The Highly Potent AhR Agonist Picoberin Modulates Hh-Dependent Osteoblast Differentiation.


Journal

Journal of medicinal chemistry
ISSN: 1520-4804
Titre abrégé: J Med Chem
Pays: United States
ID NLM: 9716531

Informations de publication

Date de publication:
22 12 2022
Historique:
pubmed: 3 12 2022
medline: 24 12 2022
entrez: 2 12 2022
Statut: ppublish

Résumé

Identification and analysis of small molecule bioactivity in target-agnostic cellular assays and monitoring changes in phenotype followed by identification of the biological target are a powerful approach for the identification of novel bioactive chemical matter in particular when the monitored phenotype is disease-related and physiologically relevant. Profiling methods that enable the unbiased analysis of compound-perturbed states can suggest mechanisms of action or even targets for bioactive small molecules and may yield novel insights into biology. Here we report the enantioselective synthesis of natural-product-inspired 8-oxotetrahydroprotoberberines and the identification of Picoberin, a low picomolar inhibitor of Hedgehog (Hh)-induced osteoblast differentiation. Global transcriptome and proteome profiling revealed the aryl hydrocarbon receptor (AhR) as the molecular target of this compound and identified a cross talk between Hh and AhR signaling during osteoblast differentiation.

Identifiants

pubmed: 36459434
doi: 10.1021/acs.jmedchem.2c00956
pmc: PMC9791665
doi:

Substances chimiques

Receptors, Aryl Hydrocarbon 0
Hedgehog Proteins 0

Types de publication

Journal Article Research Support, Non-U.S. Gov't

Langues

eng

Sous-ensembles de citation

IM

Pagination

16268-16289

Subventions

Organisme : Wellcome Trust
ID : 210664/Z/18/Z
Pays : United Kingdom

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Auteurs

Jana Flegel (J)

Department of Chemical Biology, Max Planck Institute of Molecular Physiology, Dortmund 44227, Germany.
Faculty of Chemistry, Chemical Biology, Technical University Dortmund, Dortmund 44227, Germany.

Saad Shaaban (S)

Department of Chemical Biology, Max Planck Institute of Molecular Physiology, Dortmund 44227, Germany.
Faculty of Chemistry, Institute of Organic Chemistry, University of Vienna Währinger Str. 38, Vienna 1090, Austria.

Zhi Jun Jia (ZJ)

Department of Chemical Biology, Max Planck Institute of Molecular Physiology, Dortmund 44227, Germany.
Key Laboratory of Birth Defects and Related Diseases of Women and Children, Evidence-Based Pharmacy Center, West China Second University Hospital, Sichuan University, Chengdu 610041, China.

Britta Schulte (B)

Department of Chemical Biology, Max Planck Institute of Molecular Physiology, Dortmund 44227, Germany.
Faculty of Chemistry, Chemical Biology, Technical University Dortmund, Dortmund 44227, Germany.

Yilong Lian (Y)

Ludwig Institute for Cancer Research, Nuffield Department of Clinical Medicine, University of Oxford, Oxford OX3 7DQ, United Kingdom.

Adrian Krzyzanowski (A)

Department of Chemical Biology, Max Planck Institute of Molecular Physiology, Dortmund 44227, Germany.
Faculty of Chemistry, Chemical Biology, Technical University Dortmund, Dortmund 44227, Germany.

Malte Metz (M)

Department of Chemical Biology, Max Planck Institute of Molecular Physiology, Dortmund 44227, Germany.

Tabea Schneidewind (T)

Department of Chemical Biology, Max Planck Institute of Molecular Physiology, Dortmund 44227, Germany.
Faculty of Chemistry, Chemical Biology, Technical University Dortmund, Dortmund 44227, Germany.

Fabian Wesseler (F)

Department of Chemical Biology, Max Planck Institute of Molecular Physiology, Dortmund 44227, Germany.
Faculty of Chemistry, Chemical Biology, Technical University Dortmund, Dortmund 44227, Germany.

Anke Flegel (A)

Department of Chemical Biology, Max Planck Institute of Molecular Physiology, Dortmund 44227, Germany.

Alisa Reich (A)

Department of Chemical Biology, Max Planck Institute of Molecular Physiology, Dortmund 44227, Germany.

Alexandra Brause (A)

Department of Chemical Biology, Max Planck Institute of Molecular Physiology, Dortmund 44227, Germany.

Gang Xue (G)

Department of Chemical Biology, Max Planck Institute of Molecular Physiology, Dortmund 44227, Germany.

Minghao Zhang (M)

Nuffield Department of Medicine, Target Discovery Institute, University of Oxford, Oxford, OX3 7FZ, UK.

Lara Dötsch (L)

Department of Chemical Biology, Max Planck Institute of Molecular Physiology, Dortmund 44227, Germany.
Faculty of Chemistry, Chemical Biology, Technical University Dortmund, Dortmund 44227, Germany.

Isabelle D Stender (ID)

Protein Chemistry Facility, Max Planck Institute of Molecular Physiology, Dortmund 44227, Germany.

Jan-Erik Hoffmann (JE)

Protein Chemistry Facility, Max Planck Institute of Molecular Physiology, Dortmund 44227, Germany.

Rebecca Scheel (R)

Faculty of Chemistry, Inorganic Chemistry, Technical University Dortmund, Dortmund 44227, Germany.

Petra Janning (P)

Department of Chemical Biology, Max Planck Institute of Molecular Physiology, Dortmund 44227, Germany.

Fraydoon Rastinejad (F)

Nuffield Department of Medicine, Target Discovery Institute, University of Oxford, Oxford, OX3 7FZ, UK.

Dennis Schade (D)

Dept. of Pharmaceutical & Medicinal Chemistry, Institute of Pharmacy, Christian-Albrechts-University of Kiel, Kiel 24118, Germany.

Carsten Strohmann (C)

Faculty of Chemistry, Inorganic Chemistry, Technical University Dortmund, Dortmund 44227, Germany.

Andrey P Antonchick (AP)

Department of Chemical Biology, Max Planck Institute of Molecular Physiology, Dortmund 44227, Germany.
Faculty of Chemistry, Chemical Biology, Technical University Dortmund, Dortmund 44227, Germany.
Department of Chemistry and Forensics, School of Science and Technology, Nottingham Trent University, Clifton Lane, Nottingham, NG11 8NS, United Kingdom.

Sonja Sievers (S)

Department of Chemical Biology, Max Planck Institute of Molecular Physiology, Dortmund 44227, Germany.
Compound Management and Screening Center, Dortmund 44227, Germany.

Pedro Moura-Alves (P)

Ludwig Institute for Cancer Research, Nuffield Department of Clinical Medicine, University of Oxford, Oxford OX3 7DQ, United Kingdom.
i3S-Instituto de Investigação e Inovação em Saúde, Universidade do Porto, 4200-135 Porto, Portugal.
IBMC-Instituto de Biologia Molecular e Celular, Universidade do Porto, 4200-135 Porto, Portugal.

Slava Ziegler (S)

Department of Chemical Biology, Max Planck Institute of Molecular Physiology, Dortmund 44227, Germany.

Herbert Waldmann (H)

Department of Chemical Biology, Max Planck Institute of Molecular Physiology, Dortmund 44227, Germany.
Faculty of Chemistry, Chemical Biology, Technical University Dortmund, Dortmund 44227, Germany.

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Classifications MeSH