Design and chemical synthesis of root gravitropism inhibitors: Bridged analogues of ku-76 have more potent activity.

Compositae Gravitropism Inhibitor Lactuca sativa Organic synthesis Structure modification

Journal

Phytochemistry
ISSN: 1873-3700
Titre abrégé: Phytochemistry
Pays: England
ID NLM: 0151434

Informations de publication

Date de publication:
Nov 2020
Historique:
received: 01 04 2020
revised: 22 08 2020
accepted: 25 08 2020
pubmed: 10 9 2020
medline: 11 11 2020
entrez: 9 9 2020
Statut: ppublish

Résumé

Previously, we found (2Z,4E)-5-phenylpenta-2,4-dienoic acid (ku-76) to be a selective inhibitor of root gravitropic bending of lettuce radicles at 5 μM, with no concomitant growth inhibition, and revealed the structure-activity relationship in this inhibitory activity. The conformation of ku-76 is flexible owing to the open-chain structure of pentan-2,4-dienoic acid with freely rotating single bonds, and the (2Z)-alkene moiety may be isomerized by external factors. To develop more potent inhibitors and obtain insight into the target biomolecules, various analogues of ku-76, fixed through conformation and/or configuration, were synthesized and evaluated. Stereochemical fixation was effective in improving the potency of gravitropic bending inhibition. Finally, we found highly potent conformational and/or configurational analogues (ku-257, ku-294 and ku-308), that did not inhibit root growth. The inhibition of root curvature by these analogues was comparable to that of naptalam.

Identifiants

pubmed: 32905916
pii: S0031-9422(20)30353-8
doi: 10.1016/j.phytochem.2020.112508
pii:
doi:

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

112508

Informations de copyright

Copyright © 2020 Elsevier Ltd. All rights reserved.

Auteurs

Mitsuru Shindo (M)

Institute for Materials Chemistry and Engineering, Kyushu University, Kasuga-koen, Kasuga, 816-8580, Japan. Electronic address: shindo@cm.kyushu-u.ac.jp.

Saki Makigawa (S)

Interdisciplinary Graduate School of Engineering Sciences, Kyushu University, Kasuga-koen, Kasuga, 816-8580, Japan.

Kozue Kodama (K)

Institute for Materials Chemistry and Engineering, Kyushu University, Kasuga-koen, Kasuga, 816-8580, Japan.

Hiromi Sugiyama (H)

Institute for Materials Chemistry and Engineering, Kyushu University, Kasuga-koen, Kasuga, 816-8580, Japan.

Kenji Matsumoto (K)

Institute for Materials Chemistry and Engineering, Kyushu University, Kasuga-koen, Kasuga, 816-8580, Japan.

Takayuki Iwata (T)

Institute for Materials Chemistry and Engineering, Kyushu University, Kasuga-koen, Kasuga, 816-8580, Japan.

Naoya Wasano (N)

International Environmental and Agricultural Sciences, Tokyo University of Agriculture and Technology, 3-5-8, Saiwai-cho, Fuchu, Tokyo, 183-8509, Japan.

Arihiro Kano (A)

Institute for Materials Chemistry and Engineering, Kyushu University, Kasuga-koen, Kasuga, 816-8580, Japan.

Miyo Terao Morita (MT)

Division of Plant Environmental Responses, National Institute for Basic Biology, Nishigonaka 38, Myodaiji, Okazaki, 444-8585, Japan.

Yoshiharu Fujii (Y)

International Environmental and Agricultural Sciences, Tokyo University of Agriculture and Technology, 3-5-8, Saiwai-cho, Fuchu, Tokyo, 183-8509, Japan.

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Classifications MeSH