Enhanced Concanavalin A Binding to Preorganized Mannose Nanoarrays in Glycodendrimersomes Revealed Multivalent Interactions.


Journal

Angewandte Chemie (International ed. in English)
ISSN: 1521-3773
Titre abrégé: Angew Chem Int Ed Engl
Pays: Germany
ID NLM: 0370543

Informations de publication

Date de publication:
06 04 2021
Historique:
received: 17 01 2021
pubmed: 26 1 2021
medline: 23 7 2021
entrez: 25 1 2021
Statut: ppublish

Résumé

The effect of the two-dimensional glycan display on glycan-lectin recognition remains poorly understood despite the importance of these interactions in a plethora of cellular processes, in (patho)physiology, as well as its potential for advanced therapeutics. Faced with this challenge we utilized glycodendrimersomes, a type of synthetic vesicles whose membrane mimics the surface of a cell and offers a means to probe the carbohydrate biological activity. These single-component vesicles were formed by the self-assembly of sequence-defined mannose-Janus dendrimers, which serve as surrogates for glycolipids. Using atomic force microscopy and molecular modeling we demonstrated that even mannose, a monosaccharide, was capable of organizing the sugar moieties into periodic nanoarrays without the need of the formation of liquid-ordered phases as assumed necessary for rafts. Kinetics studies of Concanavalin A binding revealed that those nanoarrays resulted in a new effective ligand yielding a ten-fold increase in the kinetic and thermodynamic constant of association.

Identifiants

pubmed: 33493389
doi: 10.1002/anie.202100400
pmc: PMC8048596
doi:

Substances chimiques

Dendrimers 0
Concanavalin A 11028-71-0
Mannose PHA4727WTP

Types de publication

Journal Article Research Support, Non-U.S. Gov't Research Support, U.S. Gov't, Non-P.H.S.

Langues

eng

Sous-ensembles de citation

IM

Pagination

8352-8360

Informations de copyright

© 2021 The Authors. Angewandte Chemie International Edition published by Wiley-VCH GmbH.

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Auteurs

Nina Yu Kostina (N)

DWI- Leibniz Institute for Interactive Materials, Institute of Technical and Macromolecular Chemistry RWTH Aachen University, Forckenbeckstraße 50, 52074, Aachen, Germany.

Dominik Söder (D)

DWI- Leibniz Institute for Interactive Materials, Institute of Technical and Macromolecular Chemistry RWTH Aachen University, Forckenbeckstraße 50, 52074, Aachen, Germany.

Tamás Haraszti (T)

DWI- Leibniz Institute for Interactive Materials, Institute of Technical and Macromolecular Chemistry RWTH Aachen University, Forckenbeckstraße 50, 52074, Aachen, Germany.

Qi Xiao (Q)

Roy & Diana Vagelos Laboratories, Department of Chemistry, University of Pennsylvania, Philadelphia, PA, 19104-6323, USA.
Institute of Computational Molecular Science, Temple University, Philadelphia, PA, 19122, USA.

Khosrow Rahimi (K)

DWI- Leibniz Institute for Interactive Materials, Institute of Technical and Macromolecular Chemistry RWTH Aachen University, Forckenbeckstraße 50, 52074, Aachen, Germany.

Benjamin E Partridge (BE)

Roy & Diana Vagelos Laboratories, Department of Chemistry, University of Pennsylvania, Philadelphia, PA, 19104-6323, USA.

Michael L Klein (ML)

Institute of Computational Molecular Science, Temple University, Philadelphia, PA, 19122, USA.

Virgil Percec (V)

Roy & Diana Vagelos Laboratories, Department of Chemistry, University of Pennsylvania, Philadelphia, PA, 19104-6323, USA.

Cesar Rodriguez-Emmenegger (C)

DWI- Leibniz Institute for Interactive Materials, Institute of Technical and Macromolecular Chemistry RWTH Aachen University, Forckenbeckstraße 50, 52074, Aachen, Germany.

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Classifications MeSH