Surface roughness and filler particles characterization of resin-based composites.

X-ray emission spectrometry composite resins filler particles scanning electron microscopy surface roughness

Journal

Microscopy research and technique
ISSN: 1097-0029
Titre abrégé: Microsc Res Tech
Pays: United States
ID NLM: 9203012

Informations de publication

Date de publication:
Oct 2019
Historique:
received: 07 03 2019
revised: 22 05 2019
accepted: 27 06 2019
pubmed: 18 7 2019
medline: 11 1 2020
entrez: 18 7 2019
Statut: ppublish

Résumé

The purpose of this study was to evaluate the surface roughness (Ra), and the morphology and composition of filler particles of different composites submitted to toothbrushing and water storage. Disc-shaped specimens (15 mm × 2 mm) were made from five composites: two conventional (Z100™, and Filtek™ Supreme Ultra Universal, 3M), one "quick-cure" (Estelite ∑ Quick, Tokuyama), one fluoride-releasing (Beautiful II, Shofu), and one self-adhering (Vertise Flow, Kerr) composite. Samples were finished/polished using aluminum oxide discs (Sof-Lex, 3M), and their surfaces were analyzed by profilometry (n = 5) and scanning electron microscopy (SEM; n = 3) at 1 week and after 30,000 toothbrushing cycles and 6-month water storage. Ra data were analyzed by two-way analysis of variance and Tukey's test (α = 0.05). Filler particles morphology and composition were analyzed by SEM and X-ray dispersive energy spectroscopy, respectively. Finishing/polishing resulted in similar Ra for all the composites, while toothbrushing and water storage increased the Ra of all the tested materials, also changing their surface morphology. Beautifil II and Vertise Flow presented the highest Ra after toothbrushing and water storage. Filler particles were mainly composed of silicon, zirconium, aluminum, barium, and ytterbium. Size and morphology of fillers, and composition of the tested composites influenced their Ra when samples were submitted to toothbrushing and water storage.

Identifiants

pubmed: 31313442
doi: 10.1002/jemt.23342
doi:

Substances chimiques

Acrylic Resins 0
Composite Dental Resin 0
Composite Resins 0
Polyurethanes 0

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

1756-1767

Subventions

Organisme : Fundação de Amparo à Pesquisa do Estado de São Paulo
ID : 2011/21670-9

Informations de copyright

© 2019 Wiley Periodicals, Inc.

Références

Abedin, F., Ye, Q., Parthasarathy, R., Misra, A., & Spencer, P. (2015). Polymerization behavior of hydrophilic-rich phase of dentin adhesive. Journal of Dental Research, 94, 500-507. https://doi.org/10.1177/0022034514565646
Abuna, G., Feitosa, V. P., Correr, A. B., Cama, G., Giannini, M., Sinhoreti, M. A., … Sauro, S. (2016). Bonding performance of experimental bioactive/biomimetic self-etch adhesives doped with calcium-phosphate fillers and biomimetic analogs of phosphoproteins. Journal of Dentistry, 52, 79-86. https://doi.org/10.1016/j.jdent.2016.07.016
Abzal, M. S., Rathakrishnan, M., Prakash, V., Vivekanandhan, P., Subbiya, A., & Sukumaran, V. G. (2016). Evaluation of surface roughness of three different composite resins with three different polishing systems. Journal of Conservative Dentistry, 19, 171-174. https://doi.org/10.4103/0972-0707.178703
Aker, D. A., Aker, J. R., & Sorensen, S. E. (1980). Toothbrush abrasion of color-corrective porcelain stains applied to porcelain-fused-to-metal restorations. The Journal of Prosthetic Dentistry, 44, 161-163. https://doi.org/10.1016/0022-3913(80)90130-4
Al-Samadani, K. H. (2016). Surface hardness of dental composite resin restorations in response to preventive agents. The Journal of Contemporary Dental Practice, 17, 978-984.
Alshali, R. Z., Salim, N. A., Satterthwaite, J. D., & Silikas, N. (2015). Long-term sorption and solubility of bulk-fill and conventional resin-composites in water and artificial saliva. Journal of Dentistry, 43, 1511-1518. https://doi.org/10.1016/j.jdent.2015.10.001
Anusavice, K. J., Shen, C., & Rawls, H. R. (2012). Phillips' science of dental materials (12th ed.). St. Louis: Saunders.
Atai, M., Nekoomanesh, M., Hashemi, S. A., & Amani, S. (2004). Physical and mechanical properties of an experimental dental composite based on a new monomer. Dental Materials, 20, 663-668. https://doi.org/10.1016/j.dental.2003.08.008
Attar, N. (2007). The effect of finishing and polishing procedures on the surface roughness of composite resin materials. The Journal of Contemporary Dental Practice, 8, 27-35.
Berger, S. B., Palialol, A. R., Cavalli, V., & Giannini, M. (2009). Characterization of water sorption, solubility and filler particles of light-cured composite resins. Brazilian Dental Journal, 20, 314-318.
Bollen, C. M., Lambrechts, P., & Quirynen, M. (1997). Comparison of surface roughness of oral hard materials to the threshold surface roughness for bacterial plaque retention: A review of the literature. Dental Materials, 13, 258-269.
Cazzaniga, G., Ottobelli, M., Ionescu, A., Garcia-Godoy, F., & Brambilla, E. (2015). Surface properties of resin-based composite materials and biofilm formation: A review of the current literature. American Journal of Dentistry, 28, 311-320.
Cazzaniga, G., Ottobelli, M., Ionescu, A. C., Paolone, G., Gherlone, E., Ferracane, J. L., & Brambilla, E. (2017). In vitro biofilm formation on resin-based composites after different finishing and polishing procedures. Journal of Dentistry, 67, 43-52. https://doi.org/10.1016/j.jdent.2017.07.012
Chinelatti, M. A., Chimello, D. T., Ramos, R. P., & Palma-Dibb, R. G. (2006). Evaluation of the surface hardness of composite resins before and after polishing at different times. Journal of Applied Oral Science, 14, 188-192.
Condo, R., Cerroni, L., Pasquantonio, G., Mancini, M., Pecora, A., Convertino, A., … Maiolo, L. (2017). A deep morphological characterization and comparison of different dental restorative materials. BioMed Research International, 2017, 7346317. https://doi.org/10.1155/2017/7346317
Cury, J. A., de Oliveira, B. H., dos Santos, A. P., & Tenuta, L. M. (2016). Are fluoride releasing dental materials clinically effective on caries control? Dental Materials, 32, 323-333. https://doi.org/10.1016/j.dental.2015.12.002
Cury, J. A., & Tenuta, L. M. A. (2014). Evidence-based recommendation on toothpaste use. Brazilian Oral Research, 28(Spec. Iss. 1), 1-7. https://doi.org/10.1590/S1806-83242014.50000001
Da Costa, J., Ferracane, J., Paravina, R. D., Mazur, R. F., & Roeder, L. (2007). The effect of different polishing systems on surface roughness and gloss of various resin composites. Journal of Esthetic and Restorative Dentistry, 19, 214-224. https://doi.org/10.1111/j.1708-8240.2007.00104.x
Davis, H. B., Gwinner, F., Mitchell, J. C., & Ferracane, J. L. (2014). Ion release from, and fluoride recharge of a composite with a fluoride-containing bioactive glass. Dental Materials, 30, 1187-1194. https://doi.org/10.1016/j.dental.2014.07.012
Di Francescantonio, M., Pacheco, R. R., Aguiar, T. R., Boaro, L. C. C., Braga, R. R., Martins, A. L., & Giannini, M. (2016). Evaluation of composition and morphology of filler particles in low-shrinkage and conventional composite resins carried out by means of SEM and EDX. Journal of Clinical Dentistry and Research, 13, 49-58. https://doi.org/10.14436/2447-911x.13.1.049-058.oar
Eliades, A., Birpou, E., Eliades, T., & Eliades, G. (2013). Self-adhesive restoratives as pit and fissure sealants: A comparative laboratory study. Dental Materials, 29, 752-762. https://doi.org/10.1016/j.dental.2013.04.005
Feng, L., Suh, B. I., & Shortall, A. C. (2010). Formation of gaps at the filler-resin interface induced by polymerization contraction stress: Gaps at the interface. Dental Materials, 26, 719-729. https://doi.org/10.1016/j.dental.2010.03.004
Ferracane, J. L. (2006). Hygroscopic and hydrolytic effects in dental polymer networks. Dental Materials, 22, 211-222. https://doi.org/10.1016/j.dental.2005.05.005
Ferracane, J. L. (2011). Resin composite-State of the art. Dental Materials, 27, 29-38. https://doi.org/10.1016/j.dental.2010.10.020
Froes-Salgado, N. R., Gajewski, V., Ornaghi, B. P., Pfeifer, C. S., Meier, M. M., Xavier, T. A., & Braga, R. R. (2015). Influence of the base and diluent monomer on network characteristics and mechanical properties of neat resin and composite materials. Odontology, 103, 160-168. https://doi.org/10.1007/s10266-014-0153-6
Fronza, B. M., Ayres, A., Pacheco, R. R., Rueggeberg, F. A., Dias, C., & Giannini, M. (2017). Characterization of inorganic filler content, mechanical properties, and light transmission of bulk-fill resin composites. Operative Dentistry, 42, 445-455. https://doi.org/10.2341/16-024-L
Furuse, A. Y., Gordon, K., Rodrigues, F. P., Silikas, N., & Watts, D. C. (2008). Colour-stability and gloss-retention of silorane and dimethacrylate composites with accelerated aging. Journal of Dentistry, 36, 945-952. https://doi.org/10.1016/j.jdent.2008.08.001
Garoushi, S., Vallittu, P. K., & Lassila, L. (2018). Characterization of fluoride releasing restorative dental materials. Dental Materials Journal, 37, 293-300. https://doi.org/10.4012/dmj.2017-161
Gonulol, N., Ozer, S., & Sen Tunc, E. (2015). Water sorption, solubility, and color stability of Giomer restoratives. Journal of Esthetic and Restorative Dentistry, 27, 300-306. https://doi.org/10.1111/jerd.12119
Gonulol, N., & Yilmaz, F. (2012). The effects of finishing and polishing techniques on surface roughness and color stability of nanocomposites. Journal of Dentistry, 40(Suppl 2), e64-e70. https://doi.org/10.1016/j.jdent.2012.07.005
Heintze, S. D., Forjanic, M., Ohmiti, K., & Rousson, V. (2010). Surface deterioration of dental materials after simulated toothbrushing in relation to brushing time and load. Dental Materials, 26, 306-319. https://doi.org/10.1016/j.dental.2009.11.152
Ilie, N., Kreppel, I., & Durner, J. (2014). Effect of radical amplified photopolymerization (RAP) in resin-based composites. Clinical Oral Investigations, 18, 1081-1088. https://doi.org/10.1007/s00784-013-1085-1
Imazato, S., Tarumi, H., Kato, S., Ebi, N., Ehara, A., & Ebisu, S. (1999). Water sorption, degree of conversion, and hydrophobicity of resins containing Bis-GMA and TEGDMA. Dental Materials Journal, 18, 124-132.
Ito, S., Hashimoto, M., Wadgaonkar, B., Svizero, N., Carvalho, R. M., Yiu, C., … Pashley, D. H. (2005). Effects of resin hydrophilicity on water sorption and changes in modulus of elasticity. Biomaterials, 26, 6449-6459. https://doi.org/10.1016/j.biomaterials.2005.04.052
Jin, J., Takahashi, R., Hickel, R., & Kunzelmann, K. H. (2014). Surface properties of universal and flowable nanohybrid composites after simulated tooth brushing. American Journal of Dentistry, 27, 149-154.
Jones, C. S., Billington, R. W., & Pearson, G. J. (2004). The in vivo perception of roughness of restorations. British Dental Journal, 196, 42-45; discussion 31. https://doi.org/10.1038/sj.bdj.4810881
Jung, M., Sehr, K., & Klimek, J. (2007). Surface texture of four nanofilled and one hybrid composite after finishing. Operative Dentistry, 32, 45-52. https://doi.org/10.2341/06-9
Kakuta, K., Wonglamsam, A., Goto, S., & Ogura, H. (2012). Surface textures of composite resins after combined wear test simulating both occlusal wear and brushing wear. Dental Materials Journal, 31, 61-67.
Kemaloglu, H., Karacolak, G., & Turkun, L. S. (2017). Can reduced-step polishers be as effective as multiple-step polishers in enhancing surface smoothness? Journal of Esthetic and Restorative Dentistry, 29, 31-40. https://doi.org/10.1111/jerd.12233
Khan, A. S., Aamer, S., Chaudhry, A. A., Wong, F. S., & Ur Rehman, I. (2013). Synthesis and characterizations of a fluoride-releasing dental restorative material. Materials Science & Engineering. C, Materials for Biological Applications, 33, 3458-3464. https://doi.org/10.1016/j.msec.2013.04.029
Kim, K. H., Ong, J. L., & Okuno, O. (2002). The effect of filler loading and morphology on the mechanical properties of contemporary composites. The Journal of Prosthetic Dentistry, 87, 642-649.
Klapdohr, S., & Moszner, N. (2005). New inorganic components for dental filling composites. Monatshefte für Chemie, 136, 21-45. https://doi.org/10.1007/s00706-004-0254-y
Kooi, T. J., Tan, Q. Z., Yap, A. U., Guo, W., Tay, K. J., & Soh, M. S. (2012). Effects of food-simulating liquids on surface properties of giomer restoratives. Operative Dentistry, 37, 665-671. https://doi.org/10.2341/11-419-L
Lai, G., Zhao, L., Wang, J., & Kunzelmann, K. H. (2018). Surface properties and color stability of dental flowable composites influenced by simulated toothbrushing. Dental Materials Journal, 37, 717-724. https://doi.org/10.4012/dmj.2017-233
Lim, B. S., Ferracane, J. L., Condon, J. R., & Adey, J. D. (2002). Effect of filler fraction and filler surface treatment on wear of microfilled composites. Dental Materials, 18, 1-11.
Lu, H., Lee, Y. K., Oguri, M., & Powers, J. M. (2006). Properties of a dental resin composite with a spherical inorganic filler. Operative Dentistry, 31, 734-740. https://doi.org/10.2341/05-154
Lu, H., Roeder, L. B., & Powers, J. M. (2003). Effect of polishing systems on the surface roughness of microhybrid composites. Journal of Esthetic and Restorative Dentistry, 15, 297-303 discussion 304.
Ludovichetti, F. S., Trindade, F. Z., Werner, A., Kleverlaan, C. J., & Fonseca, R. G. (2018). Wear resistance and abrasiveness of CAD-CAM monolithic materials. Journal of Prosthetic Dentistry, 120, 318.e1-318.e8. https://doi.org/10.1016/j.prosdent.2018.05.011
Macgregor, I. D., & Rugg-Gunn, A. J. (1985). Toothbrushing duration in 60 uninstructed young adults. Community Dentistry and Oral Epidemiology, 13, 121-122. https://doi.org/10.1111/j.1600-0528.1985.tb00423.x
Malavasi, C. V., Macedo, E. M., Souza Kda, C., Rego, G. F., Schneider, L. F., & Cavalcante, L. M. (2015). Surface texture and optical properties of self-adhering composite materials after toothbrush abrasion. The Journal of Contemporary Dental Practice, 16, 775-782.
Marghalani, H. Y. (2010). Effect of finishing/polishing systems on the surface roughness of novel posterior composites. Journal of Esthetic and Restorative Dentistry, 22, 127-138. https://doi.org/10.1111/j.1708-8240.2010.00324.x
McCabe, J. F., & Rusby, S. (2004). Water absorption, dimensional change and radial pressure in resin matrix dental restorative materials. Biomaterials, 25, 4001-4007. https://doi.org/10.1016/j.biomaterials.2003.10.088
Mine, A., De Munck, J., Van Ende, A., Poitevin, A., Matsumoto, M., Yoshida, Y., … Van Meerbeek, B. (2017). Limited interaction of a self-adhesive flowable composite with dentin/enamel characterized by TEM. Dental Materials, 33, 209-217. https://doi.org/10.1016/j.dental.2016.11.010
Naoum, S., Ellakwa, A., Martin, F., & Swain, M. (2011). Fluoride release, recharge and mechanical property stability of various fluoride-containing resin composites. Operative Dentistry, 36, 422-432. https://doi.org/10.2341/10-414-L
Nasoohi, N., Hoorizad, M., & Tabatabaei, S. F. (2017). Effects of wet and dry finishing and polishing on surface roughness and microhardness of composite resins. Journal of Dentistry (Tehran, Iran), 14, 69-75.
O'Neill, C., Kreplak, L., Rueggeberg, F. A., Labrie, D., Shimokawa, C. A. K., & Price, R. B. (2018). Effect of tooth brushing on gloss retention and surface roughness of five bulk-fill resin composites. Journal of Esthetic and Restorative Dentistry, 30, 59-69. https://doi.org/10.1111/jerd.12350
Park, C. A., Hyun, S. H., Lee, J. H., Seol, H. J., Kim, H. I., & Kwon, Y. H. (2007). Evaluation of polymerization in fluoride-containing composite resins. Journal of Materials Science. Materials in Medicine, 18, 1549-1556. https://doi.org/10.1007/s10856-007-3023-8
Peterson, J., Rizk, M., Hoch, M., & Wiegand, A. (2018). Bonding performance of self-adhesive flowable composites to enamel, dentin and a nano-hybrid composite. Odontology, 106, 171-180. https://doi.org/10.1007/s10266-017-0324-3
Peyton, J. H. (2004). Finishing and polishing techniques: Direct composite resin restorations. Practical Procedures & Aesthetic Dentistry, 16, 293-298 quiz 300.
Puckett, A. D., Fitchie, J. G., Kirk, P. C., & Gamblin, J. (2007). Direct composite restorative materials. Dental Clinics of North America, 51, 659-675, vii. https://doi.org/10.1016/j.cden.2007.04.003
Randolph, L. D., Palin, W. M., Leloup, G., & Leprince, J. G. (2016). Filler characteristics of modern dental resin composites and their influence on physico-mechanical properties. Dental Materials, 32, 1586-1599. https://doi.org/10.1016/j.dental.2016.09.034
Reis, A. F., Giannini, M., Lovadino, J. R., & Ambrosano, G. M. (2003). Effects of various finishing systems on the surface roughness and staining susceptibility of packable composite resins. Dental Materials, 19, 12-18.
Roselino Lde, M., Chinelatti, M. A., Alandia-Roman, C. C., & Pires-de-Souza Fde, C. (2015). Effect of brushing time and dentifrice abrasiveness on color change and surface roughness of resin composites. Brazilian Dental Journal, 26, 507-513. https://doi.org/10.1590/0103-6440201300399
Salgado, V. E., Cavalcante, L. M., Moraes, R. R., Davis, H. B., Ferracane, J. L., & Schneider, L. F. (2017). Degradation of optical and surface properties of resin-based composites with distinct nanoparticle sizes but equivalent surface area. Journal of Dentistry, 59, 48-53. https://doi.org/10.1016/j.jdent.2017.02.008
Salgado, V. E., Cavalcante, L. M., Silikas, N., & Schneider, L. F. (2013). The influence of nanoscale inorganic content over optical and surface properties of model composites. Journal of Dentistry, 41(Suppl 5), e45-e53. https://doi.org/10.1016/j.jdent.2013.05.011
Schemehorn, B. R., Moore, M. H., & Putt, M. S. (2011). Abrasion, polishing, and stain removal characteristics of various commercial dentifrices in vitro. The Journal of Clinical Dentistry, 22, 11-18.
Shibasaki, S., Takamizawa, T., Nojiri, K., Imai, A., Tsujimoto, A., Endo, H., … Miyazaki, M. (2017). Polymerization behavior and mechanical properties of high-viscosity bulk fill and low shrinkage resin composites. Operative Dentistry, 42, E177-E187. https://doi.org/10.2341/16-385-L
Shimokawa, C. A. K., Giannini, M., André, C. B., Sahadi, B. O., Faraoni, J. J., Palma-Dibb, R. G., … Price, R. B. (2019). In vitro evaluation of surface properties and wear resistance of conventional and bulk-fill resin-based composites after brushing with a dentifrice. Operative Dentistry. https://doi.org/10.2341/18-200-L
Shinohara, M. S., de Oliveira, M. T., Di Hipolito, V., Giannini, M., & de Goes, M. F. (2006). SEM analysis of the acid-etched enamel patterns promoted by acidic monomers and phosphoric acids. Journal of Applied Oral Science, 14, 427-435.
Sideridou, I., Tserki, V., & Papanastasiou, G. (2002). Effect of chemical structure on degree of conversion in light-cured dimethacrylate-based dental resins. Biomaterials, 23, 1819-1829.
Sideridou, I. D., Achilias, D. S., & Karabela, M. M. (2007). Sorption kinetics of ethanol/water solution by dimethacrylate-based dental resins and resin composites. Journal of Biomedical Materials Research. Part B, Applied Biomaterials, 81, 207-218. https://doi.org/10.1002/jbm.b.30655
Stamm, J. W. (2007). Multi-function toothpastes for better oral health: A behavioural perspective. International Dental Journal, 57, 351-363. https://doi.org/10.1111/j.1875-595X.2007.tb00162.x
Sturz, C. R., Faber, F. J., Scheer, M., Rothamel, D., & Neugebauer, J. (2015). Effects of various chair-side surface treatment methods on dental restorative materials with respect to contact angles and surface roughness. Dental Materials Journal, 34, 796-813. https://doi.org/10.4012/dmj.2014-098
Sunico, M. C., Shinkai, K., & Katoh, Y. (2005). Two-year clinical performance of occlusal and cervical giomer restorations. Operative Dentistry, 30, 282-289.
Takahashi, R., Jin, J., Nikaido, T., Tagami, J., Hickel, R., & Kunzelmann, K. H. (2013). Surface characterization of current composites after toothbrush abrasion. Dental Materials Journal, 32, 75-82.
Takanashi, E., Kishikawa, R., Ikeda, M., Inai, N., Otsuki, M., Foxton, R. M., & Tagami, J. (2008). Influence of abrasive particle size on surface properties of flowable composites. Dental Materials Journal, 27, 780-786.
Tamura, Y., Kakuta, K., & Ogura, H. (2013). Wear and mechanical properties of composite resins consisting of different filler particles. Odontology, 101, 156-169. https://doi.org/10.1007/s10266-012-0074-1
Terry, D. A., & Geller, W. (2004). Selection defines design. Journal of Esthetic and Restorative Dentistry, 16, 213-225 discussion 226.
Turssi, C. P., De Moraes Purquerio, B., & Serra, M. C. (2003). Wear of dental resin composites: Insights into underlying processes and assessment methods-A review. Journal of Biomedical Materials Research. Part B, Applied Biomaterials, 65, 280-285. https://doi.org/10.1002/jbm.b.10563
Van Landuyt, K. L., Nawrot, T., Geebelen, B., De Munck, J., Snauwaert, J., Yoshihara, K., … Van Meerbeek, B. (2011). How much do resin-based dental materials release? A meta-analytical approach. Dental Materials, 27, 723-747. https://doi.org/10.1016/j.dental.2011.05.001
Van Landuyt, K. L., Snauwaert, J., De Munck, J., Peumans, M., Yoshida, Y., Poitevin, A., … Van Meerbeek, B. (2007). Systematic review of the chemical composition of contemporary dental adhesives. Biomaterials, 28, 3757-3785. https://doi.org/10.1016/j.biomaterials.2007.04.044
Wang, L., Garcia, F. C., Amarante de Araujo, P., Franco, E. B., & Mondelli, R. F. (2004). Wear resistance of packable resin composites after simulated toothbrushing test. Journal of Esthetic and Restorative Dentistry, 16, 303-314 discussion 314-305.
Warangkulkasemkit, S., & Pumpaluk, P. (2018). Comparison of physical properties of three commercial composite core build up materials. Dental Materials Journal, 38, 177-181. https://doi.org/10.4012/dmj.2018-038
Wei, Y. J., Silikas, N., Zhang, Z. T., & Watts, D. C. (2011). Diffusion and concurrent solubility of self-adhering and new resin-matrix composites during water sorption/desorption cycles. Dental Materials, 27, 197-205. https://doi.org/10.1016/j.dental.2010.10.014
Wilson, N. H. F. (2007). Minimally invasive dentistry: The management of caries (1st ed.). Surrey: Quintessence Publishing.
Yadav, R. D., Raisingani, D., Jindal, D., & Mathur, R. (2016). A comparative analysis of different finishing and polishing devices on nanofilled, microfilled, and hybrid composite: A scanning electron microscopy and profilometric study. International Journal of Clinical Pediatric Dentistry, 9, 201-208. https://doi.org/10.5005/jp-journals-10005-1364
Yoshihara, K., Nagaoka, N., Hayakawa, S., Okihara, T., Yoshida, Y., & Van Meerbeek, B. (2018). Chemical interaction of glycero-phosphate dimethacrylate (GPDM) with hydroxyapatite and dentin. Dental Materials, 34, 1072-1081. https://doi.org/10.1016/j.dental.2018.04.003

Auteurs

Melissa A Ruivo (MA)

Department of Restorative Dentistry, Dental Materials Division, University of Campinas, Piracicaba Dental School, Piracicaba, SP, Brazil.

Rafael R Pacheco (RR)

Department of Restorative Dentistry, Dental Materials Division, University of Campinas, Piracicaba Dental School, Piracicaba, SP, Brazil.

Maicon Sebold (M)

Department of Restorative Dentistry, Operative Dentistry Division, University of Campinas, Piracicaba Dental School, Piracicaba, SP, Brazil.

Marcelo Giannini (M)

Department of Restorative Dentistry, Operative Dentistry Division, University of Campinas, Piracicaba Dental School, Piracicaba, SP, Brazil.

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