Carbon fibers as green and sustainable sorbent for the extraction of isoflavones from environmental waters.

Carbon Fiber Chromatography, Liquid Isoflavones / analysis Solid Phase Extraction Tandem Mass Spectrometry Water Pollutants, Chemical / analysis
Carbon fibers Environmental analysis In-syringe dispersive solid phase extraction Isoflavones Phytoestrogens Surface waters

Journal

Talanta
ISSN: 1873-3573
Titre abrégé: Talanta
Pays: Netherlands
ID NLM: 2984816R

Informations de publication

Date de publication:
01 Oct 2021
Historique:
received: 19 04 2021
revised: 28 05 2021
accepted: 30 05 2021
entrez: 3 7 2021
pubmed: 4 7 2021
medline: 8 7 2021
Statut: ppublish

Résumé

Isoflavones are a group of phytoestrogens of important environmental concern due to their endocrine disrupting effects. This article presents a rapid, green, and sustainable method for determining four isoflavones (daidzein, genistein, formononetin, and biochanin A) in environmental waters complying with current trends in Analytical Chemistry. The method consists of in-syringe dispersive solid-phase extraction (DSPE) as the extraction approach, using carbon fibers as extraction material. The synthesis of carbon fibers is simple and sustainable, since it only requires a natural product such as raw cotton as precursor, which is thermally treated (600 °C for 30 min) in an inert (Ar) atmosphere to convert it into carbon fibers. After extraction, the final eluate is analyzed by liquid chromatography-tandem mass spectrometry (LC-MS/MS). The proposed methodology allows the determination of the four isoflavones in water samples at the ng L

Identifiants

DOI: 10.1016/j.talanta.2021.122582 PMID: 34215074
pubmed: 34215074
pii: S0039-9140(21)00503-8
doi: 10.1016/j.talanta.2021.122582
pii:
doi:

Substances chimiques

Carbon Fiber 0
Isoflavones 0
Water Pollutants, Chemical 0

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

122582

Informations de copyright

Copyright © 2021 Elsevier B.V. All rights reserved.

Auteurs

Juan L Benedé (JL)

Affordable and Sustainable Sample Preparation (AS2P) Research Group, Departamento de Química Analítica, Instituto Universitario de Investigación en Química Fina y Nanoquímica IUNAN, Universidad de Córdoba, Campus de Rabanales, Edificio Marie Curie (anexo), E-14071, Córdoba, Spain; GICAPC Research Group, Department of Analytical Chemistry, University of Valencia, 46100, Burjassot, Valencia, Spain. Electronic address: benede@uv.es.

Alberto Chisvert (A)

GICAPC Research Group, Department of Analytical Chemistry, University of Valencia, 46100, Burjassot, Valencia, Spain.

Rafael Lucena (R)

Affordable and Sustainable Sample Preparation (AS2P) Research Group, Departamento de Química Analítica, Instituto Universitario de Investigación en Química Fina y Nanoquímica IUNAN, Universidad de Córdoba, Campus de Rabanales, Edificio Marie Curie (anexo), E-14071, Córdoba, Spain.

Soledad Cárdenas (S)

Affordable and Sustainable Sample Preparation (AS2P) Research Group, Departamento de Química Analítica, Instituto Universitario de Investigación en Química Fina y Nanoquímica IUNAN, Universidad de Córdoba, Campus de Rabanales, Edificio Marie Curie (anexo), E-14071, Córdoba, Spain. Electronic address: scardenas@uco.es.

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Classifications MeSH

questionsmedicales.fr › Technologie, industrie et agriculture › Produits manufacturés › Matériaux biomédicaux et dentaires › Polymères › Fibre de carbone › Carbon fibers as green and sustainable sorbent...
questionsmedicales.fr › Techniques d'investigation › Techniques de chimie analytique › Chromatographie › Chromatographie en phase liquide › Carbon fibers as green and sustainable sorbent...
questionsmedicales.fr › Composés hétérocycliques › Composés hétérocycliques à cycles fusionnés › Composés hétérobicycliques › Benzopyranes › 4H-1-Benzopyran-4-ones › Flavonoïdes › Isoflavones › Carbon fibers as green and sustainable sorbent...
questionsmedicales.fr › Techniques d'investigation › Techniques de chimie analytique › Fractionnement chimique › Extraction en phase solide › Carbon fibers as green and sustainable sorbent...
questionsmedicales.fr › Techniques d'investigation › Techniques de chimie analytique › Spectrométrie de masse › Spectrométrie de masse en tandem › Carbon fibers as green and sustainable sorbent...
questionsmedicales.fr › Actions chimiques et utilisations › Actions toxiques › Polluants environnementaux › Polluants de l'eau › Polluants chimiques de l'eau › Carbon fibers as green and sustainable sorbent...