Development of a green liquid-phase microextraction procedure using a customized device for the comprehensive determination of legacy and current pesticides in distinct types of wine samples.
Chemometrics
Customized devices
Gas chromatography
Green analytical chemistry
Mass spectrometry
Journal
Talanta
ISSN: 1873-3573
Titre abrégé: Talanta
Pays: Netherlands
ID NLM: 2984816R
Informations de publication
Date de publication:
01 Jan 2024
01 Jan 2024
Historique:
received:
04
04
2023
revised:
30
06
2023
accepted:
02
07
2023
medline:
20
9
2023
pubmed:
1
8
2023
entrez:
31
7
2023
Statut:
ppublish
Résumé
In this work, we reported the development of a novel, simple, and green liquid-phase microextraction (LPME) procedure based on the use of a customized device for the determination of 47 multiclass pesticides in red, white, and rosè wine samples by GC-MS. The main parameters that affect the LPME were optimized using multivariate statistical techniques such as centroid-simplex mixture design and Doehlert design. The optimal conditions were: 70 μL of toluene as extractor solvent; concentration of NaCl (2.7%, m v
Identifiants
pubmed: 37524042
pii: S0039-9140(23)00665-3
doi: 10.1016/j.talanta.2023.124914
pii:
doi:
Substances chimiques
Pesticides
0
Solvents
0
Fungicides, Industrial
0
Types de publication
Journal Article
Langues
eng
Sous-ensembles de citation
IM
Pagination
124914Informations de copyright
Copyright © 2023. Published by Elsevier B.V.
Déclaration de conflit d'intérêts
Declaration of competing interest The authors declare no conflict of interest.