Periodic Nucleation of Calcium Phosphate in a Stirred Biocatalytic Reaction.


Journal

Angewandte Chemie (International ed. in English)
ISSN: 1521-3773
Titre abrégé: Angew Chem Int Ed Engl
Pays: Germany
ID NLM: 0370543

Informations de publication

Date de publication:
10 02 2020
Historique:
received: 03 09 2019
pubmed: 14 12 2019
medline: 9 1 2021
entrez: 14 12 2019
Statut: ppublish

Résumé

Highly ordered superstructures composed of inorganic nanoparticles appear in natural and synthetic systems, however the mechanisms of non-equilibrium self-organization that may be involved are still poorly understood. Herein, we performed a kinetic investigation of the precipitation of calcium phosphate using a process widely found in microorganisms: the hydrolysis of urea by enzyme urease. With high initial ratio of calcium ion to phosphate, periodic precipitation was obtained accompanied by pH oscillations in a well-stirred, closed reactor. We propose that an internal pH-regulated change in the concentration of phosphate ion is the driving force for periodicity. A simple model involving the biocatalytic reaction network coupled with burst nucleation of nanoparticles above a critical supersaturation reproduced key features of the experiments. These findings may provide insight to the self-organization of nanoparticles in biomineralization and improve design strategies of biomaterials for medical applications.

Identifiants

pubmed: 31833161
doi: 10.1002/anie.201911213
pmc: PMC7027757
doi:

Substances chimiques

Calcium Phosphates 0
Urea 8W8T17847W
calcium phosphate 97Z1WI3NDX
Urease EC 3.5.1.5

Types de publication

Journal Article Research Support, Non-U.S. Gov't

Langues

eng

Sous-ensembles de citation

IM

Pagination

2823-2828

Informations de copyright

© 2020 The Authors. Published by Wiley-VCH Verlag GmbH & Co. KGaA.

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Auteurs

Bíborka Bohner (B)

Department of Physical Chemistry and Materials Science, University of Szeged, Rerrich Béla tér 1., 6720, Szeged, Hungary.

Tamás Bánsági (T)

School of Chemistry, University of Birmingham, Edgbaston, Birmingham, B15 2TT, UK.

Ágota Tóth (Á)

Department of Physical Chemistry and Materials Science, University of Szeged, Rerrich Béla tér 1., 6720, Szeged, Hungary.

Dezső Horváth (D)

Department of Applied and Environmental Chemistry, University of Szeged, Rerrich Béla tér 1., 6720, Szeged, Hungary.

Annette F Taylor (AF)

Department of Chemical and Biological Engineering, University of Sheffield, Mappin Street, Sheffield, S1 3JD, UK.

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Classifications MeSH