Bimetallic Aluminum- and Niobium-Doped MCM-41 for Efficient Conversion of Biomass-Derived 2-Methyltetrahydrofuran to Pentadienes.

2-Methyltetrahydrofuran Cleavage of C−O Bond Niobium Sites Pentadienes

Journal

Angewandte Chemie (International ed. in English)
ISSN: 1521-3773
Titre abrégé: Angew Chem Int Ed Engl
Pays: Germany
ID NLM: 0370543

Informations de publication

Date de publication:
19 12 2022
Historique:
received: 17 08 2022
pubmed: 15 10 2022
medline: 15 12 2022
entrez: 14 10 2022
Statut: ppublish

Résumé

The production of conjugated C4-C5 dienes from biomass can enable the sustainable synthesis of many important polymers and liquid fuels. Here, we report the first example of bimetallic (Nb, Al)-atomically doped mesoporous silica, denoted as AlNb-MCM-41, which affords quantitative conversion of 2-methyltetrahydrofuran (2-MTHF) to pentadienes with a high selectivity of 91 %. The incorporation of Al

Identifiants

pubmed: 36240785
doi: 10.1002/anie.202212164
pmc: PMC10098840
doi:

Substances chimiques

Niobium 05175J654G
Aluminum CPD4NFA903
Alkadienes 0
MCM-41 0

Types de publication

Journal Article Research Support, Non-U.S. Gov't

Langues

eng

Sous-ensembles de citation

IM

Pagination

e202212164

Informations de copyright

© 2022 The Authors. Angewandte Chemie International Edition published by Wiley-VCH GmbH.

Références

Solid State Nucl Magn Reson. 2005 Sep;28(2-4):204-24
pubmed: 16216475
Angew Chem Int Ed Engl. 2021 Mar 1;60(10):5527-5535
pubmed: 33269513
Angew Chem Int Ed Engl. 2020 Aug 3;59(32):13260-13266
pubmed: 32413202
ChemSusChem. 2008;1(5):397-400
pubmed: 18702131
Angew Chem Int Ed Engl. 2013 Sep 9;52(37):9620-33
pubmed: 23893613
Nat Mater. 2020 Jan;19(1):86-93
pubmed: 31844281
Chem Soc Rev. 2013 May 7;42(9):3956-76
pubmed: 23132427
Nat Commun. 2016 Mar 30;7:11162
pubmed: 27025898
Chem Cent J. 2018 Oct 20;12(1):104
pubmed: 30343387
Angew Chem Int Ed Engl. 2022 Dec 19;61(51):e202212164
pubmed: 36240785

Auteurs

Mengtian Fan (M)

Department of Chemistry, University of Manchester, Manchester, M13 9PL, UK.

Shaojun Xu (S)

Department of Chemical Engineering, University of Manchester, Manchester, M13 9PL, UK.

Bing An (B)

Department of Chemistry, University of Manchester, Manchester, M13 9PL, UK.

Alena M Sheveleva (AM)

Department of Chemistry, University of Manchester, Manchester, M13 9PL, UK.

Alexander Betts (A)

Department of Chemistry, University of Manchester, Manchester, M13 9PL, UK.

Joseph Hurd (J)

Department of Chemical Engineering, University of Manchester, Manchester, M13 9PL, UK.

Zhaodong Zhu (Z)

Department of Chemistry, University of Manchester, Manchester, M13 9PL, UK.

Meng He (M)

Department of Chemistry, University of Manchester, Manchester, M13 9PL, UK.

Dinu Iuga (D)

Department of Physics, University of Warwick, Coventry, CV4 7AL, UK.

Longfei Lin (L)

Beijing National Laboratory for Molecular Sciences, Key Laboratory of Colloid and Interface and Thermodynamics, Institute of Chemistry, Chinese Academy of Sciences, Beijing, 100190, China.

Xinchen Kang (X)

Beijing National Laboratory for Molecular Sciences, Key Laboratory of Colloid and Interface and Thermodynamics, Institute of Chemistry, Chinese Academy of Sciences, Beijing, 100190, China.

Christopher M A Parlett (CMA)

Department of Chemical Engineering, University of Manchester, Manchester, M13 9PL, UK.
Diamond of Light Source, Harwell Science and Innovation Campus, Oxfordshire, OX11 0DE, UK.
University of Manchester at Harwell, Harwell Science and Innovation Campus, Oxfordshire, OX11 0DE, UK.

Floriana Tuna (F)

Department of Chemistry, University of Manchester, Manchester, M13 9PL, UK.

Eric J L McInnes (EJL)

Department of Chemistry, University of Manchester, Manchester, M13 9PL, UK.

Luke L Keenan (LL)

Diamond of Light Source, Harwell Science and Innovation Campus, Oxfordshire, OX11 0DE, UK.

Daniel Lee (D)

Department of Chemical Engineering, University of Manchester, Manchester, M13 9PL, UK.

Martin P Attfield (MP)

Department of Chemistry, University of Manchester, Manchester, M13 9PL, UK.

Sihai Yang (S)

Department of Chemistry, University of Manchester, Manchester, M13 9PL, UK.

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Classifications MeSH