historique:
received: 25 05 2020
revised: 22 06 2020
accepted: 09 07 2020
entrez: 25 11 2020
pubmed: 26 11 2020
medline: 11 5 2021
Statut: ppublish

Résumé

Saturated solutions of calcium l-lactate in water or in deuterium oxide continuously dissolve calcium l-lactate by addition of solid sodium d-gluconate and become strongly supersaturated in calcium d-gluconate due to no or slow precipitation. The quantification of total dissolved calcium allied with the calcium complexes equilibrium constants allowed an ion speciation, which shows an initial non-thermal and spontaneous supersaturation of more than a factor of 50 at 25 °C only slowly decreasing after initiation of precipitation of calcium d-gluconate after a lag phase of several hours. A mathematical model is proposed, based on numerical solution of coupled differential equations of dynamics of l-lactate and d-gluconate exchange during the lag phase for precipitation and during precipitation. A slow exchange of l-lactate coordinated to calcium with d-gluconate is indicated with a time constant of 0.20 h

Identifiants

pubmed: 33233167
pii: S0963-9969(20)30564-0
doi: 10.1016/j.foodres.2020.109539
pii:
doi:

Substances chimiques

Gluconates 0
Water 059QF0KO0R
Lactic Acid 33X04XA5AT
gluconic acid R4R8J0Q44B
Calcium SY7Q814VUP

Types de publication

Journal Article Research Support, Non-U.S. Gov't

Langues

eng

Sous-ensembles de citation

IM

Pagination

109539

Informations de copyright

Copyright © 2020 Elsevier Ltd. All rights reserved.

Auteurs

André C Garcia (AC)

Department of Food Science, University of Copenhagen, Rolighedsvej 30, DK-1958 Frederiksberg C, Denmark; Instituto Federal de Educação, Ciência e Tecnologia de São Paulo, Campus Capivari. Avenida Doutor Ênio Pires de Camargo, 2971, São João Batista, CEP: 13360-000 Capivari, SP, Brazil.

Jesper S Hansen (JS)

IMFUFA, Department of Science and Environment, Roskilde University, Universitetsvej 1, DK-4000 Roskilde, Denmark.

Nicholas Bailey (N)

IMFUFA, Department of Science and Environment, Roskilde University, Universitetsvej 1, DK-4000 Roskilde, Denmark.

Leif H Skibsted (LH)

Department of Food Science, University of Copenhagen, Rolighedsvej 30, DK-1958 Frederiksberg C, Denmark. Electronic address: ls@food.ku.dk.

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Classifications MeSH