FFF-based high-throughput sequence shortlisting to support the development of aptamer-based analytical strategies.

Aptamer selectivity Aptamers Field-flow fractionation Lysozyme Screening method

Journal

Analytical and bioanalytical chemistry
ISSN: 1618-2650
Titre abrégé: Anal Bioanal Chem
Pays: Germany
ID NLM: 101134327

Informations de publication

Date de publication:
Jul 2022
Historique:
received: 11 12 2021
accepted: 08 02 2022
revised: 05 02 2022
pubmed: 20 2 2022
medline: 2 7 2022
entrez: 19 2 2022
Statut: ppublish

Résumé

Aptamers are biomimetic receptors that are increasingly exploited for the development of optical and electrochemical aptasensors. They are selected in vitro by the SELEX (Systematic Evolution of Ligands by Exponential Enrichment) procedure, but although they are promising recognition elements, for their reliable applicability for analytical purposes, one cannot ignore sample components that cause matrix effects. This particularly applies when different SELEX-selected aptamers and related truncated sequences are available for a certain target, and the choice of the aptamer should be driven by the specific downstream application. In this context, the present work aimed at investigating the potentialities of asymmetrical flow field-flow fractionation (AF4) with UV detection for the development of a screening method of a large number of anti-lysozyme aptamers towards lysozyme, including randomized sequences and an interfering agent (serum albumin). The possibility to work in native conditions and selectively monitor the evolution of untagged aptamer signal as a result of aptamer-protein binding makes the devised method effective as a strategy for shortlisting the most promising aptamers both in terms of affinity and in terms of selectivity, to support subsequent development of aptamer-based analytical devices.

Identifiants

pubmed: 35182166
doi: 10.1007/s00216-022-03971-2
pii: 10.1007/s00216-022-03971-2
pmc: PMC9242963
doi:

Substances chimiques

Aptamers, Nucleotide 0
Ligands 0

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

5519-5527

Subventions

Organisme : Ministero dell'Istruzione, dell'Università e della Ricerca
ID : PRIN 2017 (Progetti di Ricerca di Rilevante Intere

Informations de copyright

© 2022. The Author(s).

Références

Matthews CJ, Andrews ESV, Patrick WM. Enzyme-based amperometric biosensors for malic acid – a review. Anal Chim Acta. 2021;1156:338218. https://doi.org/10.1016/j.aca.2021.338218 .
doi: 10.1016/j.aca.2021.338218 pubmed: 33781460
Mattarozzi M, Giannetto M, Careri M. Electrochemical immunomagnetic assay as biosensing strategy for determination of ovarian cancer antigen HE4 in human serum. Talanta. 2020;217:120991. https://doi.org/10.1016/j.talanta.2020.120991 .
doi: 10.1016/j.talanta.2020.120991 pubmed: 32498877
Fortunati S, Rozzi A, Curti F, Giannetto M, Corradini R, Careri M. Novel amperometric genosensor based on peptide nucleic acid (PNA) probes immobilized on carbon nanotubes-screen printed electrodes for the determination of trace levels of non-amplified DNA in genetically modified (GM) soy. Biosens Bioelectron. 2019;129:7–14. https://doi.org/10.1016/j.bios.2019.01.020 .
doi: 10.1016/j.bios.2019.01.020 pubmed: 30682690
Menger M, Yarman A, Erdȍssy J, Yildiz HB, Gyurcsányi RE, Scheller FW. MIPs and aptamers for recognition of proteins in biomimetic sensing. Biosensors. 2016;6:35. https://doi.org/10.3390/bios6030035 .
doi: 10.3390/bios6030035 pmcid: 5039654
Yarman A, Kurbanoglu S, Zebger I, Scheller FW. Simple and robust: the claims of protein sensing by molecularly imprinted polymers. Sensor Actuat B. 2021;330:129369. https://doi.org/10.1016/j.snb.2020.129369 .
doi: 10.1016/j.snb.2020.129369
Mattarozzi M, Toma L, Bertucci A, Giannetto M, Careri M. Aptamer-based assays: strategies in the use of aptamers conjugated to magnetic micro- and nanobeads as recognition elements in food control. Anal Bioanal Chem. 2022;414:63–74. https://doi.org/10.1007/s00216-021-03501-6 .
doi: 10.1007/s00216-021-03501-6 pubmed: 34245326
McKeague M, De Girolamo A, Valenzano S, Pascale M, Ruscito A, Velu R, Frost NR, Hill K, Smith M, McConnell EM, DeRosa MC. Comprehensive analytical comparison of strategies used for small molecule aptamer evaluation. Anal Chem. 2015;87:8608–12. https://pubs.acs.org/doi/abs/10.1021/acs.analchem.5b02102 .
doi: 10.1021/acs.analchem.5b02102
Kotlarek D, Curti F, Vorobii M, Corradini R, Careri M, Knoll W, Rodriguez-Emmenegger C, Dostalek J. Surface plasmon resonance-based aptasensor for direct monitoring of thrombin in a minimally processed human blood. Sensors Act B Chem. 2020;320:128380. https://doi.org/10.1016/j.snb.2020.128380 .
doi: 10.1016/j.snb.2020.128380
Chang AL, McKeague M, Liang JC, Smolke CD. Kinetic and equilibrium binding characterization of aptamers to small molecules using a label-free, sensitive, and scalable platform. Anal Chem. 2014;7:3273–8. https://doi.org/10.1021/ac5001527 .
doi: 10.1021/ac5001527
Nowak PM, Śpiewak K, Woźniakiewicz M, Kościelniak P. Minimizing the impact of Joule heating as a prerequisite for the reliable analysis of metal-protein complexes by capillary electrophoresis. J Chromatogr A. 2017;1495:83–7. https://doi.org/10.1016/j.chroma.2017.03.028 .
doi: 10.1016/j.chroma.2017.03.028 pubmed: 28341433
Ashby J, Schachermeyer S, Duana Y, Jimenez LA, Zhong W. Probing and quantifying DNA–protein interactions with asymmetrical flow field-flow fractionation. J Chromatogr A. 2014;1358:217–24. https://doi.org/10.1016/j.chroma.2014.07.002 .
doi: 10.1016/j.chroma.2014.07.002 pubmed: 25064532
Marassi V, Roda B, Zattoni A, Tanase M, Reschiglian P. Hollow fiber flow field-flow fractionation and size-exclusion chromatography with multi-angle light scattering detection: a complementary approach in biopharmaceutical industry. J Chromatogr A. 2014;1372:196–203.
doi: 10.1016/j.chroma.2014.10.072
Wang L, Lee JY, Gao L, Yin J, Duan Y, Jimenez LA, Adkins GB, Ren W, Li L, Fang J, Wang Y, Song J, Zhong W. A DNA aptamer for binding and inhibition of DNA methyltransferase 1. Nucleic Acids Res. 2019;47(22):11527–37. https://doi.org/10.1093/nar/gkz1083 .
doi: 10.1093/nar/gkz1083 pubmed: 31733056 pmcid: 7145629
Wankar J, Bonvicini F, Benkovics G, Marassi V, Malanga M, Fenyvesi E, Gentilomi GA, Reschiglian P, Roda B, Manet I. Widening the therapeutic perspectives of clofazimine by its loading in sulfobutylether β-cyclodextrin nanocarriers: nanomolar IC 50 values against MDR S. epidermidis. Mol Pharmaceutics. 2018;15:3823–36. https://pubs.acs.org/doi/10.1021/acs.molpharmaceut.8b00321 .
doi: 10.1021/acs.molpharmaceut.8b00321
Roda B, Marassi V, Zattoni A, Borghi F, Anand R, Agostoni V, Gref R, Reschiglian P, Monti S. Flow field-flow fractionation and multi-angle light scattering as a powerful tool for the characterization and stability evaluation of drug-loaded metal–organic framework nanoparticles. Anal Bioanal Chem. 2018;410:5245–53. https://doi.org/10.1007/s00216-018-1176-6 .
doi: 10.1007/s00216-018-1176-6 pubmed: 29947896
Marassi V, Beretti F, Roda B, Alessandrini A, Facci P, Maraldi T, Zattoni A, Reschiglian P, Portolani M. A new approach for the separation, characterization and testing of potential prionoid protein aggregates through hollow-fiber flow field-flow fractionation and multi-angle light scattering. Anal Chim Acta. 2019;1087:121–30. https://doi.org/10.1016/j.aca.2019.08.003 .
doi: 10.1016/j.aca.2019.08.003 pubmed: 31585560
Bocca B, Battistini B, Petrucci F. Silver and gold and nanoparticles characterization by SP-ICP-MS and FFF-MALS-UV-ICP-MS in human samples used for biomonitoring. Talanta. 2020;220:121404. https://doi.org/10.1016/j.talanta.2020.121404 .
doi: 10.1016/j.talanta.2020.121404 pubmed: 32928420
Leeman M, Albers WM, Bombera R, Kuncova-Kallio J, Tuppurainen J, Nilsson L. Asymmetric flow field-flow fractionation coupled to surface plasmon resonance detection for analysis of therapeutic proteins in blood serum. Anal Bioanal Chem. 2021;413:117–27. https://doi.org/10.1007/s00216-020-03011-x .
doi: 10.1007/s00216-020-03011-x pubmed: 33098467
Schachermeyer S, Ashby J, Zhong W. Aptamer–protein binding detected by asymmetric flow field flow fractionation. J Chromatogr A. 2013;1295:107–13. https://doi.org/10.1016/j.chroma.2013.04.063 .
doi: 10.1016/j.chroma.2013.04.063 pubmed: 23688685
Melinte G, Selvolini G, Cristea C, Marrazza G. Aptasensors for lysozyme detection: recent advances. Talanta. 2021;226:122169. https://doi.org/10.1016/j.talanta.2021.122169 .
doi: 10.1016/j.talanta.2021.122169 pubmed: 33676711
Han B, Zhao C, Yin J, Wang H. High performance aptamer affinity chromatography for single-step selective extraction and screening of basic protein lysozyme. J Chromatogra B. 2012;903:112–7. https://doi.org/10.1016/j.jchromb.2012.07.003 .
doi: 10.1016/j.jchromb.2012.07.003
Mishra RK, Hayat A, Mishra GK, Catanante G, Sharma V, Marty J-L. A novel colorimetric competitive aptamer assay for lysozyme detection based on superparamagnetic nanobeads. Talanta. 2017;165:436–41. https://doi.org/10.1016/j.talanta.2016.12.083 .
doi: 10.1016/j.talanta.2016.12.083 pubmed: 28153279
Khan NI, Maddaus AG, Song E. A low-cost inkjet-printed aptamer-based electrochemical biosensor for the selective detection of lysozyme. Biosensors. 2018;8:7. https://doi.org/10.3390/bios8010007 .
doi: 10.3390/bios8010007 pmcid: 5872055
Mihai I, Vezeanu A, Polonschii C, Albu C, Radu G-L, Vasilescu A. Label-free detection of lysozyme in wines using an aptamer based biosensor and SPR detection. Sensor Actuat B. 2015;206:198–204. https://doi.org/10.1016/j.snb.2014.09.050 .
doi: 10.1016/j.snb.2014.09.050
Kirby R, Cho EJ, Gehrke B, Bayer T, Park YS, Neikirk DP, McDevitt JT, Ellington AD. Aptamer-based sensor arrays for the detection and quantitation of proteins. Anal Chem. 2004;76:4066–75. https://doi.org/10.1021/ac049858n .
doi: 10.1021/ac049858n pubmed: 15253644
Tran DT, Janssen KPF, Pollet J, Lammertyn E, Anné J, Van Schepdael A, Lammertyn J. Selection and characterization of DNA aptamers for egg white lysozyme. Molecules. 2010;15:1127–40. https://doi.org/10.3390/molecules15031127 .
doi: 10.3390/molecules15031127 pubmed: 20335968 pmcid: 6257241
Steinrauf LK, Shiuan D, Yang W-J, Chiang M. Lysozyme association with nucleic acids. Biochem Biophys Res Commun. 2000;266:366–70. https://doi.org/10.1006/bbrc.1999.1804 .
doi: 10.1006/bbrc.1999.1804

Auteurs

Valentina Marassi (V)

Department of Chemistry, University of Bologna, Via Selmi 2, Bologna, Italy. valentina.marassi2@unibo.it.
byFlow Srl, Bologna, Italy. valentina.marassi2@unibo.it.

Monica Mattarozzi (M)

Department of Chemistry, Life Sciences and Environmental Sustainability, University of Parma, Parco Area delle Scienze 17/A, 43124, Parma, Italy. monica.mattarozzi@unipr.it.

Lorenzo Toma (L)

Department of Chemistry, Life Sciences and Environmental Sustainability, University of Parma, Parco Area delle Scienze 17/A, 43124, Parma, Italy.

Stefano Giordani (S)

Department of Chemistry, University of Bologna, Via Selmi 2, Bologna, Italy.

Luca Ronda (L)

Department of Medicine and Surgery, University of Parma, Parco Area delle Scienze, 23/A, 43124, Parma, Italy.
Institute of Biophysics, CNR, 56124, Pisa, Italy.

Barbara Roda (B)

Department of Chemistry, University of Bologna, Via Selmi 2, Bologna, Italy.
byFlow Srl, Bologna, Italy.

Andrea Zattoni (A)

Department of Chemistry, University of Bologna, Via Selmi 2, Bologna, Italy.
byFlow Srl, Bologna, Italy.

Pierluigi Reschiglian (P)

Department of Chemistry, University of Bologna, Via Selmi 2, Bologna, Italy.
byFlow Srl, Bologna, Italy.

Maria Careri (M)

Department of Chemistry, Life Sciences and Environmental Sustainability, University of Parma, Parco Area delle Scienze 17/A, 43124, Parma, Italy.

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