One-step purification/extraction method to access glyphosate, glufosinate, and their metabolites in natural waters.
3-(methyl phosphinico)-propionic acid
Aminomethylphosphonic acid
Glufosinate
Glyphosate
Red River Delta
UPLC-MS/MS
Journal
Journal of chromatography. A
ISSN: 1873-3778
Titre abrégé: J Chromatogr A
Pays: Netherlands
ID NLM: 9318488
Informations de publication
Date de publication:
19 Jul 2021
19 Jul 2021
Historique:
received:
08
02
2021
revised:
15
04
2021
accepted:
18
04
2021
pubmed:
26
5
2021
medline:
16
6
2021
entrez:
25
5
2021
Statut:
ppublish
Résumé
A new green method for trace level quantification of four herbicides, glyphosate (GLYP), glufosinate (GLUF), and their main metabolites, aminomethylphosphonic acid (AMPA) and 3-(methyl-phosphinico)-propionic acid (MPPA), was developed. The purification step without any derivatization was conducted by solid-phase extraction using Chelex-100 resin in the Fe (III) form, followed by elution with 5% NH
Identifiants
pubmed: 34034108
pii: S0021-9673(21)00312-5
doi: 10.1016/j.chroma.2021.462188
pii:
doi:
Substances chimiques
Aminobutyrates
0
Herbicides
0
Organophosphonates
0
Water Pollutants, Chemical
0
phosphinothricin
51276-47-2
aminomethylphosphonic acid (AMPA)
90825O5C1U
Glycine
TE7660XO1C
Types de publication
Journal Article
Langues
eng
Sous-ensembles de citation
IM
Pagination
462188Informations de copyright
Copyright © 2021 Elsevier B.V. All rights reserved.
Déclaration de conflit d'intérêts
Declaration of Competing Interest The authors declare no competing financial interest.