Tailor-Made Poly(vinylamine) via Purple LED-Activated RAFT Polymerization of N-vinylformamide.

Polymerization Polyvinyls Spectrometry, Mass, Matrix-Assisted Laser Desorption-Ionization / methods
PI-RAFT poly(N-vinylformamide) poly(vinylamine) xanthate

Journal

Macromolecular rapid communications
ISSN: 1521-3927
Titre abrégé: Macromol Rapid Commun
Pays: Germany
ID NLM: 9888239

Informations de publication

Date de publication:
Feb 2023
Historique:
revised: 15 11 2022
received: 05 09 2022
pubmed: 30 11 2022
medline: 25 2 2023
entrez: 29 11 2022
Statut: ppublish

Résumé

Photo-iniferter reversible addition-fragmentation chain transfer (PI-RAFT) polymerization of N-vinylformamide (NVF) is demonstrated by using purple light. PNVFs with predetermined molar masses and narrow molar mass distributions are obtained. High RAFT chain-end fidelity is confirmed by matrix-assisted laser desorption ionization time-of-flight (MALDI-TOF) and electrospray-ionization time-of-flight mass spectrometry (ESI-TOF-MS), and chain extension experiment. To demonstrate the potential of this approach, an original poly(N-vinylpyrrolidone)-b-poly(N-vinylformamide) (PVP-b-PNVF) diblock copolymer is synthesized and characterized by aqueous size-exclusion chromatography (SEC), asymmetric flow field-flow fractionation (A4F), and

Identifiants

DOI: 10.1002/marc.202200729 PMID: 36443826
pubmed: 36443826
doi: 10.1002/marc.202200729
doi:

Substances chimiques

poly(vinylamine) 26336-38-9
poly(N-vinylformamide) 0
Polyvinyls 0

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

e2200729

Subventions

Organisme : Grant-in-Aid for Scientific Research on Innovative Areas
ID : JP22H04547

Informations de copyright

© 2022 The Authors. Macromolecular Rapid Communications published by Wiley-VCH GmbH.

Références

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Auteurs

Izabela Kurowska (I)

Laboratoire des IMRCP, UMR 5623, Université Paul Sabatier, CNRS, Toulouse, 31062, France.
Faculty of Chemistry, University of Bialystok, Ciolkowskiego 1k, Bialystok, 15-245, Poland.
Doctoral School of Exact and Natural Sciences, University of Bialystok, Ciolkowskiego 1k, Bialystok, 15-245, Poland.

Alexis Dupre-Demorsy (A)

Laboratoire des IMRCP, UMR 5623, Université Paul Sabatier, CNRS, Toulouse, 31062, France.
Division of Materials Science, Graduate School of Science and Technology, Nara Institute of Science and Technology, Ikoma, Nara, 630-0192, Japan.

Stéphane Balayssac (S)

Laboratoire des IMRCP, UMR 5623, Université Paul Sabatier, CNRS, Toulouse, 31062, France.

Marie Hennetier (M)

Université de Toulouse, Institut National Polytechnique de Toulouse - Ecole d'Ingénieur de Purpan, Département Sciences Agronomiques et Agroalimentaires, Toulouse Cedex 03, Toulouse, 31076, France.

Audrey Ric (A)

Université de Toulouse, Institut National Polytechnique de Toulouse - Ecole d'Ingénieur de Purpan, Département Sciences Agronomiques et Agroalimentaires, Toulouse Cedex 03, Toulouse, 31076, France.

Valérie Bourdon (V)

Institut de Chimie de Toulouse, UAR 2599, Université Paul Sabatier, CNRS, Toulouse, 31062, France.

Tsuyoshi Ando (T)

Division of Materials Science, Graduate School of Science and Technology, Nara Institute of Science and Technology, Ikoma, Nara, 630-0192, Japan.

Hiroharu Ajiro (H)

Division of Materials Science, Graduate School of Science and Technology, Nara Institute of Science and Technology, Ikoma, Nara, 630-0192, Japan.

Olivier Coutelier (O)

Laboratoire des IMRCP, UMR 5623, Université Paul Sabatier, CNRS, Toulouse, 31062, France.

Mathias Destarac (M)

Laboratoire des IMRCP, UMR 5623, Université Paul Sabatier, CNRS, Toulouse, 31062, France.
ORCID: 0000-0002-9718-2239

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Classifications MeSH

questionsmedicales.fr › Phénomènes chimiques › Polymérisation › Tailor-Made Poly(vinylamine) via Purple...
questionsmedicales.fr › Technologie, industrie et agriculture › Produits manufacturés › Matériaux biomédicaux et dentaires › Polymères › Matières plastiques › Polyvinyles › Tailor-Made Poly(vinylamine) via Purple...
questionsmedicales.fr › Techniques d'investigation › Techniques de chimie analytique › Spectrométrie de masse › Spectrométrie de masse MALDI › Tailor-Made Poly(vinylamine) via Purple...